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US4378380A Expired / Lapsed US ⏱️ 0.0 years remaining

Method for producing products enhanced with synthetic coffee grinder gas flavor

Assignee: General Electric Co
•
Filing: 1982-03-01
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Granted: 1983-03-29
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Expires: 2002-03-01
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Abstract

Abstract Known coffee flavor compounds including methyl mercaptan, a molar excess of carbonyl compounds and furfuryl mercaptan are combined in an aqueous solution of an inert, water-soluble carbohydrate at a preferred level of less than about 3% and then promptly dried, such as by spray-drying. These compounds may be fixed either separately or together. The dried fixed enhancer material is then combined with soluble coffee solids and/or soluble coffee-like solids powdered foodstuffs.

Inventors

  • 👤 Richard J. Scarpellino
  • 👤 Ellen Danielczik
  • 👤 Charles L. Teitelbaum

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-03 21:46
CPC Classifications
A; A23; A23F; A23F5/00; A23F5/44; A23F5/46; A23F5/465; A23L; A23L27/00; A23L27/70

Claims Analysis

Total Claims: 16
Claim 1
Independent Claim 194 words
A method for preparing a soluble, enhanced coffee-flavored foodstuff, coffee and/or coffee-like product comprising the steps of: (a) adding methyl mercaptan and a molar excess of carbonyl compounds, including for each mole of methyl mercaptan 2 to 50 moles of acetaldehyde, 0.02 to 3 moles of a 4 to 5 carbon alkane aldehyde and 0.2 to 5 moles of a lower alkane α-diketone selected from the group consisting of 2,3-butanedione, 2,3-pentanedione and mixtures thereof, to an aqueous solution of a non-reactive fixative, said materials being added in a total amount less than 10% by weight of the fixative, (b) drying the solution from step(a), (c) adding furfuryl mercaptan to an aqueous solution of a non-reactive fixative at a level below about 1% by weight of the fixative, (d) drying the solution of step (c), (e) combining the dried materials from steps (b) and (d) with soluble particles of a powdered foodstuff, coffee and/or coffee-like material, such that furfuryl mercaptan is present in an amount of from 2 to 8 parts per million by weight of the combined material and also present in an amount of from 1:4 to 2:1 by weight of methyl mercaptan.
Claim 2
Independent Claim 194 words
A method for preparing a soluble, enhanced coffee-flavored foodstuff, coffee and/or coffee-like product comprising the steps of: (a) adding methyl mercaptan and a molar excess of carbonyl compounds, including for each mole of methyl mercaptan 2 to 50 moles of acetaldehyde, 0.02 to 3 moles of a 4 to 5 carbon alkane aldehyde and 0.2 to 5 moles of a lower alkane α-diketone selected from the group consisting of 2,3-butanedione, 2,3-pentanedione and mixtures thereof, to an aqueous solution of a non-reactive fixative, said materials being added in a total amount less than 10% by weight of the fixative, (b) drying the solution from step(a), (c) adding furfuryl mercaptan to an aqueous solution of a non-reactive fixative at a level below about 1% by weight of the fixative, (d) drying the solution of step (c), (e) combining the dried materials from steps (b) and (d) with soluble particles of a powdered foodstuff, coffee and/or coffee-like material, such that furfuryl mercaptan is present in an amount of from 2 to 8 parts per million by weight of the combined material and also present in an amount of from 1:4 to 2:1 by weight of methyl mercaptan.
Claim 3
Dependent Claim 23 words
The method of claim 1 wherein the weight of materials added in step (a) in less than 3% by weight of the fixative.
Claim 4
Dependent Claim 19 words
The method of claim 2 wherein the drying in steps (b) and (d) is effected by low-temperature spray drying.
Claim 5
Independent Claim 27 words
The method of claims 2 or 3 wherein the dry combination of step (e) is agglomerated by means of saturated steam having a temperature below 135° C.
Claim 6
Dependent Claim 48 words
The method of claim 3 wherein one or more coffee enhancers having a boiling point in excess of 180° C. are added to the solution of step (c) at a level such that the total amount of enhancers fixed is less than 3% by weight of the fixative.
Claim 7
Dependent Claim 17 words
The method of claim 5 wherein 2-nonenol or 2-nonenal is added to the solution of step (c).
Claim 8
Dependent Claim 26 words
The method of claim 1 wherein the fixative of steps (a) and (c) is a hydrolyzed starch material having a dextrose equivalent of 10 or less.
Claim 9
Independent Claim 164 words
A method for preparing a soluble, enhanced coffee-flavored foodstuff, coffee and/or coffee-like product comprising the steps of: (a) adding methyl mercaptan, a molar excess of carbonyl compounds, including for each mole of methyl mercaptan 2 to 50 moles of acetaldehyde, 0.02 to 3 moles of a 4 to 5 carbon alkane aldehyde and 0.2 to 5 moles of a lower alkane α-diketone selected from the group consisting of 2,3-butanedione, 2,3-pentanedione and mixtures thereof, and furfural mercaptan in an amount of from 1:4 to 2:1 by weight of methyl mercaptan to an aqueous solution of a non-reactive fixation said materials being added in a total amount less than 10% by weight of the fixative. (b) drying the solution from step (a), (c) combining the said material from step (b) with soluble particles of a powdered foodstuff, a coffee and/or a coffee-like material such that furfuryl mercaptan is present in an amount of from 2 to 8 parts per million by weight of the combined material.
Claim 10
Independent Claim 164 words
A method for preparing a soluble, enhanced coffee-flavored foodstuff, coffee and/or coffee-like product comprising the steps of: (a) adding methyl mercaptan, a molar excess of carbonyl compounds, including for each mole of methyl mercaptan 2 to 50 moles of acetaldehyde, 0.02 to 3 moles of a 4 to 5 carbon alkane aldehyde and 0.2 to 5 moles of a lower alkane α-diketone selected from the group consisting of 2,3-butanedione, 2,3-pentanedione and mixtures thereof, and furfural mercaptan in an amount of from 1:4 to 2:1 by weight of methyl mercaptan to an aqueous solution of a non-reactive fixation said materials being added in a total amount less than 10% by weight of the fixative. (b) drying the solution from step (a), (c) combining the said material from step (b) with soluble particles of a powdered foodstuff, a coffee and/or a coffee-like material such that furfuryl mercaptan is present in an amount of from 2 to 8 parts per million by weight of the combined material.
Claim 11
Dependent Claim 23 words
The method of claim 8 wherein the weight of materials added to step (a) is less than 3% by weight of the fixative.
Claim 12
Independent Claim 74 words
The method of claims 8 or 9 wherein one or more coffee enhancers having a boiling point in excess of 180° C. are added to an aqueous solution of a non-reactive fixative at a level such that the total amount of enhancer fixed is less than 3% by weight of the fixation, said solution is dried and the dried material combined with the dry powdered foodstuff, soluble coffee or coffee-like material of step (c).
Claim 13
Dependent Claim 22 words
The method of claim 10 wherein 2-nonenol or 2-nonenal is added as a coffee enhancer having a boiling point about 180° C.
Claim 14
Dependent Claim 21 words
A method of claim 8 wherein the fixation is a hydrolyzed starch material having a dextrose equivalent of 10 or less.
Claim 15
Dependent Claim 14 words
The method of claim 8 wherein the drying is effected by low-temperature spray drying.
Claim 16
Dependent Claim 23 words
The method of claim 10 wherein the combined materials are is agglomerated by means of saturated steam having a temperature below 135° C.

References Cited (Backward Citations)

US1696419A Cited
US3852481A Cited
US4076852A Cited
US3973049A Cited
US4009291A Cited
US4041185A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1986-03-28 1986-09-27 1987-03-29 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1990-03-28 1990-09-27 1991-03-29 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1994-03-28 1994-09-27 1995-03-29 $7700.00 Window Closed / Lapsed

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