US4377602A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Process for the preparation of a hydrolyzed product from whole grain and such a product
Assignee: BIONOVA BV
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Filing: 1981-02-17
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Granted: 1983-03-22
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Expires: 2001-02-17
Abstract
Abstract The present invention relates to a process for the preparation of hydrolyzed products from whole grain, and such derived products. The invention solves the problem of obtaining a protein and sugar containing product able to be filtrated whereby this is achieved by treating whole grain, as wheat, maize, rye, barley, oat, and rice, with a proteolytic enzyme to transform waterinsoluble proteins into watersoluble products, and further to treat the starch contents with an amylase free from other carbohydrate hydrolyzing enzymes to form watersoluble starch products, as mono and disaccharides, removing the bran fraction and removing water to obtain a dry, semimoist, or liquid but concentrated derived product. The product is to be added as a sweetening agent in food products as bread, drinks, and cereal products, whereby the bran obtained can be used in bread as fiber additive.
Inventors
- 👤 Ernst Conrad
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-06 02:35
CPC Classifications
C; C12; C12C; C12C5/00; C12C5/004; A; A21; A21D; A21D13/00; A21D13/02; A23; A23C; A23C21/00; A23C21/02; A23J; A23J3/00; A23J3/30; A23J3/32; A23J3/34; A23J3/341; A23J3/343; A23L; A23L7/00; A23L7/10; A23L7/104; A23L7/107; C12C7/00; C12C7/01; C12C7/04; C12C9/00; C12G; C12G3/00; C12G3/02; C12G3/021; C13; C13K; C13K1/00; C13K1/06; A23V; A23V2002/00
Claims Analysis
Total Claims: 4
Claim 1
Independent Claim
206 words
A hydrolyzed protein and starch product prepared according to the process for preparing in situ, enzymatically hydrolyzed protein and starch products from whole grain, comprising crushing said grain and thereafter subjecting the crushed grain to a treatment which consists essentially of both the following steps: (a) subjecting said grain to an enzymatic treatment in an aqueous medium with an endopeptidase so as to transform substantially all water-insoluble proteins present in the grain to water-soluble protein products, which thereafter are filtered and recovered from the crushed grain as a clear filtrate containing protein products containing about 50 to 60% peptides having at least 25 amino acid residues, 35 to 45% peptides having between about 5 to 20 amino acid residues and 4-8% peptides having up to 4 amino acid residues and subjecting the remaining crushed grain to (b) an enzymatic treatment in an aqueous medium with α-amylase followed sequentially by an amyloglucosidase both enzymes substantially free from other carbohydrate hydrolyzing enzymes so as to transform substantially all the water-insoluble starch fraction in the grain to watersoluble, degraded products of starch, wherein the amyloglucosidase is at a pH of between 4 to 4.5, so as to transform substantially all the water-insoluble starch fractions in the grain to glucose.
Claim 2
Dependent Claim
206 words
A hydrolyzed protein and starch product prepared according to the process for preparing in situ, enzymatically hydrolyzed protein and starch products from whole grain, comprising crushing said grain and thereafter subjecting the crushed grain to a treatment which consists essentially of both the following steps: (a) subjecting said grain to an enzymatic treatment in an aqueous medium with an endopeptidase so as to transform substantially all water-insoluble proteins present in the grain to water-soluble protein products, which thereafter are filtered and recovered from the crushed grain as a clear filtrate containing protein products containing about 50 to 60% peptides having at least 25 amino acid residues, 35 to 45% peptides having between about 5 to 20 amino acid residues and 4-8% peptides having up to 4 amino acid residues and subjecting the remaining crushed grain to (b) an enzymatic treatment in an aqueous medium with α-amylase followed sequentially by an amyloglucosidase both enzymes substantially free from other carbohydrate hydrolyzing enzymes so as to transform substantially all the water-insoluble starch fraction in the grain to watersoluble, degraded products of starch, wherein the amyloglucosidase is at a pH of between 4 to 4.5, so as to transform substantially all the water-insoluble starch fractions in the grain to glucose.
Claim 3
Dependent Claim
238 words
The hydrolyzed protein and starch products prepared according to the process for preparing in situ, enzymatically hydrolyzed protein and starch products from whole grain, comprising crushing said grain and thereafter subjecting the crushed grain to a treatment which consists essentially of both the following steps: (a) subjecting said grain to an enzymatic treatment in an aqueous medium with an endopeptidase so as to transform substantially all water-insoluble proteins present in the grain to water-soluble protein products, which thereafter are filtered and recovered from the crushed grain as a clear filtrate containing protein products containing about 50 to 60% peptides having at least 25 amino acid residues, 35 to 45% peptides having between about 5 to 20 amino acid residues and 4-8% peptides having up to 4 amino acid residues and subjecting the remaining crushed grain to (b) an enzymatic treatment in an aqueous medium with at least one starch hydrolyzing enzyme so as to transform substantially all of the water-insoluble starch fraction in the grain to water-soluble, degraded products of starch, and wherein the starch hydrolyzing enzyme is amylase substantially free from other carbohydrate hydrolyzing enzymes, Wherein upon completion of process steps (a) and (b) any remaining water-insoluble husk components of said grain such as bran and water-insoluble starch components are separated, wherein said husk component, after washing, contain at least about 60% by weight of fibers and no more than about 2% by weight of residual starch.
Claim 4
Dependent Claim
238 words
The hydrolyzed protein and starch products prepared according to the process for preparing in situ, enzymatically hydrolyzed protein and starch products from whole grain, comprising crushing said grain and thereafter subjecting the crushed grain to a treatment which consists essentially of both the following steps: (a) subjecting said grain to an enzymatic treatment in an aqueous medium with an endopeptidase so as to transform substantially all water-insoluble proteins present in the grain to water-soluble protein products, which thereafter are filtered and recovered from the crushed grain as a clear filtrate containing protein products containing about 50 to 60% peptides having at least 25 amino acid residues, 35 to 45% peptides having between about 5 to 20 amino acid residues and 4-8% peptides having up to 4 amino acid residues and subjecting the remaining crushed grain to (b) an enzymatic treatment in an aqueous medium with at least one starch hydrolyzing enzyme so as to transform substantially all of the water-insoluble starch fraction in the grain to water-soluble, degraded products of starch, and wherein the starch hydrolyzing enzyme is amylase substantially free from other carbohydrate hydrolyzing enzymes, Wherein upon completion of process steps (a) and (b) any remaining water-insoluble husk components of said grain such as bran and water-insoluble starch components are separated, wherein said husk component, after washing, contain at least about 60% by weight of fibers and no more than about 2% by weight of residual starch.
References Cited (Backward Citations)
US2051017A
Cited
US3157513A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1986-03-21 | 1986-09-20 | 1987-03-22 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1990-03-21 | 1990-09-20 | 1991-03-22 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1994-03-21 | 1994-09-20 | 1995-03-22 | $7700.00 | Window Closed / Lapsed |