← Back to Patent Explorer
US4376083A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for the preparation of aluminum-containing high-energy explosive compositions

Assignee: Dyno Industrier AS
•
Filing: 1981-01-26
•
Granted: 1983-03-08
•
Expires: 2001-01-26
📄 Original PDF 🌐 Google Patents 🔄 Sync Now

Abstract

Abstract A castable high-energy explosive composition comprising trinitrotoluene (TNT) and crystalline explosives of the RDX or HMX type as well as aluminum powder, and, optionally, flegmatizing agents and stablizers consisting of wax, lecithin and nitrocellulose (NC), is prepared by dispersing crystals of RDX (or HMX) in water with wax, under heavy stirring and a temperature above the melting point of the wax, then adding aluminum powder, treated in order to tolerate water, to the dispersion, and then, optionally, cooling in order to separate the explosive as granules. A further step comprises melting and dispersing TNT in hot water under heavy stirring, optionally under the addition of wetted NC and lecithin, then reducing the temperature to below 80° C., and separating the solidifying, dispersed explosive droplets in the form of granules. The final step comprises mixing the products from the former steps in specific ratios so as to provide the final explosive compositions known by the name "Hexotonal" or "Octonal", respectively. Alternatively, the mixtures of granules from the first two steps are melted together and cast on a drum, ribbon or plate, or the first two are combined in the same reactor before any part of the dispersed phases has solidified.

Inventors

  • 👤 Kare Ulsteen

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-29 08:22
CPC Classifications
C; C06; C06B; C06B25/00; C06B25/34; C06B21/00; C06B21/0033; C06B21/005; C06B21/0066

Claims Analysis

Total Claims: 16
Claim 1
Independent Claim 96 words
A process for the preparation of a castable, high-energy explosive composition comprising trinitrotoluene (TNT), RDX or HMX crystalline explosive and aluminum powder, comprising the following steps: A. dispersing wax and crystals of RDX or HMX in water with heavy stirring at a temperature above the melting point of the wax, then adding aluminum powder, treated in order to tolerate water, to the dispersion, thereby forming a dispersed mixture, cooling the mixture and separating it in the form of granules; and B. combining TNT with said dispersed mixture or with said granules, thereby obtaining said castable composition.
Claim 2
Dependent Claim 96 words
A process for the preparation of a castable, high-energy explosive composition comprising trinitrotoluene (TNT), RDX or HMX crystalline explosive and aluminum powder, comprising the following steps: A. dispersing wax and crystals of RDX or HMX in water with heavy stirring at a temperature above the melting point of the wax, then adding aluminum powder, treated in order to tolerate water, to the dispersion, thereby forming a dispersed mixture, cooling the mixture and separating it in the form of granules; and B. combining TNT with said dispersed mixture or with said granules, thereby obtaining said castable composition.
Claim 3
Dependent Claim 50 words
A process according to claim 1, wherein the TNT of step B is separately melted and dispersed in hot water with heavy stirring, the temperature is reduced to below 80° C., granules of TNT are separated and are combined with the granules obtained from the dispersed mixture of step A.
Claim 4
Dependent Claim 29 words
A process according to claim 2, wherein the combined granules are melted together and the melt is cast on a drum, ribbon or plate, thereby producing a plate granulate.
Claim 5
Dependent Claim 39 words
A process according to claim 1, wherein the TNT of step B is combined with the dispersed mixture of step A forming a combined mixture which is cooled and separated in the form of granules of said castable composition.
Claim 6
Dependent Claim 18 words
A process according to claim 1, wherein lecithin and nitrocellulose are added to the dispersion of step A.
Claim 7
Dependent Claim 18 words
A process according to claim 2, wherein lecithin and nitrocellulose are added to the separate dispersion of TNT.
Claim 8
Dependent Claim 17 words
A process according to claim 6, wherein additionally wax is added to the separate dispersion of TNT.
Claim 9
Dependent Claim 16 words
A process according to claim 1, wherein the wax in step A is pure montan wax.
Claim 10
Dependent Claim 17 words
A process according to claim 1, wherein the wax is petroleum wax admixed with refined montan wax.
Claim 11
Dependent Claim 22 words
A process according to claim 9, wherein the refined montan wax amounts to 1 to 12%, calculated on the total wax amount.
Claim 12
Dependent Claim 22 words
A process according to claim 8 or 9, wherein the montan wax is KP wax or S wax, separately or in admixture.
Claim 13
Dependent Claim 38 words
A process according to claim 1, wherein the obtained castable composition is composed of the following, by weight: ______________________________________ RDX or HMX 25 to 50% TNT 25 to 50% Al 13 to 37% Wax up to 7%. ______________________________________
Claim 14
Dependent Claim 46 words
A process according to claim 5 wherein the obtained castable composition is composed of the following, by weight: ______________________________________ RDX or HMX 25 to 50% TNT 25 to 50% Al 13 to 37% Wax up to 7% Nitrocellulose up to 3% Lecithin up to 2%. ______________________________________
Claim 15
Dependent Claim 35 words
A process according to claim 6 wherein the obtained TNT granules are composed of the following, by weight: ______________________________________ TNT 8 to 30 parts Nitrocellulose 0.5 to 3 parts Lecithin 0.1 to 0.5 parts. ______________________________________
Claim 16
Dependent Claim 40 words
A process according to claim 7, wherein the obtained TNT granules are composed of the following by weight: ______________________________________ TNT 8 to 20 parts Nitrocellulose 0.5 to 3 parts Lecithin 0.1 to 0.5 parts Wax up to 20 parts. ______________________________________

References Cited (Backward Citations)

US2982641A Cited
GB1183916A Cited
US3706609A Cited
US4089715A Cited
US4100000A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1986-03-07 1986-09-06 1987-03-08 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1990-03-07 1990-09-06 1991-03-08 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1994-03-07 1994-09-06 1995-03-08 $7700.00 Window Closed / Lapsed

Assigned Categories & Tags

No categories assigned to this patent yet.

Assign Category Tag