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US4366271A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for the production of colorant preparations and the colorant preparations obtained thereby

Assignee: Novartis Corp
•
Filing: 1981-05-26
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Granted: 1982-12-28
•
Expires: 2001-05-26
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Abstract

Abstract An improved flush process for the production of a colorant composition, which involves mixing a colorant in the presence of water with the organic carrier material in a kneader at a temperature sufficient to melt said organic carrier material and flushing the colorant onto the organic carrier material with the concomitant formation of a colorant-free separate water phase, wherein the improvement consists essentially of kneading the mixture of molten colorant composition and separate colorant-free water while cooling the kneader and the mixture to a temperature below the softening point of the organic carrier, a temperature sufficient to cause the molten colorant composition to solidify, and concomitantly comminuting the solidified colorant composition into broken, irregular granulates in the presence of the colorant-free water.

Inventors

  • 👤 Albert Riegler

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-07 19:38
CPC Classifications
C; C09; C09B; C09B67/00; C09B67/0071; C09B67/0092; C09B67/0095; C08; C08J; C08J3/00; C08J3/20; C08J3/205; C08J3/2053; C08J3/2056; C08J3/22; C08J3/226

Claims Analysis

Total Claims: 10
Claim 1
Independent Claim 271 words
In an improved flush process for the production of a colorant composition, which contains, by weight of the total composition, 10 to 90% of a water-insoluble colorant and 90 to 10% of a water-repellent organic carrier material, which involves mixing a colorant in the presence of water with the organic carrier material, which material has a softening point between 60° and 100° C., in a kneader at a temperature sufficient to melt said organic carrier material and flushing the colorant into the organic carrier material with the concomitant formation of a colorant-free separate water phase, wherein the improvement consists essentially of (a) mixing the organic carrier material with an aqueous colorant paste or with a dry colorant and water, in a kneader and heating the kneader to a temperature sufficient to melt said organic carrier material, or adding the organic carrier material, at room temperature, to a kneader preheated to a temperature sufficient to melt said organic carrier material and then adding dry colorant and water or an aqueous colorant paste to the now molten organic carrier material in the heated kneader, (b) kneading the mixture of colorant, water and molten organic carrier material to flush the colorant into the molten organic carrier material to form a molten colorant composition with the concomitant formation of a colorant-free separate water phase, (c) now cooling the kneader, while continuing kneading, to a temperature below the softening point of the organic carrier, a temperature sufficient to cause the molten colorant composition to solidify, and concomitantly (d) comminuting the solidified colorant composition into broken irregular granulates in the presence of the colorant-free separate water phase.
Claim 2
Dependent Claim 271 words
In an improved flush process for the production of a colorant composition, which contains, by weight of the total composition, 10 to 90% of a water-insoluble colorant and 90 to 10% of a water-repellent organic carrier material, which involves mixing a colorant in the presence of water with the organic carrier material, which material has a softening point between 60° and 100° C., in a kneader at a temperature sufficient to melt said organic carrier material and flushing the colorant into the organic carrier material with the concomitant formation of a colorant-free separate water phase, wherein the improvement consists essentially of (a) mixing the organic carrier material with an aqueous colorant paste or with a dry colorant and water, in a kneader and heating the kneader to a temperature sufficient to melt said organic carrier material, or adding the organic carrier material, at room temperature, to a kneader preheated to a temperature sufficient to melt said organic carrier material and then adding dry colorant and water or an aqueous colorant paste to the now molten organic carrier material in the heated kneader, (b) kneading the mixture of colorant, water and molten organic carrier material to flush the colorant into the molten organic carrier material to form a molten colorant composition with the concomitant formation of a colorant-free separate water phase, (c) now cooling the kneader, while continuing kneading, to a temperature below the softening point of the organic carrier, a temperature sufficient to cause the molten colorant composition to solidify, and concomitantly (d) comminuting the solidified colorant composition into broken irregular granulates in the presence of the colorant-free separate water phase.
Claim 3
Dependent Claim 12 words
A process according to claim 1, wherein the colorant is a pigment.
Claim 4
Dependent Claim 16 words
A process according to claim 1, wherein the water-repellant organic carrier material is a thermoplastic resin.
Claim 5
Dependent Claim 14 words
A process according to claim 3, wherein the thermoplastic resin is a polyacrylic resin.
Claim 6
Dependent Claim 14 words
A process according to claim 3, wherein the thermoplastic resin is a hydrocarbon resin.
Claim 7
Dependent Claim 15 words
A process according to claim 3, wherein the thermoplastic resin is an ethylene/vinyl acetate copolymer.
Claim 8
Dependent Claim 19 words
A process according to claim 6, wherein the ethylene/vinyl acetate copolymer contains 5 to 30% by weight vinyl acetate.
Claim 9
Dependent Claim 24 words
A process according to claim 6, wherein a polyolefin wax, a metal soap or mixture thereof are also present with the ethlylene/vinyl acetate copolymer.
Claim 10
Dependent Claim 10 words
A colorant composition produced by the process of claim 1.

References Cited (Backward Citations)

US2755195A Cited
AT233699B Cited
US3308211A Cited
GB1155550A Cited
US3582384A Cited
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GB1323086A Cited
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GB1542369A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1985-12-27 1986-06-28 1986-12-28 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1989-12-27 1990-06-28 1990-12-28 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1993-12-27 1994-06-28 1994-12-28 $7700.00 Window Closed / Lapsed

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