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US4353758A Expired / Lapsed US ⏱️ 0.0 years remaining

Direct process for explosives

Assignee: Individual
•
Filing: 1979-11-29
•
Granted: 1982-10-12
•
Expires: 1999-11-29
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Abstract

Abstract A direct process of making ethylenediamine dinitrate through the reaction of ethylenediamine and ammonium nitrate.

Inventors

  • 👤 Irving B. Akst
  • 👤 Mary M. Stinecipher

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-25 22:07
CPC Classifications
C; C06; C06B; C06B31/00; C06B31/28; C06B31/32

Claims Analysis

Total Claims: 4
Claim 1
Independent Claim 73 words
A method of forming an explosive mixture of ammonium nitrate and ethylenediamine dinitrate which comprises: (a) combining ethylenediamine and a stoichiometric excess of ammonium nitrate, said ammonium nitrate being present in an amount to form, after reaction of said ethylenediamine therewith, a mixture of ammonium nitrate and ethylenediamine dinitrate; and (b) reacting said ethylenediamine with the stoichiometric portion of said ammonium dinitrate to form said explosive mixture of ammonium nitrate and ethylenediamine dinitrate.
Claim 2
Independent Claim 73 words
A method of forming an explosive mixture of ammonium nitrate and ethylenediamine dinitrate which comprises: (a) combining ethylenediamine and a stoichiometric excess of ammonium nitrate, said ammonium nitrate being present in an amount to form, after reaction of said ethylenediamine therewith, a mixture of ammonium nitrate and ethylenediamine dinitrate; and (b) reacting said ethylenediamine with the stoichiometric portion of said ammonium dinitrate to form said explosive mixture of ammonium nitrate and ethylenediamine dinitrate.
Claim 3
Dependent Claim 26 words
The method of claim 1 wherein the mixture of step (b) is heated to form a uniform melt and thereafter cooled to solidify said uniform melt.
Claim 4
Independent Claim 18 words
The method of claims 1 or 2 wherein said explosive mixture of step (b) is an eutectic mixture.

References Cited (Backward Citations)

US1968158A Cited
US2165470A Cited
US2168562A Cited
US3013382A Cited
US3082593A Cited
US3431155A Cited
US3471346A Cited
AU1773476A Cited
US4110136A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1985-10-11 1986-04-12 1986-10-12 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1989-10-11 1990-04-12 1990-10-12 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1993-10-11 1994-04-12 1994-10-12 $7700.00 Window Closed / Lapsed

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