US4347118A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Solvent extraction process for tar sands
Assignee: ExxonMobil Technology and Engineering Co
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Filing: 1979-10-01
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Granted: 1982-08-31
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Expires: 1999-10-01
Abstract
Abstract A solvent extraction process for tar sands is disclosed wherein a low boiling solvent having a normal boiling point of from 20 DEG to 70 DEG C. is used to extract tar sands. The solvent is mixed with tar sands in a dissolution zone, the solvent:bitumen weight ratio being maintained at from about 0.5:1 to 2:1. This mixture is passed to a separation zone in which bitumen and inorganic fines are separated from extracted sand, the separation zone containing a classifier and countercurrent extraction column. The extracted sand is introduced into a first fluid-bed drying zone fluidized by heated solvent vapors, so as to remove unbound solvent from extracted sand while at the same time lowering the water content of the sand to less than about 2 wt. %. The so-treated sand is then passed into a second fluid-bed drying zone fluidized by a heated inert gas to remove bound solvent. Recovered solvent is recycled to the dissolution zone.
Inventors
- 👤 Edward W. Funk
- 👤 Walter G. May
- 👤 James C. Pirkle, Jr.
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-03 19:50
CPC Classifications
C; C10; C10G; C10G1/00; C10G1/04; C10G1/006; Y; Y10; Y10S; Y10S208/00; Y10S208/951
Claims Analysis
Total Claims: 9
Claim 1
Independent Claim
210 words
A process for solvent extraction of bitumen from tar sands containing water and inorganic fines and recovering the solvent which comprises mixing the tar sands in a dissolution zone with C 5 to C 6 hydrocarbon solvent having a normal boiling point of from about 25° to 60° C.; maintaining the solvent to bitumen weight ratio in the dissolution zone at from about 0.5:1 to 1.5:1; passing the resultant mixture to a classifier wherein an overflow of a viscous mixture of bitumen and inorganic fines is separated from an underflow of extracted sand, then passing the underflow of extracted sand through a countercurrent extraction column wherein the sand is further extracted; introducing the extracted sand into a first fluid-bed drying zone fluidized by C 5 to C 6 hydrocarbon solvent vapors and heated to a drying temperature which is about 25° to 60° C. higher than the normal boiling point of said C 5 to C 6 hydrocarbon solvent, wherein unbound solvent is removed from extracted sand and the sand water content is lowered to less than about 2 wt.%; and conducting the so-treated sand to a second fluid-bed drying zone fluidized by inert gas heated to a temperature of from 25° to 100° C. wherein bound solvent is removed.
Claim 2
Dependent Claim
210 words
A process for solvent extraction of bitumen from tar sands containing water and inorganic fines and recovering the solvent which comprises mixing the tar sands in a dissolution zone with C 5 to C 6 hydrocarbon solvent having a normal boiling point of from about 25° to 60° C.; maintaining the solvent to bitumen weight ratio in the dissolution zone at from about 0.5:1 to 1.5:1; passing the resultant mixture to a classifier wherein an overflow of a viscous mixture of bitumen and inorganic fines is separated from an underflow of extracted sand, then passing the underflow of extracted sand through a countercurrent extraction column wherein the sand is further extracted; introducing the extracted sand into a first fluid-bed drying zone fluidized by C 5 to C 6 hydrocarbon solvent vapors and heated to a drying temperature which is about 25° to 60° C. higher than the normal boiling point of said C 5 to C 6 hydrocarbon solvent, wherein unbound solvent is removed from extracted sand and the sand water content is lowered to less than about 2 wt.%; and conducting the so-treated sand to a second fluid-bed drying zone fluidized by inert gas heated to a temperature of from 25° to 100° C. wherein bound solvent is removed.
Claim 3
Dependent Claim
10 words
The process of claim 1 wherein the solvent is pentane.
Claim 4
Dependent Claim
14 words
The process of claim 2 wherein the pentane to bitumen ratio is about 1:1.
Claim 5
Dependent Claim
30 words
The process of claim 1 wherein the second fluid-bed drying zone is fluidized with an inert gas selected from the group consisting of nitrogen, carbon dioxide, steam or flue gas.
Claim 6
Dependent Claim
11 words
The process of claim 1 wherein the inert gas is nitrogen.
Claim 7
Dependent Claim
18 words
The process of claim 1 wherein the flow rate of solvent vapor is from 10 to 500 cm/sec.
Claim 8
Dependent Claim
17 words
The process of claim 1 wherein flow rate of inert gas is from 10 to 500 cm/sec.
Claim 9
Dependent Claim
13 words
The process of claim 1 wherein extract is recycled to the dissolution zone.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1985-08-30 | 1986-03-01 | 1986-08-31 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1989-08-30 | 1990-03-01 | 1990-08-31 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1993-08-30 | 1994-03-01 | 1994-08-31 | $7700.00 | Window Closed / Lapsed |