← Back to Patent Explorer
US4342844A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for preparing peroxide master batches

Assignee: Akzona Inc
•
Filing: 1980-12-04
•
Granted: 1982-08-03
•
Expires: 2000-12-04
📄 Original PDF 🌐 Google Patents 🔄 Sync Now

Abstract

Abstract A process for the preparation of an organic peroxide master batch comprising about 20-60% by weight of an organic peroxide and about 40-80% by weight of a polymer capable of being cross-linked by the peroxide, is disclosed. The process comprises contacting particles of such a polymer, having a diameter from about 200 microns to about 20 millimeters, at a temperature from about 15° C. to about 95° C., with a liquid medium which is not a physically stable emulsion and which comprises from about 2 to about 100 percent, by weight, of a peroxide which is a liquid at said temperature and from about 0 to about 98 percent, by weight, of a suitable liquid in which the peroxide and the polymer are insoluble, for a period of time sufficient to incorporate from about 20 to about 60 percent of peroxide in the polymer particles, based on the total weight of the polymer particles containing the peroxide, said medium being present in such an amount that after the incorporation of the peroxide essentially all of the polymer particles are completely surrounded by the liquid medium.

Inventors

  • 👤 Reinder Torenbeek
  • 👤 Jan D. van Drumpt
  • 👤 Gerrit F. Drost

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-25 20:54
CPC Classifications
C; C08; C08J; C08J3/00; C08J3/20; C08J3/203; C08J3/205; C08J3/22; C08J3/226

Claims Analysis

Total Claims: 5
Claim 1
Independent Claim 202 words
A process for the preparation of an organic peroxide master batch comprising from about 20 to about 60 percent by weight of an organic peroxide and from about 40 to about 80 percent by weight of a polymer capable of being cross-linked by the peroxide comprising (1) contacting particles of said polymer, having a diameter from about 200 microns to about 20 millimeters, at a temperature from about 15° C. to about 95° C., with a liquid medium which is not a physically stable emulsion and which comprises from about 2 to about 100 percent, by weight, of a peroxide which is a liquid at said temperature and from about 0 to about 98 percent, by weight, of a suitable liquid in which the peroxide and the polymer are insoluble, for a period of time sufficient to incorporate from about 20 to about 60 percent of peroxide in the polymer particles, based on the total weight of the polymer particles containing the peroxide, said medium being present in such an amount that after the incorporation of the peroxide essentially all of the polymer particles are completely surrounded by the liquid medium (2) and subsequently separating the liquid medium from the polymer particles.
Claim 2
Dependent Claim 202 words
A process for the preparation of an organic peroxide master batch comprising from about 20 to about 60 percent by weight of an organic peroxide and from about 40 to about 80 percent by weight of a polymer capable of being cross-linked by the peroxide comprising (1) contacting particles of said polymer, having a diameter from about 200 microns to about 20 millimeters, at a temperature from about 15° C. to about 95° C., with a liquid medium which is not a physically stable emulsion and which comprises from about 2 to about 100 percent, by weight, of a peroxide which is a liquid at said temperature and from about 0 to about 98 percent, by weight, of a suitable liquid in which the peroxide and the polymer are insoluble, for a period of time sufficient to incorporate from about 20 to about 60 percent of peroxide in the polymer particles, based on the total weight of the polymer particles containing the peroxide, said medium being present in such an amount that after the incorporation of the peroxide essentially all of the polymer particles are completely surrounded by the liquid medium (2) and subsequently separating the liquid medium from the polymer particles.
Claim 3
Dependent Claim 16 words
The process of claim 1 wherein the polymer particles are comprised of a copolymer of ethylene.
Claim 4
Dependent Claim 35 words
The process of claim 1 wherein the liquid medium comprises from about 5 to about 20 percent by weight of peroxide and from about 80 to about 95 percent by weight of the suitable liquid.
Claim 5
Dependent Claim 14 words
The process of claim 1, 2, or 3 wherein the suitable liquid is water.

References Cited (Backward Citations)

US3105057A Cited
US3242159A Cited
US3923947A Cited
US4006283A Cited
US4243773A Cited
US4278777A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1985-08-02 1986-02-01 1986-08-03 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1989-08-02 1990-02-01 1990-08-03 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1993-08-02 1994-02-01 1994-08-03 $7700.00 Window Closed / Lapsed

Assigned Categories & Tags

No categories assigned to this patent yet.

Assign Category Tag