Abstract A diamond-anvil, high-pressure cell having an apertured steel gasket interposed between the opposed diamonds is lowered into a liquified hydrogen bath at cryogenic temperatures. After the liquid hydrogen permeates the cell through the viewing apertures an initial sealing pressure is applied to the cell by a remotely operated threaded arrangement sufficient to prohibit escape of the liquified hydrogen from the aperture in the steel plate which is closed by the opposed diamonds. The cell is then typically removed from the liquified hydrogen bath and introduced into a lever type pressure applicator to further increase the pressure on the hydrogen at room temperature for the observation of its effects through suitable apertures in the cell and to convert the same to solid form.
An apparatus for filling a cell means defined by an apertured gasket and two opposed diamond anvils with hydrogen comprising cold chamber means, vessel means, means for supporting said vessel in said chamber means, means for supporting said cell means in said vessel with said diamond anvils spared from said gasket, means for supplying liquid hydrogen to said vessel whereby said cell would be filled with liquid hydrogen and remotely controlled means for moving said diamond anvils into engagement with said gasket about the aperture therein to trap an amount of liquid hydrogen in said cell means.
Claim 2
Independent Claim
97 words
An apparatus for filling a cell means defined by an apertured gasket and two opposed diamond anvils with hydrogen comprising cold chamber means, vessel means, means for supporting said vessel in said chamber means, means for supporting said cell means in said vessel with said diamond anvils spared from said gasket, means for supplying liquid hydrogen to said vessel whereby said cell would be filled with liquid hydrogen and remotely controlled means for moving said diamond anvils into engagement with said gasket about the aperture therein to trap an amount of liquid hydrogen in said cell means.