US4336272A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Process for the preparation of an oil-in-water emulsion
Assignee: Lever Brothers Co
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Filing: 1980-10-17
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Granted: 1982-06-22
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Expires: 2000-10-17
Abstract
Abstract Oil-in-water emulsions, which are microbiologically stable upon storage, consisting of oil, water, thickeners, emulsifiers, and optional further ingredients, are obtained by subjecting at least one of these components to an osmotic and/or acid shock and to a temperature shock by heating said component(s) within 3 minutes, preferably within 1 minute, to 40°-55° C., preferably to 45°-50° C., and processing the thus treated component(s) with the remaining ingredients into a final emulsion, during which the temperature of the final emulsion up to and including the filling and hermetically sealing of the containers into which it is being packed, is maintained at 40°-55° C. Preferably the temperature shock is achieved by adding during the preparation of the final emulsion a thickener suspension having a temperature of 70°-95° C. to the remaining components which have been subjected to an osmotic and/or acid shock.
Inventors
- 👤 Cornelis T. Verrips
- 👤 Renee van Rhee
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-05 19:17
CPC Classifications
A; A23; A23L; A23L27/00; A23L27/60
Claims Analysis
Total Claims: 15
Claim 1
Independent Claim
127 words
A process for the preparation of an edible, microbiologically stable oil-in-water emulsion from components comprising an oil, water, a thickener and an emulsifier, at least one of said components being microbiologically contaminated, comprising: (a) subjecting the microbiologically contaminated component to an osmotic shock and/or an acid shock; (b) subjecting said component from step (a) to a temperature shock by raising the temperature at least 20° C. to a value between 40° and 55° C. within three minutes; (c) processing the component from step (b) with the remaining ingredients into a final emulsion; (d) filling the final emulsion into containers; and (e) sealing the containers, the temperature of the emulsion during the processing, filling and sealing steps being maintained within the temperature range of 40° to 55° C.
Claim 2
Dependent Claim
127 words
A process for the preparation of an edible, microbiologically stable oil-in-water emulsion from components comprising an oil, water, a thickener and an emulsifier, at least one of said components being microbiologically contaminated, comprising: (a) subjecting the microbiologically contaminated component to an osmotic shock and/or an acid shock; (b) subjecting said component from step (a) to a temperature shock by raising the temperature at least 20° C. to a value between 40° and 55° C. within three minutes; (c) processing the component from step (b) with the remaining ingredients into a final emulsion; (d) filling the final emulsion into containers; and (e) sealing the containers, the temperature of the emulsion during the processing, filling and sealing steps being maintained within the temperature range of 40° to 55° C.
Claim 3
Dependent Claim
26 words
A process according to claim 1 wherein the temperature of the temperature shock, and the processing, filling and sealing steps is from 45° to 50° C.
Claim 4
Dependent Claim
28 words
A process according to claim 1 wherein the temperature of the microbiologically contaminated component is raised at least 20° C. to 40° to 55° C. within one minute.
Claim 5
Dependent Claim
21 words
A process according to claim 1 wherein the temperature shock is effected at most one minute after effecting the acid shock.
Claim 6
Dependent Claim
42 words
A process according to claims 1, 2, 3 or 4 wherein the temperature shock is achieved by adding a heated aqueous suspension of the thickener heated to 70°-95° C. to the component which has been subjected to the osmotic and/or acid shock.
Claim 7
Dependent Claim
11 words
A process according to claim 5 wherein the thickener is starch.
Claim 8
Dependent Claim
29 words
A process according to claims 1, 2, 3 or 4 wherein the component to be subjected to the osmotic and/or acid shock and the temperature shock comprises the emulsifier.
Claim 9
Dependent Claim
12 words
A process according to claim 7 wherein the emulsifier comprises egg yolk.
Claim 10
Dependent Claim
38 words
A process according to claim 8 wherein egg yolk is subjected to an osmotic shock by contacting said egg yolk with sodium chloride in an amount of 7 to 12% based on the weight of the egg yolk.
Claim 11
Dependent Claim
28 words
A process according to claims 1, 2, 3 or 4 wherein said components further comprise spices, flavoring substances, coloring agents, and particles of vegetables, meat, chicken and/or fish.
Claim 12
Dependent Claim
92 words
A process according to claim 10 wherein an amount of an acidic aqueous suspension comprising at least one of said thickeners, spices, flavoring substances, coloring agents, and particles of vegetables, meat, chicken and/or fish; and mixtures thereof, said amount being suitable for use in an edible oil-in-water emulsion and sufficient to achieve a pH in the final emulsion ranging from 3.0 to 5.0, and said acidic aqueous suspension having a temperature of from 70° C. to 95° C., is quickly added with vigorous stirring to a mixture containing an emulsifier and oil.
Claim 13
Dependent Claim
30 words
A process according to claim 11 wherein acetic acid is added in a proportion sufficient to achieve a concentration in the final emulsion ranging from 0.15 to 0.40% by weight.
Claim 14
Dependent Claim
17 words
A process according to claims 1, 2, 3 or 4 wherein the filled containers are sealed hermetically.
Claim 15
Dependent Claim
18 words
A process according to claims 1, 2, 3 or 4 wherein the final emulsion contains no chemical preservative.
References Cited (Backward Citations)
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1985-06-21 | 1985-12-21 | 1986-06-22 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1989-06-21 | 1989-12-21 | 1990-06-22 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1993-06-21 | 1993-12-21 | 1994-06-22 | $7700.00 | Window Closed / Lapsed |