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US4326901A Expired / Lapsed US ⏱️ 0.0 years remaining

Fragmentable charges of propelland powder coated with polyvinyl nitrate, and the process for their manufacture

Assignee: Societe Nationale des Poudres et Explosifs
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Filing: 1979-09-05
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Granted: 1982-04-27
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Expires: 1999-09-05
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Abstract

Abstract The present invention relates to a new type of fragmentable charge for weapons of small and medium caliber. The process for the manufacture of fragmentable charges of propellant powder containing nitrocellulose, according to the invention, is characterized in that, in a conventional process for the manufacture of propellant powder containing nitrocellulose, with solvent, a glazing operation is carried out, in which a glazing solution containing at least polyvinyl nitrate and a stabilizer is sprayed onto the grains of powder, and in that, after evaporation of the solvent from the said solution, the grains of powder thus obtained are compressed at between about 80 DEG and 120 DEG . The invention also relates to the fragmentable charges obtained by means of this process.

Inventors

  • 👤 Louis Leneveu
  • 👤 Didier Treneules

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-03 13:41
CPC Classifications
C; C06; C06B; C06B45/00; C06B45/04; C06B45/06; C06B45/10; C06B45/105; C06B45/18; C06B45/20; C06B45/28

Claims Analysis

Total Claims: 15
Claim 1
Independent Claim 101 words
Process for the manufacture of fragmentable charges from grains of propellant powder containing nitrocellulose comprising (1) malaxating nitrocellulose in a first solvent which has a gelatinizing action for nitrocellulose thus obtaining a paste, (2) extruding the paste to obtain strands, (3) chopping the strands to obtain grains, (4) drying the grains, (5) spraying the grains with a glazing solution containing at least polyvinyl nitrate, a second solvent, and a stabiliser to obtain grains coated with polyvinyl nitrate, (6) evaporating the second solvent and (7) compressing the resulting grains at a temperature of 80° to 120° C. to form said fragmentable charges.
Claim 2
Dependent Claim 101 words
Process for the manufacture of fragmentable charges from grains of propellant powder containing nitrocellulose comprising (1) malaxating nitrocellulose in a first solvent which has a gelatinizing action for nitrocellulose thus obtaining a paste, (2) extruding the paste to obtain strands, (3) chopping the strands to obtain grains, (4) drying the grains, (5) spraying the grains with a glazing solution containing at least polyvinyl nitrate, a second solvent, and a stabiliser to obtain grains coated with polyvinyl nitrate, (6) evaporating the second solvent and (7) compressing the resulting grains at a temperature of 80° to 120° C. to form said fragmentable charges.
Claim 3
Dependent Claim 13 words
Process according to claim 1, wherein the second solvent is a ketone/alcohol mixture.
Claim 4
Dependent Claim 13 words
Process according to claim 1, wherein the second solvent is an ester/alcohol mixture.
Claim 5
Dependent Claim 15 words
Process according to claim 2, wherein the said ketone/alcohol mixture is an acetone/ethyl alcohol mixture.
Claim 6
Dependent Claim 16 words
Process according to claim 3, wherein, the said ester/alcohol mixture is an ethyl acetate/ethyl alcohol mixture.
Claim 7
Dependent Claim 13 words
Process according to claim 1, wherein the said glazing solution contains a plasticiser.
Claim 8
Dependent Claim 12 words
Process according to claim 1, wherein the said glazing solution contains nitrocellulose.
Claim 9
Dependent Claim 28 words
Process according to claim 1, wherein the amount of polyvinyl nitrate in the glazing solution is between 2 and 10% by weight of the powder to be treated.
Claim 10
Dependent Claim 24 words
Process according to claim 8, wherein the amount of polyvinyl nitrate is between 3 and 5% by weight of the powder to be treated.
Claim 11
Dependent Claim 20 words
Process according to claim 1, wherein said compressing is carried out at a pressure of between 100 and 200 bars.
Claim 12
Dependent Claim 24 words
The process according to claim 1 wherein said spraying with a glazing solution is carried out at a temperature of 30° to 50° C.
Claim 13
Dependent Claim 19 words
The process according to claim 1 wherein said first solvent is a mixture of an ether and ethyl alcohol.
Claim 14
Dependent Claim 98 words
Fragmentable charges based on grains of propellant powder containing nitrocellulose, prepared by (1) malaxating nitrocellulose in a first solvent which has a gelatinizing action for nitrocellulose thus obtaining a paste, (2) extruding the paste to obtain strands, (3) chopping the strands to obtain grains, (4) drying the grains, (5) spraying the grains with a glazing solution containing at least polyvinyl nitrate, a second solvent and a stabilizer to obtain grains coated with polyvinyl nitrate, (6) evaporating the second solvent and (7) compressing the resulting grains at a temperature of 80° to 120° C. to form said fragmentable charges.
Claim 15
Dependent Claim 98 words
Fragmentable charges based on grains of propellant powder containing nitrocellulose, prepared by (1) malaxating nitrocellulose in a first solvent which has a gelatinizing action for nitrocellulose thus obtaining a paste, (2) extruding the paste to obtain strands, (3) chopping the strands to obtain grains, (4) drying the grains, (5) spraying the grains with a glazing solution containing at least polyvinyl nitrate, a second solvent and a stabilizer to obtain grains coated with polyvinyl nitrate, (6) evaporating the second solvent and (7) compressing the resulting grains at a temperature of 80° to 120° C. to form said fragmentable charges.

References Cited (Backward Citations)

US3711343A Cited
DE2361879A1 Cited
US4023996A Cited
US4202713A Cited
US4214927A Cited
EP0002968A1 Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1985-04-26 1985-10-26 1986-04-27 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1989-04-26 1989-10-26 1990-04-27 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1993-04-26 1993-10-26 1994-04-27 $7700.00 Window Closed / Lapsed

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