Apparatus for continuously separating purified volatile liquid from crude volatile liquid containing non-volatile constituents and dissolved incondensible gas, by the use of mechanical energy

Claim 1

Apparatus for continuously separating purified volatile liquid from crude volatile liquid containing non-volatile constituents and dissolved incondensible gas, by the use of mechanical energy, said apparatus comprising a container closed to free communication with the atmosphere, and adapted for maintenance therein of a body of crude volatile liquid having a predetermined substantially constant surface level with an evacuated space thereabove containing a low pressure mixture of evaporated volatile liquid vapor and incondensible gas; an array of heat-conducting tubes within said closed container located for immersion of their outer surfaces in said body of crude liquid with their upper ends entering into a plate above said predetermined surface level and their lower ends entering into a closed drum member within said container in the lower portion thereof; a manifold member in said evacuated space adapted to make sealing contact with said plate to form an outer portion of said evacuated space above said crude liquid surface level and an inner portion above said tubes; a fan blower located in an orifice in said manifold member and supported so that its input side is in said outer portion of said evacuated space and its output side in said inner portion, said fan blower being adapted for normal constant high speed of rotation to maintain a substantially constant pressure differential between the input and output sides thereof for continuously moving the low pressure vapor and gas mixture through the fan blower, thereby heating said mixture by compression and friction and then impelling the heated mixture into the upper ends of said tubes, whereby the vapor is condensed during passage downwardly through the tubes by heat exchange with said surrounding body of crude liquid to produce purified volatile liquid which emerges from the lower ends of the tubes together with incondensible gas into said closed drum member, and whereby the surrounding crude liquid is heated to cause further evaporation of the vapor and gas mixture from the crude liquid surface into said evacuated space; liquid transporting means for removing the resulting concentrated crude liquid containing non-volatile constituents from the lower portion of the closed container and conveying it at atmospheric pressure outside the container; and liquid transporting means for removing condensed pure volatile liquid from said closed drum member and conveying it at atmospheric pressure outside the container; the apparatus being protected from pertubations that would affect maintenance of said pressure differential, by including in the apparatus; gas transporting means for enabling the fan blower to continuously recirculate a substantially constant predetermined amount of incondensible gas from said drum member back through said heat exchange tubes, whereby increase in pressure at the output side of the fan blower due to gas accumulation is substantially eliminated; and means for returning the crude liquid surface to said predetermined level when it begins to be lowered due to removal from said body of crude liquid of volatile liquid in the form of evaporated vapor and as concentrate, whereby pressure fluctuations in the evaporated vapor and gas mixture at the input side of the fan blower due to heat exchange variations between the body of crude liquid and the compressed heated vapor and gas in the tube array are substantially eliminated.