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US4304566A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for the dyeing of wool with reactive dyestuffs

Assignee: Hoechst AG
•
Filing: 1979-11-01
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Granted: 1981-12-08
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Expires: 1999-11-01
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Abstract

Abstract A process for the dyeing of textiles consisting of wool without anti-felt finish or wool having an anti-felt finish in the form of a coating of a polyimine resin or a polyacrylic resin, or textiles containing such wool, with reactive dyes according to the exhaust method, which comprises dyeing said textiles in aqueous dyeing baths containing at least one commercial reactive dyestuff the starting pH of which is in the weakly acidic to neutral range, by heating rapidly to the dyeing temperature of 110 DEG to 125 DEG C. immediately after addition of the dissolved dyestuff, and by dyeing at this temperature for 10 to 20 minutes, while omitting the addition of pH-regulating substances during the whole dyeing operation.

Inventors

  • 👤 Hans-Ulrich von der Eltz
  • 👤 Armand Lehinant
  • 👤 Joachim W. Lehmann
  • 👤 Hans-Peter Maier

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-29 16:20
CPC Classifications
D; D06; D06P; D06P3/00; D06P3/02; D06P3/04; D06P3/14; D06P3/148; D06P3/82; D06P3/8204; D06P3/8214

Claims Analysis

Total Claims: 11
Claim 1
Independent Claim 158 words
In a process for the dyeing of a textile containing wool without anti-felting finish, or wool having an anti-felting finish in the form of a coating layer of a polyimine resin or a polyacrylic resin, with reactive dyes according to the batchwise exhaustion method, the improvement which comprises contacting the textile material with an aqueous dyeing liquor containing one or more reactive dyestuffs, the initial pH value of said dye liquor being in the weakly acidic to neutral range, heating said dye liquor, beginning immediately after addition of the dissolved reactive dyestuff, to a dyeing temperature in the range of from 110° to 125° C. within 5 to 10 minutes, and dyeing the textile material at this temperature for 10 to 20 minutes, without pretreatment of the textile with an amphoteric auxiliary and without the addition of a pH-regulating substance in the course of the effective contact of the textile material with the dye liquor during the process.
Claim 2
Dependent Claim 158 words
In a process for the dyeing of a textile containing wool without anti-felting finish, or wool having an anti-felting finish in the form of a coating layer of a polyimine resin or a polyacrylic resin, with reactive dyes according to the batchwise exhaustion method, the improvement which comprises contacting the textile material with an aqueous dyeing liquor containing one or more reactive dyestuffs, the initial pH value of said dye liquor being in the weakly acidic to neutral range, heating said dye liquor, beginning immediately after addition of the dissolved reactive dyestuff, to a dyeing temperature in the range of from 110° to 125° C. within 5 to 10 minutes, and dyeing the textile material at this temperature for 10 to 20 minutes, without pretreatment of the textile with an amphoteric auxiliary and without the addition of a pH-regulating substance in the course of the effective contact of the textile material with the dye liquor during the process.
Claim 3
Dependent Claim 40 words
A process as defined in claim 1, wherein the textile is wool or a blend thereof, and the dye liquor further contains from 1 to 5%, calculated on the weight of the dry textile material, of a wool protection agent.
Claim 4
Dependent Claim 17 words
A process as defined in claim 2, wherein the wool protection agent is an aqueous formaldehyde solution.
Claim 5
Dependent Claim 50 words
A process as defined in claim 1, 2 or 3, which further comprises dyeing a mixture of wool, or wool having an anti-felting finish, and polyester fibers in a two-step, single-bath operation, and adding one or more disperse dyes to the dye liquor after the reactive dyes have been exhausted.
Claim 6
Dependent Claim 47 words
A process as defined in claim 1, 2 or 3, which further comprises dyeing a mixture of wool, or wool having an anti-felting finish, and polyester fibers in a one-step, single-bath operation, the dye liquor additionally containing one or more disperse dyes, but not a pH-regulating substance.
Claim 7
Dependent Claim 48 words
A process as defined in claim 1, 2 or 3, which further comprises after-treating the dyed textiles, following the exhaust dyeing, for 5 to 15 minutes with an amount of an aqueous 25% ammonia solution equivalent to 1 to 2% of the weight of the dry textile material.
Claim 8
Dependent Claim 33 words
A process as defined in claim 6, wherein the after-treatment is carried out in the dyeing liquor itself after cooling same to a temperature in the range of from 70° to 80° C.
Claim 9
Dependent Claim 15 words
A process as defined in claim 6, which further comprises after-treating in a fresh bath.
Claim 10
Dependent Claim 29 words
A process as defined in claim 1, wherein the initial pH value of the aqueous dyeing liquor containing one or more reactive dyestuffs is of from 4 to 7.
Claim 11
Dependent Claim 17 words
A process as defined in claim 9, wherein said pH value is of from 6 to 7.

References Cited (Backward Citations)

US2869969A Cited
US3930795A Cited
US4063877A Cited
US4115457A Cited
US4219332A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1984-12-07 1985-06-08 1985-12-08 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1988-12-07 1989-06-08 1989-12-08 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1992-12-07 1993-06-08 1993-12-08 $7700.00 Window Closed / Lapsed

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