← Back to Patent Explorer
US4302272A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for heat sealing polyurethane foam

Assignee: Bayer Corp
•
Filing: 1980-01-14
•
Granted: 1981-11-24
•
Expires: 2000-01-14
📄 Original PDF 🌐 Google Patents 🔄 Sync Now

Abstract

Abstract The instant invention is directed to a process for heat sealing flexible polyurethane foam, comprising: A. reacting and foaming a polyurethane foam produced by the steps comprising reacting: (I) an organic polyisocyanate; (II) a polyol having a molecular weight of 2,000 to 8,000 comprising the adduct obtained by sequentially reacting: (a) a polyhydroxyl initiator, with a functionality of 2 to 5 and a weight average molecular weight as determined by gel permeation chromatography of from 62 to 200; with (b) 10 to 90%, most preferably 10 to 50%, by weight, based on the total oxide present in (b)+(c)+(d), a first alkylene oxide; and subsequently reacting the product with (c) 10 to 80%, preferably 20 to 50% by weight, based on the total oxide present in (b)+(c)+(d), 4,4,4-trichloro-1,2-epoxybutane and/or epihalohydrin; and subsequently reacting the product with (d) 10 to 60%, most preferably 10 to 40%, by weight, based on the total oxide present in (b)+(c)+(d), a second alkylene oxide. (III) foaming agent; and optionally (IV) catalyst; B. heating a portion of the surface of said flexible polyurethane foam of (A) above its melting or fusion point; and C. cooling said flexible polyurethane foam below its melting or fusion point.

Inventors

  • 👤 Barry A. Phillips
  • 👤 Keith G. Spitler
  • 👤 Richard E. Keegan

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-05 21:09
CPC Classifications
C; C08; C08G; C08G18/00; C08G18/06; C08G18/28; C08G18/40; C08G18/48; C08G18/50; C08G18/5003; C08G18/5006; C08G18/5009; B; B32; B32B; B32B5/00; B32B5/18; B29; B29C; B29C44/00; B29C44/34; B29C44/56; C08J; C08J5/00; C08J5/12; C08J5/121; B32B2266/00; B32B2266/02; B32B2266/0214; B32B2266/0278; C08J2375/00; C08J2375/04; Y; Y10; Y10S; Y10S521/00; Y10S521/904; Y10S521/914; Y10T; Y10T428/00; Y10T428/249921; Y10T428/249953

Claims Analysis

Total Claims: 20
Claim 1
Independent Claim 218 words
A process for heat sealing flexible polyurethane foam to a substrate comprising: A. reacting and foaming a flexible polyurethane foam produced by the steps comprising reacting: (I) an organic polyisocyanate; (II) a polyol having a molecular weight of 2,000 to 8,000 comprising the adduct obtained by sequentially reacting: (a) a polyhydroxyl initiator, with a functionality of 2 to 5 and a weight average molecular weight as determined by gel permeation chromatography of from 50 to 200; with (b) 10 to 90%, by weight based on the total oxide present in (b)+(c)+(d), a first alkylene oxide; and subsequently reacting the product with (c) 10 to 80%, by weight, based on the total oxide present in (b)+(c)+(d), 4,4,4-trichloro-1,2-epoxybutane and/or epihalohydrin; and subsequently reacting the product with (d) 10 to 60%, by weight, based on the total oxide present in (b)+(c)+(d), a second alkylene oxide; (III) foaming agent; and optionally (IV) catalyst; B. allowing said resulting polyurethane foam to cure; C. heating a portion of the surface of said flexible polyurethane foam of (B) above its melting or fusion point; and D. contacting the melted or fused surface of said polyurethane flexible foam with a substrate whereby a flexible polyurethane foam/substrate laminate is formed; and E. cooling said flexible polyurethane foam/substrate laminate below the melting or fusion point of said foam.
Claim 2
Dependent Claim 218 words
A process for heat sealing flexible polyurethane foam to a substrate comprising: A. reacting and foaming a flexible polyurethane foam produced by the steps comprising reacting: (I) an organic polyisocyanate; (II) a polyol having a molecular weight of 2,000 to 8,000 comprising the adduct obtained by sequentially reacting: (a) a polyhydroxyl initiator, with a functionality of 2 to 5 and a weight average molecular weight as determined by gel permeation chromatography of from 50 to 200; with (b) 10 to 90%, by weight based on the total oxide present in (b)+(c)+(d), a first alkylene oxide; and subsequently reacting the product with (c) 10 to 80%, by weight, based on the total oxide present in (b)+(c)+(d), 4,4,4-trichloro-1,2-epoxybutane and/or epihalohydrin; and subsequently reacting the product with (d) 10 to 60%, by weight, based on the total oxide present in (b)+(c)+(d), a second alkylene oxide; (III) foaming agent; and optionally (IV) catalyst; B. allowing said resulting polyurethane foam to cure; C. heating a portion of the surface of said flexible polyurethane foam of (B) above its melting or fusion point; and D. contacting the melted or fused surface of said polyurethane flexible foam with a substrate whereby a flexible polyurethane foam/substrate laminate is formed; and E. cooling said flexible polyurethane foam/substrate laminate below the melting or fusion point of said foam.
Claim 3
Dependent Claim 19 words
The process of claim 1 wherein said alkylene oxide of (b) and (d) is ethylene oxide and/or propylene oxide.
Claim 4
Dependent Claim 15 words
The process of claim 1, wherein said polyhydroxyl initiator (a) has a functionality of 3.
Claim 5
Dependent Claim 12 words
The process of claim 3, wherein said polyhydroxyl initiator (a) is glycerol.
Claim 6
Dependent Claim 13 words
The process of claim 1, wherein said organic polyisocyanate (I) is toluene diisocyanate.
Claim 7
Dependent Claim 10 words
The process of claim 1, wherein component (c) is 4,4,4-trichloro-1,2-epoxybutane.
Claim 8
Dependent Claim 10 words
The process of claim 1, wherein component (c) is epihalohydrin.
Claim 9
Dependent Claim 16 words
The process of claim 1, wherein said polyol has a molecular weight of 5,500 to 7,000.
Claim 10
Dependent Claim 23 words
The process of claim 1, wherein component (b) is 10 to 50%; (c) is 20 to 50%; and (d) is 10 to 40%.
Claim 11
Dependent Claim 186 words
A process for melting or fusing portions of flexible polyurethane foam, comprising: A. preparing a polyurethane foam by the steps comprising reacting: (I) an organic polyisocyanate; (II) a polyol having a molecular weight of 2,000 to 8,000 comprising the adduct obtained by sequentially reacting: (a) a polyhydroxyl initiator, with a functionality of 2 to 5 and a weight average molecular weight as determined by gel permeation chromatography of from 62 to 200; with (b) 10 to 90%, by weight, based on the total oxide present in (b)+(c)+(d), a first alkylene oxide; and subsequently reacting the product with (c) 10 to 80%, by weight, based on the total oxide present in (b)+(c)+(d), 4,4,4-trichloro-1,2-epoxybutane and/or epihalohydrin; and subsequently reacting the product with (d) 10 to 60%, by weight, based on the total oxide present in (b)+(c)+(d), a second alkylene oxide; (III) foaming agent; and optionally (IV) catalyst; B. allowing said resulting polyurethane foam to cure; C. heating a portion of the surface of said flexible polyurethane foam of (B) above its melting or fusion point; and D. cooling said flexible polyurethane foam below its melting or fusion point.
Claim 12
Dependent Claim 186 words
A process for melting or fusing portions of flexible polyurethane foam, comprising: A. preparing a polyurethane foam by the steps comprising reacting: (I) an organic polyisocyanate; (II) a polyol having a molecular weight of 2,000 to 8,000 comprising the adduct obtained by sequentially reacting: (a) a polyhydroxyl initiator, with a functionality of 2 to 5 and a weight average molecular weight as determined by gel permeation chromatography of from 62 to 200; with (b) 10 to 90%, by weight, based on the total oxide present in (b)+(c)+(d), a first alkylene oxide; and subsequently reacting the product with (c) 10 to 80%, by weight, based on the total oxide present in (b)+(c)+(d), 4,4,4-trichloro-1,2-epoxybutane and/or epihalohydrin; and subsequently reacting the product with (d) 10 to 60%, by weight, based on the total oxide present in (b)+(c)+(d), a second alkylene oxide; (III) foaming agent; and optionally (IV) catalyst; B. allowing said resulting polyurethane foam to cure; C. heating a portion of the surface of said flexible polyurethane foam of (B) above its melting or fusion point; and D. cooling said flexible polyurethane foam below its melting or fusion point.
Claim 13
Dependent Claim 19 words
The process of claim 10 wherein said alkylene oxide of (b) and (d) is ethylene oxide and/or propylene oxide.
Claim 14
Dependent Claim 15 words
The process of claim 10, wherein said polyhydroxyl initiator (a) has a functionality of 3.
Claim 15
Dependent Claim 12 words
The process of claim 12, wherein said polyhydroxyl initiator (a) is glycerol.
Claim 16
Dependent Claim 13 words
The process of claim 10, wherein said organic polyisocyanate (I) is toluene diisocyanate.
Claim 17
Dependent Claim 10 words
The process of claim 10, wherein component (c) is 4,4,4-trichloro-1,2-epoxybutane.
Claim 18
Dependent Claim 10 words
The process of claim 10, wherein component (c) is epihalohydrin.
Claim 19
Dependent Claim 16 words
The process of claim 10, wherein said polyol has a molecular weight of 5,500 to 7.000.
Claim 20
Dependent Claim 23 words
The process of claim 10, wherein component (b) is 10 to 50%; (c) is 20 to 50%; and (d) is 10 to 40%.

References Cited (Backward Citations)

US3238273A Cited
US3244754A Cited
US3255126A Cited
US3400196A Cited
US3497416A Cited
US3530030A Cited
JPS487999U Cited
US3801518A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1984-11-23 1985-05-25 1985-11-24 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1988-11-23 1989-05-25 1989-11-24 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1992-11-23 1993-05-25 1993-11-24 $7700.00 Window Closed / Lapsed

Assigned Categories & Tags

No categories assigned to this patent yet.

Assign Category Tag