US4300044A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Method and apparatus for the analysis of chemical compounds in aqueous solution by mass spectroscopy of evaporating ions
Assignee: Canada Minister of Environment
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Filing: 1980-05-07
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Granted: 1981-11-10
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Expires: 2000-05-07
Abstract
Abstract A method for analysis of chemical compounds comprising forming a fine droplet spray of a solution containing the compound to be detected and analyzed, electrically charging the spray droplets and allowing said spray to evaporate such that either ionized molecules or atoms of the compound of interest or the neutral species attached to another ion are ejected into the air introducing the ions which may or may not be clustered with neutral solvent molecules into an analyzer, and obtaining a read-out indicative of the chemical compound is obtained.
Inventors
- 👤 Julio V. Iribarne
- 👤 Bruce A. Thomson
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-25 04:02
CPC Classifications
H; H01; H01J; H01J49/00; H01J49/02; H01J49/10; H01J49/16; H01J49/165
Claims Analysis
Total Claims: 6
Claim 1
Independent Claim
97 words
A method for analysis of chemical compounds comprising forming at or near normal room temperature a fine droplet spray of a solution containing the compound to be detected and analyzed, electrically charging the spray droplets and allowing said spray to evaporate such that either ionized molecules or atoms of the compound of interest or the neutral species attached to another ion are ejected into the air, introducing the ions which may or may not be clustered with neutral solvent molecules into a mass spectrometer, and obtaining mass spectrum a read-out indicative of the chemical compound is obtained.
Claim 2
Independent Claim
97 words
A method for analysis of chemical compounds comprising forming at or near normal room temperature a fine droplet spray of a solution containing the compound to be detected and analyzed, electrically charging the spray droplets and allowing said spray to evaporate such that either ionized molecules or atoms of the compound of interest or the neutral species attached to another ion are ejected into the air, introducing the ions which may or may not be clustered with neutral solvent molecules into a mass spectrometer, and obtaining mass spectrum a read-out indicative of the chemical compound is obtained.
Claim 3
Dependent Claim
25 words
A method for analysis as in claim 1 where the solution containing the compound is sprayed into a gas at or close to atmospheric pressure.
Claim 4
Dependent Claim
27 words
A method for analysis of chemical compounds as in claim 1 wherein the chemical compound to be tested is brought into the form of an aqueous solution.
Claim 5
Dependent Claim
29 words
A method for analysis of chemical compounds as in claim 1 wherein the spray droplets are charged by induction of means of an induction electrode at high electrical potential.
Claim 6
Dependent Claim
32 words
A method for analysis of chemical compounds as in claim 1 wherein the ionized molecules or atoms are introduced into the mass spectrometer through a region or curtain of purified dry gas.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1984-11-09 | 1985-05-11 | 1985-11-10 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1988-11-09 | 1989-05-11 | 1989-11-10 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1992-11-09 | 1993-05-11 | 1993-11-10 | $7700.00 | Window Closed / Lapsed |