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US4294124A Expired / Lapsed US ⏱️ 0.0 years remaining

Apparatus for extraction of materials from operating pressurized vessels

Assignee: Air Products and Chemicals Inc
•
Filing: 1980-04-10
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Granted: 1981-10-13
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Expires: 2000-04-10
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Abstract

Abstract Apparatus is disclosed for withdrawing and collecting samples from a pressure vessel without disturbing either the reaction pressure contained within the vessel or the physical conditions of the sample which is extracted. A tubular probe having a perforated end is contained in a sealable second tube capable of attachment to an operating reaction pressure vessel. The probe is capable of sliding into the pressure vessel and withdrawing a sample of material from the pressure vessel without disturbing the reaction contained therein. The probe is capable of withdrawing the sample material and collecting it in the sealable second tube, which can be removed and carried away to analyze the samples.

Inventors

  • 👤 George V. Kalwaitis

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-25 13:45
CPC Classifications
G; G01; G01N; G01N1/00; G01N1/02; G01N1/10

Claims Analysis

Total Claims: 9
Claim 1
Independent Claim 134 words
A sampling apparatus for withdrawing and collecting samples from an operating pressure vessel without disturbing a reaction in said pressure vessel and while maintaining physical conditions of said sample, which apparatus comprises: (a) a pressure vessel having an aperture; (b) a first valve attached to said vessel and aligned with said aperture; (c) a first tube having a sealed end and an open end; (d) a second valve attached to said open end of said first tube and removably attached to said first valve; (e) a second tube coaxially oriented within said first tube, said second tube having a perforated end for receiving a sample from said vessel; and (f) means for sliding said perforated end of said second tube in and out of said second valve, said first valve, and said pressure vessel.
Claim 2
Dependent Claim 134 words
A sampling apparatus for withdrawing and collecting samples from an operating pressure vessel without disturbing a reaction in said pressure vessel and while maintaining physical conditions of said sample, which apparatus comprises: (a) a pressure vessel having an aperture; (b) a first valve attached to said vessel and aligned with said aperture; (c) a first tube having a sealed end and an open end; (d) a second valve attached to said open end of said first tube and removably attached to said first valve; (e) a second tube coaxially oriented within said first tube, said second tube having a perforated end for receiving a sample from said vessel; and (f) means for sliding said perforated end of said second tube in and out of said second valve, said first valve, and said pressure vessel.
Claim 3
Dependent Claim 64 words
A sampling apparatus according to claim 1, wherein said means for sliding comprises a crank, a threaded rod attached at one end to said crank and extending into said first tube to contact threads in the end of said second tube, wherein said rod has the capability when rotated of urging said perforated end of said second tube in and out of said vessel.
Claim 4
Dependent Claim 36 words
A sampling apparatus according to claim 2, wherein said sliding means further comprises a longitudinal trough in said second tube and a guiding key protruding from the wall of said first tube into said longitudinal trough.
Claim 5
Dependent Claim 36 words
A sampling apparatus according to claim 2, wherein said sliding means further comprises a longitudinal trough in said first tube and a guiding key protruding from the wall of said first tube into said longitudinal trough.
Claim 6
Dependent Claim 24 words
A sampling apparatus according to claim 3, wherein said key can be located at a plurality of predetermined longitudinal distances along said first tube.
Claim 7
Dependent Claim 14 words
A sampling apparatus according to claim 5 having an external layer of thermal insulation.
Claim 8
Dependent Claim 34 words
A sampling apparatus according to claim 6, wherein said pressure vessel is capable of containing reaction mixtures at a pressure of at least 100-300 psi and at a temperature of at least 800° F.
Claim 9
Dependent Claim 24 words
A sampling apparatus according to claim 6, wherein said pressure vessel is capable of containing reaction mixtures at pressures in the range 0.0001-100 psi.

References Cited (Backward Citations)

US2119288A Cited
US3115782A Cited
US3276264A Cited
US4054060A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1984-10-12 1985-04-13 1985-10-13 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1988-10-12 1989-04-13 1989-10-13 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1992-10-12 1993-04-13 1993-10-13 $7700.00 Window Closed / Lapsed

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