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US4293570A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for the preparation of sweetener containing product

Assignee: Chimicasa GmbH
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Filing: 1979-04-02
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Granted: 1981-10-06
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Expires: 1999-04-02
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Abstract

Abstract An apparatus and process for the preparation of cryptocrystalline sweeteners, such as sorbitol, by the spraying of a heated, aqueous, low-viscosity, high-solids, sweetener solution, employing a cool, compressed, inert gas, through a nozzle into a fine spray and into a cooler atmosphere, to form very fine particles of the sprayed sweetener product.

Inventors

  • 👤 Kalman Vadasz

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-24 08:00
CPC Classifications
A; A23; A23G; A23G1/00; A23G1/30; A23G1/32; A23G1/40; A23G1/04; A23G1/042; A23G1/56; A23G3/00; A23G3/02; A23G3/0205; A23G3/0231; A23G3/34; A23G3/346; A23G3/36; A23G3/42; A23G4/00; A23G4/02; A23G4/06; A23G4/10; A23G2200/00; A23G2200/06

Claims Analysis

Total Claims: 7
Claim 1
Independent Claim 212 words
A process of preparing a cryptocrystalline sweetener containing product, which process comprises: spraying in a fine liquid spray within a vessel and into the cooler atmosphere within the vessel, through heated spray nozzles, a heated, aqueous, low-viscosity, high-solids, sweetener solution selected from the group consisting of an aqueous solution of sorbitol, sucrose fructose, mannitol, glucose, and combinations thereof, having a temperature of from about 180° F. to 315° F., and containing about 70% to 99.5% by weight of sweetener, and employing in the spraying operation cool, compressed, dry, air, which cool, compressed air is introduced into the heated spray nozzles, and wherein the heated solution is maintained in a heated condition up to the point of spraying, and wherein the compressed air has a temperature of from about 40° F. to 120° F. and is employed at a pressure of from about 40 to 125 psi, and wherein the change in phase from a liquid to a solid of the sweetener solution occurs without the substantial loss of moisture during the spraying operation, to provide for the formation in the atmosphere within the vessel of a fine particle-size, cryptocrystalline, sweetener product having a particle size of less than about 5 microns, and admixing the fine-particle-size product with a food or confectionary product.
Claim 2
Dependent Claim 212 words
A process of preparing a cryptocrystalline sweetener containing product, which process comprises: spraying in a fine liquid spray within a vessel and into the cooler atmosphere within the vessel, through heated spray nozzles, a heated, aqueous, low-viscosity, high-solids, sweetener solution selected from the group consisting of an aqueous solution of sorbitol, sucrose fructose, mannitol, glucose, and combinations thereof, having a temperature of from about 180° F. to 315° F., and containing about 70% to 99.5% by weight of sweetener, and employing in the spraying operation cool, compressed, dry, air, which cool, compressed air is introduced into the heated spray nozzles, and wherein the heated solution is maintained in a heated condition up to the point of spraying, and wherein the compressed air has a temperature of from about 40° F. to 120° F. and is employed at a pressure of from about 40 to 125 psi, and wherein the change in phase from a liquid to a solid of the sweetener solution occurs without the substantial loss of moisture during the spraying operation, to provide for the formation in the atmosphere within the vessel of a fine particle-size, cryptocrystalline, sweetener product having a particle size of less than about 5 microns, and admixing the fine-particle-size product with a food or confectionary product.
Claim 3
Dependent Claim 43 words
The process of claim 1 wherein the spraying occurs within a paddle-type mixer, which mixer contains an agitated confectionery product, and wherein the cryptocrystalline sweetener product so formed is directly incorporated into the agitated confectionery product, while being agitated by the paddle-type mixer.
Claim 4
Dependent Claim 27 words
The process of claim 1 which includes spraying the heated mixture within a vessel containing an air-exhaust means for the continuous removal of air from the container.
Claim 5
Dependent Claim 18 words
The process of claim 1 wherein the heated solution comprises from about 95% or more of the sweetener.
Claim 6
Dependent Claim 34 words
The process of claim 1 which includes spraying the heated sweetener solution directly toward an agitated mass of a confectionery product, the solid cryptocrystalline sweetener product so formed directly incorporated into the confectionery product.
Claim 7
Dependent Claim 48 words
The process of claim 1 wherein the spraying occurs within a rotating-pan apparatus, which pan contains a confectionery product on the rotating surface of the pan, and wherein the cryptocrystalline sweetener product so formed is directly incorporated into the agitated product on the surface within the rotating pan.

References Cited (Backward Citations)

US1724627A Cited
US2594863A Cited
US2726959A Cited
US3557717A Cited
US4079151A Cited
US3973041A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1984-10-05 1985-04-06 1985-10-06 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1988-10-05 1989-04-06 1989-10-06 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1992-10-05 1993-04-06 1993-10-06 $7700.00 Window Closed / Lapsed

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