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US4284418A Expired / Lapsed US ⏱️ 0.0 years remaining

Particle separation method and apparatus

Assignee: Research Corp
•
Filing: 1979-06-28
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Granted: 1981-08-18
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Expires: 1999-06-28
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Abstract

Abstract A method and apparatus for separating molecules or particles of different mass comprises combining the molecules or particles in a carrier gas of lighter molecular weight, accelerating the composite mixture in a supersonic free jet, decelerating the free jet through a light background gas at a controlled pressure, directing the decelerating jet onto a membrane wherein the constituents of the composite mixture are segregated, withdrawing a stream enriched in the high mass species which preferentially pass through the membrane, and withdrawing a stream enriched in the low mass species which are preferentially blocked by the membrane.

Inventors

  • 👤 Ronald P. Andres

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-05 14:41
CPC Classifications
B; B01; B01D; B01D53/00

Claims Analysis

Total Claims: 46
Claim 1
Independent Claim 93 words
A process for separating a gas or aerosol mixture into its constituents of different mass comprising the steps of: (a) accelerating the mixture in a carrier gas to a high velocity gas flow, (b) differentially decelerating the constituents of the flow through a background gas at a controlled pressure, (c) directing the decelerating flow onto a membrane, (d) withdrawing an output enriched in a high particle mass species which preferentially passes through the membrane, and (e) withdrawing another output enriched in a low particle mass species which is preferentially blocked by the membrane.
Claim 2
Dependent Claim 93 words
A process for separating a gas or aerosol mixture into its constituents of different mass comprising the steps of: (a) accelerating the mixture in a carrier gas to a high velocity gas flow, (b) differentially decelerating the constituents of the flow through a background gas at a controlled pressure, (c) directing the decelerating flow onto a membrane, (d) withdrawing an output enriched in a high particle mass species which preferentially passes through the membrane, and (e) withdrawing another output enriched in a low particle mass species which is preferentially blocked by the membrane.
Claim 3
Dependent Claim 22 words
The process of claim 1 further comprising the step of minimizing velocity slip between particle mass species during acceleration of the mixture.
Claim 4
Dependent Claim 31 words
The process of claim 1 further comprising the step of locating the membrane across the flow at a position corresponding to a mean deceleration distance of the low particle mass species.
Claim 5
Dependent Claim 57 words
The process of claim 1 wherein step (c) further includes directing the flow onto at least a second membrane downstream of the one membrane, and further comprising the step of withdrawing at least a third output enriched in an intermediate particle mass species which is preferentially passed by the first membrane but blocked by the second membrane.
Claim 6
Dependent Claim 20 words
The process of claim 1 wherein step (e) includes condensing the species blocked by the membrane on cryogenic collecting surfaces.
Claim 7
Dependent Claim 22 words
The process of claim 1 which comprises the step of raising the temperature of said cryogenic surfaces to recover the adsorbed molecules.
Claim 8
Dependent Claim 52 words
A particle separator comprising means for introducing a gas flow containing heavier and lighter species of particles, means for maintaining a background gas in a region of the gas flow for differentially decelerating the particle species, and means including a membrane downstream of said region for separating heavier from lighter particle species.
Claim 9
Dependent Claim 52 words
A particle separator comprising means for introducing a gas flow containing heavier and lighter species of particles, means for maintaining a background gas in a region of the gas flow for differentially decelerating the particle species, and means including a membrane downstream of said region for separating heavier from lighter particle species.
Claim 10
Dependent Claim 36 words
A particle separator comprising means for producing a velocity disequilibrium between heavier and lighter particle species in a gas flow, and means including a membrane across the gas flow for separating heavier from lighter particle species.
Claim 11
Dependent Claim 36 words
A particle separator comprising means for producing a velocity disequilibrium between heavier and lighter particle species in a gas flow, and means including a membrane across the gas flow for separating heavier from lighter particle species.
Claim 12
Dependent Claim 20 words
The particle separator of claims 7 or 8 wherein said membrane passes heavier species and blocks lighter species of particles.
Claim 13
Dependent Claim 55 words
A particle separator comprising means for introducing a gas flow containing different particle species, means for maintaining a background gas in a region of the gas flow for differentially decelerating the particle species, and means including a membrane downstream of said region for separating particles having a higher velocity from particles having a lower velocity.
Claim 14
Dependent Claim 55 words
A particle separator comprising means for introducing a gas flow containing different particle species, means for maintaining a background gas in a region of the gas flow for differentially decelerating the particle species, and means including a membrane downstream of said region for separating particles having a higher velocity from particles having a lower velocity.
Claim 15
Dependent Claim 39 words
A particle separator comprising means for producing velocity disequilibrium between different particle species in a gas flow, and means including a membrane across the gas flow for separating particles of a higher velocity from particles of a lower velocity.
Claim 16
Dependent Claim 39 words
A particle separator comprising means for producing velocity disequilibrium between different particle species in a gas flow, and means including a membrane across the gas flow for separating particles of a higher velocity from particles of a lower velocity.
Claim 17
Dependent Claim 22 words
The particle separator of claims 10 or 11 wherein said membrane passes particles of higher velocity and blocks particles of lower velocity.
Claim 18
Dependent Claim 54 words
The particle separator of claims 8 or 11 wherein said means for producing velocity disequilibrium between particle species includes means for introducing a gas flow of the particle species in a carrier gas, and means for maintaining a background gas in a region of the gas flow for differentially decelerating the different particle species.
Claim 19
Dependent Claim 17 words
The particle separator of claims 7, 8, 10 or 11 comprising a plurality of membranes in series.
Claim 20
Dependent Claim 72 words
A particle separator comprising a chamber, means for introducing into the chamber a flow of different particle species in a carrier gas, means for maintaining a background gas in a deceleration region of the chamber for differentially decelerating the different particle species in the flow, and a membrane downstream of the deceleration region for passing particles of higher velocity into an output region of the chamber and blocking particles of lower velocity.
Claim 21
Dependent Claim 72 words
A particle separator comprising a chamber, means for introducing into the chamber a flow of different particle species in a carrier gas, means for maintaining a background gas in a deceleration region of the chamber for differentially decelerating the different particle species in the flow, and a membrane downstream of the deceleration region for passing particles of higher velocity into an output region of the chamber and blocking particles of lower velocity.
Claim 22
Dependent Claim 27 words
The particle separator of claim 15 wherein the membrane is positioned at a location corresponding to a mean deceleration distance of a more rapidly decelerated particle species.
Claim 23
Dependent Claim 17 words
The particle separator of claim 15 wherein the membrane is a closely packed array of capillary tubes.
Claim 24
Dependent Claim 14 words
The particle separator of claim 15 wherein the membrane is an open honeycomb mesh.
Claim 25
Dependent Claim 18 words
The particle separator of claim 15 wherein the membrane is adapted to adsorb particles which collide with it.
Claim 26
Dependent Claim 21 words
The particle separator of claim 15 further comprising means for withdrawing the blocked particles from the deceleration region of the chamber.
Claim 27
Dependent Claim 24 words
The particle separator of claim 20 further comprising a cryogenic collecting surface in the deceleration region of the chamber for collecting the blocked particles.
Claim 28
Dependent Claim 26 words
The particle separator of claim 15 further comprising a cryogenic collecting surface in the output region of the chamber for collecting particles passing through the membrane.
Claim 29
Dependent Claim 22 words
A particle separator as described in claim 15 comprising a plurality of membranes in series for separating particles of an intermediate size.
Claim 30
Dependent Claim 164 words
A particle separator comprising a chamber having an input end and an output end, an orifice at the input end for introducing a gas flow into the chamber, means for forming a gas mixture of heavier and lighter species of particles to be separated and a carrier gas, means for expanding the mixture through the orifice into the chamber in a high velocity flow, means for maintaining a background gas in a deceleration region of the chamber downstream of the orifice for differentially decelerating the heavier and lighter particle species, a membrane at a location downstream of the deceleration region corresponding to a mean deceleration distance of the lighter particle species for passing a substantial flux of the heavier particle species to the output end of the chamber and for blocking a substantial flux of the lighter particle species, and means for withdrawing a first output enriched in particles of the heavier species and a second output enriched in particles of the lighter species.
Claim 31
Dependent Claim 164 words
A particle separator comprising a chamber having an input end and an output end, an orifice at the input end for introducing a gas flow into the chamber, means for forming a gas mixture of heavier and lighter species of particles to be separated and a carrier gas, means for expanding the mixture through the orifice into the chamber in a high velocity flow, means for maintaining a background gas in a deceleration region of the chamber downstream of the orifice for differentially decelerating the heavier and lighter particle species, a membrane at a location downstream of the deceleration region corresponding to a mean deceleration distance of the lighter particle species for passing a substantial flux of the heavier particle species to the output end of the chamber and for blocking a substantial flux of the lighter particle species, and means for withdrawing a first output enriched in particles of the heavier species and a second output enriched in particles of the lighter species.
Claim 32
Dependent Claim 61 words
The particle separator of claim 24 adapted to separate at least another particle species of weight intermediate the heavier and lighter species, further comprising at least another membrane downstream of the one membrane at a location corresponding to a mean deceleration distance of the intermediate particle species, and means for withdrawing a third output enriched in particles of the intermediate species.
Claim 33
Dependent Claim 22 words
The particle separator of claim 25 wherein said one membrane has cryogenic surfaces for absorbing particles which collide with said one membrane.
Claim 34
Dependent Claim 16 words
The particle separator of claim 24 further comprising a cryogenic collecting surface in the deceleration region.
Claim 35
Dependent Claim 18 words
The particle separator of claim 27 further comprising an external refrigeration source for cooling said cryogenic collecting surface.
Claim 36
Dependent Claim 19 words
The particle separator of claim 24 wherein the membrane has cryogenic surfaces for adsorbing particles which collide with it.
Claim 37
Dependent Claim 23 words
The particle separator of claim 29 further comprising an external refrigeration source in communication with said cryogenic surface for cooling said cryogenic surfaces.
Claim 38
Dependent Claim 116 words
A particle separator comprising a chamber, means for introducing into the chamber a flow of different particle species in a carrier gas, means for maintaining a background gas in a deceleration region of the chamber for differentially decelerating the different particle species in the flow, a membrane downstream of the deceleration region for passing particles of higher velocity into an output region of the chamber and blocking particles of lower velocity, means for withdrawing the blocked particles from the deceleration region of the chamber, means for maintaining a gas stream flowing parallel to a side of the membrane facing the deceleration region and means for withdrawing an output of the gas stream enriched with blocked particles.
Claim 39
Dependent Claim 116 words
A particle separator comprising a chamber, means for introducing into the chamber a flow of different particle species in a carrier gas, means for maintaining a background gas in a deceleration region of the chamber for differentially decelerating the different particle species in the flow, a membrane downstream of the deceleration region for passing particles of higher velocity into an output region of the chamber and blocking particles of lower velocity, means for withdrawing the blocked particles from the deceleration region of the chamber, means for maintaining a gas stream flowing parallel to a side of the membrane facing the deceleration region and means for withdrawing an output of the gas stream enriched with blocked particles.
Claim 40
Dependent Claim 103 words
A particle separator comprising a chamber, means for introducing into the chamber a flow of different particle species in a carrier gas, means for maintaining a background gas in a deceleration region of the chamber for differentially decelerating the different particle species in the flow, a membrane downstream of the deceleration region for passing particles of higher velocity into an output region of the chamber and blocking particles of lower velocity, means for introducing a gas stream flowing parallel to a side of the membrane facing the output region, and means for withdrawing the gas stream enriched with particles passing through the membrane.
Claim 41
Dependent Claim 103 words
A particle separator comprising a chamber, means for introducing into the chamber a flow of different particle species in a carrier gas, means for maintaining a background gas in a deceleration region of the chamber for differentially decelerating the different particle species in the flow, a membrane downstream of the deceleration region for passing particles of higher velocity into an output region of the chamber and blocking particles of lower velocity, means for introducing a gas stream flowing parallel to a side of the membrane facing the output region, and means for withdrawing the gas stream enriched with particles passing through the membrane.
Claim 42
Dependent Claim 190 words
A particle separator comprising a chamber having an input and an output end, an orifice at the input end for introducing a gas flow into the chamber, means for forming a mixture of heavier and lighter species of particles to be separated and a carrier gas, means for expanding the mixture through the orifice into the chamber in a high velocity flow, means for maintaining a background gas in a deceleration region of the chamber downstream of the orifice for differentially decelerating the heavier and lighter species, a membrane at a location downstream of the decleration region corresponding to a mean deceleration distance of the lighter particle species for passing a substantial flux of the heavier particle species to the output end of the chamber and for blocking a substantial flux of the lighter particle species, means for withdrawing a first output enriched in particles of the heavier species and a second output enriched in particles of the lighter species, means for maintaining a gas stream flowing parallel to a face of the membrane, and means for withdrawing an output of the gas stream enriched with a separated particle species.
Claim 43
Dependent Claim 190 words
A particle separator comprising a chamber having an input and an output end, an orifice at the input end for introducing a gas flow into the chamber, means for forming a mixture of heavier and lighter species of particles to be separated and a carrier gas, means for expanding the mixture through the orifice into the chamber in a high velocity flow, means for maintaining a background gas in a deceleration region of the chamber downstream of the orifice for differentially decelerating the heavier and lighter species, a membrane at a location downstream of the decleration region corresponding to a mean deceleration distance of the lighter particle species for passing a substantial flux of the heavier particle species to the output end of the chamber and for blocking a substantial flux of the lighter particle species, means for withdrawing a first output enriched in particles of the heavier species and a second output enriched in particles of the lighter species, means for maintaining a gas stream flowing parallel to a face of the membrane, and means for withdrawing an output of the gas stream enriched with a separated particle species.
Claim 44
Dependent Claim 74 words
A particle separator comprising means for introducing a gas flow containing heavier and lighter species of particles, means for maintaining a background gas in a region of the gas flow for differentially decelerating the particle species, and means including a membrane downstream of said region for separating said heavier from said lighter particle species, said membrane having a cryogenically cooled surface so that the molecules which collide with the membrane surface are adsorbed thereon.
Claim 45
Dependent Claim 74 words
A particle separator comprising means for introducing a gas flow containing heavier and lighter species of particles, means for maintaining a background gas in a region of the gas flow for differentially decelerating the particle species, and means including a membrane downstream of said region for separating said heavier from said lighter particle species, said membrane having a cryogenically cooled surface so that the molecules which collide with the membrane surface are adsorbed thereon.
Claim 46
Dependent Claim 12 words
The particle separator of claim 34 wherein said cryogenic surfaces are rotatable.

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1984-08-17 1985-02-16 1985-08-18 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1988-08-17 1989-02-16 1989-08-18 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1992-08-17 1993-02-16 1993-08-18 $7700.00 Window Closed / Lapsed

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