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US4283365A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for melt-spinning acrylonitrile polymer fiber using vertically disposed compression zone

Assignee: Wyeth Holdings LLC
•
Filing: 1979-02-21
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Granted: 1981-08-11
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Expires: 1999-02-21
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Abstract

Abstract Use of a vertically disposed compression zone for providing a fusion melt of acrylonitrile polymer and water in conjunction with melt spinning provides reduced bubble count in the resulting fiber.

Inventors

  • 👤 Chi C. Young
  • 👤 Francesco DeMaria

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-05 03:21
CPC Classifications
D; D01; D01D; D01D5/00; D01D5/08; D01D5/096; D01F; D01F6/00; D01F6/02; D01F6/18

Claims Analysis

Total Claims: 5
Claim 1
Independent Claim 148 words
A process for preparing acrylonitrile polymer fiber which comprises continuously feeding a particulate composition of about 70 to about 95 weight percent of a fiber-forming acrylonitrile polymer and, correspondingly, from about 30 to about 5 weight percent of water into the top of a vertically disposed compression zone operating at a compression ratio of greater than about 1:1 and less than about 1:3 and a temperature sufficient to provide a fusion melt at autogeneous pressure, said feeding being conducted at a rate which satisfies the operating capacity of said compression zone so as to provide a vapor seal, and extruding the resulting fusion melt from the bottom of said compression zone through a spinnerette assembly using the pressure generated within said compression zone, said extruding being directly into a steam-pressurized solidification zone maintained under conditions which control release of water from the nascent filaments to prevent deformation thereof.
Claim 2
Dependent Claim 148 words
A process for preparing acrylonitrile polymer fiber which comprises continuously feeding a particulate composition of about 70 to about 95 weight percent of a fiber-forming acrylonitrile polymer and, correspondingly, from about 30 to about 5 weight percent of water into the top of a vertically disposed compression zone operating at a compression ratio of greater than about 1:1 and less than about 1:3 and a temperature sufficient to provide a fusion melt at autogeneous pressure, said feeding being conducted at a rate which satisfies the operating capacity of said compression zone so as to provide a vapor seal, and extruding the resulting fusion melt from the bottom of said compression zone through a spinnerette assembly using the pressure generated within said compression zone, said extruding being directly into a steam-pressurized solidification zone maintained under conditions which control release of water from the nascent filaments to prevent deformation thereof.
Claim 3
Dependent Claim 19 words
The process of claim 1 wherein said nascent filaments are stretched for molecular orientation while in said solidification zone.
Claim 4
Dependent Claim 18 words
The process of claim 2 wherein said stretching is at a stretch ratio of at least about 25.
Claim 5
Dependent Claim 30 words
The process of claim 2 wherein said stretching is conducted in two stages with the first stage being conducted at a stretch ratio less than that of the second stage.

References Cited (Backward Citations)

US3627867A Cited
US3585263A Cited
US4163770A Cited
US4117073A Cited
US3991153A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1984-08-10 1985-02-09 1985-08-11 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1988-08-10 1989-02-09 1989-08-11 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1992-08-10 1993-02-09 1993-08-11 $7700.00 Window Closed / Lapsed

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