US4282173A
Expired / Lapsed
US
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Method for manufacturing refractory material having numerous through pores extending in a certain direction
Assignee: Isolite Insulating Products Co Ltd
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Filing: 1978-11-13
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Granted: 1981-08-04
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Expires: 1998-11-13
Abstract
Abstract The present invention relates to a method for manufacturing a refractory erial having numerous through pores in a certain direction. The refractory material is manufactured by covering a woven fabric composed of combustible weft and/or warp threads with a slurry of a refractory material, and then drying and baking the coated fabric to burn out the combustible yarns so that the desired through pores may be obtained in directions corresponding to the direction of the burned out weft and warp threads.
Inventors
- 👤 Tsunemi Ochiai
- 👤 Goro Saiki
- 👤 Teruo Shimao
- 👤 Toshitaro Saito
- 👤 Shizuo Nakanishi
- 👤 Takeo Saeki
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-09 06:10
CPC Classifications
C; C04; C04B; C04B38/00; C04B38/06; C04B38/063; C04B38/0635; C04B38/0645; C04B38/065; C04B2111/00; C04B2111/00474; C04B2111/0087; Y; Y10; Y10S; Y10S264/00; Y10S264/44; Y10S425/00; Y10S425/012
Claims Analysis
Total Claims: 13
Claim 1
Independent Claim
270 words
In a method for making a shaped article of a refractory material suitable for contact with molten metal, said shaped article being the type wherein a refractory material in paste or slurry state is contacted with a woven fabric and the thus contacted fabric and refractory material are laminated into the desired shape and the liminate preform block thus obtained is heated to dry the block and to burn off the combustible fibers of said fabric and then fired to sinter said refractory material, the improvement which comprises at least one of the weft fibers or the warp fibers of the woven fabric being combustible and said combustible fibers having a diameter between 40 to 300 microns, and wherein a vibration between about 900 to 10,000 Vpm and an amplitude of 0.1 to 1.0 mm is applied to said woven fabric in said laminating step to remove air bubbles from and increase the uniformity of the laminate, and the combustible portion of the fabric is removed by said heating to produce a multiplicity of pores extending through said shaped refractory article corresponding to the thus removed fibers and wherein prior to the burn off, the surface of the body which is parallel to the through pores is temporarily covered with an insulating layer, leaving the end faces perpendicular to the through pores uninsulated and wherein the burn off is carried out by applying heat to the uninsulated end faces so as to exhaust the gas produced by the combustion of the fibers and produce smooth escape of the gas and avoid pressure buildup, and then removing the temporary insulating layer.
Claim 2
Dependent Claim
270 words
In a method for making a shaped article of a refractory material suitable for contact with molten metal, said shaped article being the type wherein a refractory material in paste or slurry state is contacted with a woven fabric and the thus contacted fabric and refractory material are laminated into the desired shape and the liminate preform block thus obtained is heated to dry the block and to burn off the combustible fibers of said fabric and then fired to sinter said refractory material, the improvement which comprises at least one of the weft fibers or the warp fibers of the woven fabric being combustible and said combustible fibers having a diameter between 40 to 300 microns, and wherein a vibration between about 900 to 10,000 Vpm and an amplitude of 0.1 to 1.0 mm is applied to said woven fabric in said laminating step to remove air bubbles from and increase the uniformity of the laminate, and the combustible portion of the fabric is removed by said heating to produce a multiplicity of pores extending through said shaped refractory article corresponding to the thus removed fibers and wherein prior to the burn off, the surface of the body which is parallel to the through pores is temporarily covered with an insulating layer, leaving the end faces perpendicular to the through pores uninsulated and wherein the burn off is carried out by applying heat to the uninsulated end faces so as to exhaust the gas produced by the combustion of the fibers and produce smooth escape of the gas and avoid pressure buildup, and then removing the temporary insulating layer.
Claim 3
Dependent Claim
50 words
The method of claim 1 wherein a tension is applied to the woven fabric in said laminating step to form a laminate block, said tension being in the range where the total force provided by the tension and said vibration does not exceed the shearing stress of the woven fabric.
Claim 4
Dependent Claim
17 words
The method of claim 1 wherein the refractory material in paste or slurry state is vacuum deaired.
Claim 5
Dependent Claim
35 words
The method of claim 1 wherein the laminate block is formed by winding the fabric into a roll, thereby impregnating a part of the laminate block in the refractory material in paste or slurry state.
Claim 6
Dependent Claim
43 words
The method of claim 1 wherein the laminate block is wound into a roll, said roll being partially submerged in a bath of a slurry or paste of said refractory material and wherein the vibration is applied to said bath and said roll.
Claim 7
Dependent Claim
20 words
The method of claim 1 wherein the refractory material contains greater than about 30 percent by weight of fine particles.
Claim 8
Dependent Claim
25 words
The method of claim 1 wherein the number of combustible fibers is sufficient to produce from about 2000 to 8500 pores per cm 2 .
Claim 9
Dependent Claim
16 words
The method of claim 1 wherein the pores produced are less than 300 microns in diameter.
Claim 10
Dependent Claim
21 words
The method of claim 1 wherein the pores produced have a diameter in the range from about 40 to 300 microns.
Claim 11
Dependent Claim
21 words
The method of claim 1 wherein the surface parallel to the through pores is insulated with ceramic fibers or ceramic wool.
Claim 12
Dependent Claim
40 words
The method of claim 1 wherein the body, after firing, is impregnated with a liquid containing a carbonaceous composition and the thus impreganted body is fired again to produce carbon within the through pores and reduce the pore diameter thereof.
Claim 13
Dependent Claim
61 words
The method of claim 1 wherein the heating step is carried out by first heating the laminate up to a temperature of about 600° C. for a time period and a rate sufficiently low to avoid bursting the body due to escaping moisture and gases and then heating at a temperature from about 1500° to 1800° C. to effect final baking.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1984-08-03 | 1985-02-02 | 1985-08-04 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1988-08-03 | 1989-02-02 | 1989-08-04 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1992-08-03 | 1993-02-02 | 1993-08-04 | $7700.00 | Window Closed / Lapsed |