US4267049A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Biological sludge-energy recycling method
Assignee: WASTE-ENERGY Corp A NE CORP
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Filing: 1979-06-27
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Granted: 1981-05-12
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Expires: 1999-06-27
Abstract
Abstract A method is described for converting treated sludge into an improved concentrated organic feedstock. The method includes conditioning of sludge with hydrolytic enzymes, the mechanical disintegration of tissue and cell components, the removal of heavy metals, autolysis and dewatering to produce an organic fertilizer or feedstock. Product stabilization for long-term storage is achieved by acidification or addition of granular sorbents. Agricultural fertilizers are produced from input raw material such as sludge from municipal waste-water treatment facilities or sludge from biological processing of other organic wastes. Animal feed protein concentrates are produced from cultured cellular biomass sludge inputs. The separated heavy metals fraction may be refined to recover individual minerals. Energy usually expended for disposal of sludge as wastes may be applied to recycling such sludge into useful products of this invention. The commercial equivalents of these products usually are manufactured from petrochemical and other primary energy resources.
Inventors
- 👤 Lennart G. Erickson
- 👤 Howard E. Worne
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-04 17:02
CPC Classifications
C; C02; C02F; C02F1/00; C02F1/52; C02F1/5272; A; A23; A23K; A23K10/00; A23K10/10; C02F11/00; C02F11/004; C02F11/12; C02F3/00; C02F3/02; C02F3/12; C02F3/34; C02F9/00; C05; C05F; C05F17/00; C05F17/20; C05F17/40; C05F7/00; C02F2303/00; C02F2303/06; Y; Y02; Y02A; Y02A40/00; Y02A40/10; Y02A40/20; Y02P; Y02P20/00; Y02P20/141; Y02P20/145; Y02W; Y02W10/00; Y02W10/10; Y02W30/00; Y02W30/40; Y10; Y10S; Y10S210/00; Y10S210/902; Y10S210/911; Y10S210/912
Claims Analysis
Total Claims: 36
Claim 1
Independent Claim
103 words
A method for converting treated sludge into useful substances, the method comprising the steps of: hydrolyzing organic materials present in the sludge by adding to the sludge at least one of hydrolytic enzymes and hydrolytic enzyme producing microorganisms; thereafter disintegrating organic cells present in the sludge into organic particles to thereby form a colloidal slurry including the particles; holding at least one of the sludge, including the enzymes or the microorganisms, and the slurry, including the particles; and thereafter separating the slurry into an effluent and a moist product including the organic particles and adapted for a relatively rapid metabolization by living organisms.
Claim 2
Independent Claim
103 words
A method for converting treated sludge into useful substances, the method comprising the steps of: hydrolyzing organic materials present in the sludge by adding to the sludge at least one of hydrolytic enzymes and hydrolytic enzyme producing microorganisms; thereafter disintegrating organic cells present in the sludge into organic particles to thereby form a colloidal slurry including the particles; holding at least one of the sludge, including the enzymes or the microorganisms, and the slurry, including the particles; and thereafter separating the slurry into an effluent and a moist product including the organic particles and adapted for a relatively rapid metabolization by living organisms.
Claim 3
Dependent Claim
48 words
A method according to claim 1 wherein the step of holding comprises holding the slurry after the step of disintegrating so that the hydrolytic enzymes in the slurry and endocellular enzymes released into the slurry by the organic cells during the step of disintegrating further hydrolyze the particles.
Claim 4
Dependent Claim
23 words
A method according to claim 2 wherein the step of holding the slurry is carried out for no more than about 12 hours.
Claim 5
Dependent Claim
22 words
A method according to claim 3 wherein the step of holding the slurry is carried out for at least about six hours.
Claim 6
Dependent Claim
32 words
A method according to claim 3 including the step of maintaining the temperature of the slurry during the holding step in the range of between about 16° C. to about 40° C.
Claim 7
Dependent Claim
36 words
A method according to claim 1 wherein the step of holding comprises holding the sludge for no more than about two hours after the step of adding and prior to the step of disintegrating the cells.
Claim 8
Dependent Claim
29 words
A method according to claim 6 including the step of maintaining the temperature of the sludge during the holding step at between about 16° C. to about 40° C.
Claim 9
Dependent Claim
15 words
A method according to claim 7 wherein the temperature is held at about 37° C.
Claim 10
Dependent Claim
24 words
A method according to claim 6 wherein the step of holding the sludge is carried out for between about one to about two hours.
Claim 11
Dependent Claim
35 words
A method according to claim 1 including the step of adding to the product an edible acid in an amount sufficient to inhibit microbial and pathogenic activity during storage and transport of the product .
Claim 12
Dependent Claim
17 words
A method according to claim 10 including the step of utilizing the acidified product as a fertilizer.
Claim 13
Dependent Claim
18 words
A method according to claim 10 including the step of utilizing the acidified product as a feed supplement.
Claim 14
Dependent Claim
49 words
A method according to claim 1 including the step of adding to the product a sufficient amount of a sorbent material to reduce the moisture content of the product to a level at which bacteria and pathogens are prevented from being further hydrolyzed by enzymes present in the product.
Claim 15
Dependent Claim
20 words
A method according to claim 13 including the step of using the product including the sorbent material as a fertilizer.
Claim 16
Dependent Claim
21 words
A method according to claim 13 including the step of using the product including the sorbent material as a feed supplement.
Claim 17
Dependent Claim
28 words
A method according to claim 1 including the step of contacting the slurry with a metal chelating substrate after the step of disintegrating to remove heavy metals therefrom.
Claim 18
Independent Claim
124 words
A method for converting organic cells and other substances in treated sludge into a readily metabolizable product comprising the steps of: adding to the sludge hydrolytic enzymes to hydrolyze the organic cells and other hydrolyzable substances in the sludge; rupturing the hydrolyzed cells after the step of adding to form a colloidal slurry including ruptured organic cell particles and to thereby release into the colloidal slurry endocellular enzymes present in the cells; holding the colloidal slurry for a sufficient length of time so that the hydrolytic enzymes and the endocellular enzymes further hydrolyze organic substances in the slurry and thereby form a readily dewaterable, substantially gel free microparticulate slurry; and thereafter dewatering the microparticulate slurry to form a moist product comprising microparticulate, organic substances.
Claim 19
Independent Claim
124 words
A method for converting organic cells and other substances in treated sludge into a readily metabolizable product comprising the steps of: adding to the sludge hydrolytic enzymes to hydrolyze the organic cells and other hydrolyzable substances in the sludge; rupturing the hydrolyzed cells after the step of adding to form a colloidal slurry including ruptured organic cell particles and to thereby release into the colloidal slurry endocellular enzymes present in the cells; holding the colloidal slurry for a sufficient length of time so that the hydrolytic enzymes and the endocellular enzymes further hydrolyze organic substances in the slurry and thereby form a readily dewaterable, substantially gel free microparticulate slurry; and thereafter dewatering the microparticulate slurry to form a moist product comprising microparticulate, organic substances.
Claim 20
Dependent Claim
29 words
A method according to claim 17 including the step of inhibiting microbial and pathogenic activity in the product during storage and shipment of the product prior to its use.
Claim 21
Dependent Claim
32 words
A method according to claim 17 wherein the treated sludge comprises a cellular biomass substantially free of heavy metals, and including the step of using the product as an animal feed supplement.
Claim 22
Dependent Claim
45 words
A method according to claim 17 wherein the step of holding the colloidal slurry in a tank is carried out for no more than about 12 hours and maintaining the temperature of the colloidal slurry in the tank at no more than about 40° C.
Claim 23
Dependent Claim
57 words
A method according to claim 17 wherein the step of adding comprises the steps of adding to the sludge a substance comprising hydrolytic enzymes, thereafter holding the sludge for up to about two hours, and maintaining the temperature of the sludge during its holding step in the range of between about 16° C. to about 40° C.
Claim 24
Dependent Claim
25 words
A method according to claim 17 wherein the step of adding hydrolytic enzymes comprises the steps of adding to the sludge hydrolytic enzyme producing microorganisms.
Claim 25
Independent Claim
114 words
A method for converting treated sludge into a readily metabolizable product comprising the steps of: contacting the sludge with hydrolytic enzymes to hydrolyze organic cells in the sludge and thereby to make them more susceptible to rupture when subjected to mechanical forces by adding to the sludge a substance capable of providing the sludge with hydrolytic enzymes; thereafter rupturing the cells in the sludge to form a colloidal slurry including ruptured organic cell particles, endocellular enzymes and gelled substances released by the cells during their rupture; holding at least one of the sludge, including the enzymes, and the slurry, including the particles; and thereafter separating the slurry into an effluent and a moist product.
Claim 26
Independent Claim
114 words
A method for converting treated sludge into a readily metabolizable product comprising the steps of: contacting the sludge with hydrolytic enzymes to hydrolyze organic cells in the sludge and thereby to make them more susceptible to rupture when subjected to mechanical forces by adding to the sludge a substance capable of providing the sludge with hydrolytic enzymes; thereafter rupturing the cells in the sludge to form a colloidal slurry including ruptured organic cell particles, endocellular enzymes and gelled substances released by the cells during their rupture; holding at least one of the sludge, including the enzymes, and the slurry, including the particles; and thereafter separating the slurry into an effluent and a moist product.
Claim 27
Dependent Claim
69 words
A method according to claim 23 wherein the step of separating includes the step of dewatering the slurry to form the moist product comprising the ruptured cell particles, and wherein the step of holding the slurry is carried out for up to about 12 hours prior to the step of dewatering to thereby further hydrolyze the particles and gelled substances present in the slurry to facilitate the dewatering step.
Claim 28
Dependent Claim
24 words
A method according to claim 24 wherein the step of holding is performed no later than about 20 hours after the step of contacting.
Claim 29
Independent Claim
174 words
A method for converting organic cells and other organic substances in treated sludge into a readily metabolizable product comprising the steps of: adding hydrolytic enzymes or hydrolytic enzyme producing microorganisms to the sludge and holding the sludge including enzymes for a sufficient length of time to hydrolyze the polysaccharide slime coating on the cells, to release into the sludge any heavy metal ions occluded in the coating, and to soften the walls of the cells; rupturing the cells in the sludge to form a colloidal slurry comprising ruptured cell particles, heavy metal ions endocellular enzymes released by the cells during their rupture and a gel; thereafter, autolyzing the colloidal slurry by holding it in a tank for a sufficient length of time to permit enzymes present in the colloidal slurry to hydrolyze the particles and the gel and form a microparticulate slurry including the ruptured cell particles; and thereafter dewatering the microparticulate slurry to form a substantially clear effluent and a moist product comprising the ruptured cell particles previously present in the microparticulate slurry.
Claim 30
Independent Claim
174 words
A method for converting organic cells and other organic substances in treated sludge into a readily metabolizable product comprising the steps of: adding hydrolytic enzymes or hydrolytic enzyme producing microorganisms to the sludge and holding the sludge including enzymes for a sufficient length of time to hydrolyze the polysaccharide slime coating on the cells, to release into the sludge any heavy metal ions occluded in the coating, and to soften the walls of the cells; rupturing the cells in the sludge to form a colloidal slurry comprising ruptured cell particles, heavy metal ions endocellular enzymes released by the cells during their rupture and a gel; thereafter, autolyzing the colloidal slurry by holding it in a tank for a sufficient length of time to permit enzymes present in the colloidal slurry to hydrolyze the particles and the gel and form a microparticulate slurry including the ruptured cell particles; and thereafter dewatering the microparticulate slurry to form a substantially clear effluent and a moist product comprising the ruptured cell particles previously present in the microparticulate slurry.
Claim 31
Dependent Claim
27 words
A method according to claim 26 including the step of removing from the slurry heavy metals present therein by contacting the slurry with a metal chelating substrate.
Claim 32
Independent Claim
181 words
A method for processing treated sludge including organic cells and heavy metals to recover therefrom usable materials comprising the steps of: adding to the sludge hydrolytic enzymes; holding the sludge and the added enzymes for a sufficient length of time to at least partially hydrolyze the walls of the cells and any polysaccharide slime coating present on the cells; thereafter rupturing the cells in the sludge to form a collodial slurry including ruptured cell particles and a gel and to thereby further release into the collodial slurry endocellular enzymes present in the cells; contacting the slurry with a metal chelating substrate to remove heavy metals therefrom; further hydrolyzing organic substances in the colloidal slurry by holding the slurry in a tank for sufficient length of time to hydrolyze the particles and the gel and to thereby form a microparticulate slurry; dewatering the microparticulate slurry and collecting a moist product; storing the product; preventing decomposition of the product by inhibiting microbial and pathogenic activity in the product being stored; and thereafter using the product as a readily metabolizable substance for living organisms.
Claim 33
Independent Claim
181 words
A method for processing treated sludge including organic cells and heavy metals to recover therefrom usable materials comprising the steps of: adding to the sludge hydrolytic enzymes; holding the sludge and the added enzymes for a sufficient length of time to at least partially hydrolyze the walls of the cells and any polysaccharide slime coating present on the cells; thereafter rupturing the cells in the sludge to form a collodial slurry including ruptured cell particles and a gel and to thereby further release into the collodial slurry endocellular enzymes present in the cells; contacting the slurry with a metal chelating substrate to remove heavy metals therefrom; further hydrolyzing organic substances in the colloidal slurry by holding the slurry in a tank for sufficient length of time to hydrolyze the particles and the gel and to thereby form a microparticulate slurry; dewatering the microparticulate slurry and collecting a moist product; storing the product; preventing decomposition of the product by inhibiting microbial and pathogenic activity in the product being stored; and thereafter using the product as a readily metabolizable substance for living organisms.
Claim 34
Dependent Claim
33 words
A method according to claim 28 including the step of holding the slurry in a tank for a length of time which exceeds the length of time for which the sludge is held.
Claim 35
Dependent Claim
32 words
A method according to claim 29 wherein the step of preventing decomposition of the product comprises the step of acidifying the product to a pH of between about 3 to about 3.5.
Claim 36
Dependent Claim
23 words
A method according to claim 28 including the step of adjusting the pH of the sludge to between about 6.5 to about 7.2.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1984-05-11 | 1984-11-10 | 1985-05-12 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1988-05-11 | 1988-11-10 | 1989-05-12 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1992-05-11 | 1992-11-10 | 1993-05-12 | $7700.00 | Window Closed / Lapsed |