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US4265704A Expired / Lapsed US ⏱️ 0.0 years remaining

Method of dispersing bundles of glass fibers for making glass fiber mats by the wet-laid process

Assignee: Building Materials Corp of America
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Filing: 1979-03-30
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Granted: 1981-05-05
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Expires: 1999-03-30
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Abstract

Abstract What is provided herein is a method of dispersing bundles of glass fibers for making uniform glass fiber mats by the wet-laid process. Well-dispersed glass fiber compositions are prepared herein by agitating chopped bundles of glass fibers in water with a small amount of a surfactant which is a polyethoxylated derivative of the amide condensation product of fatty acids and polyethylenepolyamines. The dispersions are formed at relatively high glass fiber consistencies, and at low surfactant concentrations.

Inventors

  • 👤 Roop C. Nahta

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-01 17:26
CPC Classifications
D; D21; D21H; D21H13/00; D21H13/36; D21H13/38; D21H13/40

Claims Analysis

Total Claims: 12
Claim 1
Independent Claim 179 words
In the manufacture of uniform glass mats at a high rate of production by the wet-laid process, the improved method which comprises: forming an aqueous dispersion of glass fibers by mixing bundles of said fibers of about 1/4 to 3 inches in length in an aqueous medium at a fiber consistency of about 0.001 to 3% with about 5-500 ppm of a dispersant which is a polyethoxylated derivative of an amide condensation product of fatty acids and polyethylenepolyamines, said product comprises predominately a mixture of the I-IV compounds as defined below: ##STR2## wherein a through k are positive integers; a and e can be simultaneously or individually zero; b, f, g and j can be individually, simultaneously or in any combination, zero; b cannot be zero unless a is zero; f and g cannot be zero unless e is zero; 200≧a+b+2c+4d+e+f+g+2h+2i+j+2k≧10; and R is alkyl, C 8 -C 30 , thereby to substantially disperse said bundles into individual fibers within the aqueous medium, and, passing said dispersion through a mat-forming screen to form the desired uniform glass fiber mat.
Claim 2
Dependent Claim 179 words
In the manufacture of uniform glass mats at a high rate of production by the wet-laid process, the improved method which comprises: forming an aqueous dispersion of glass fibers by mixing bundles of said fibers of about 1/4 to 3 inches in length in an aqueous medium at a fiber consistency of about 0.001 to 3% with about 5-500 ppm of a dispersant which is a polyethoxylated derivative of an amide condensation product of fatty acids and polyethylenepolyamines, said product comprises predominately a mixture of the I-IV compounds as defined below: ##STR2## wherein a through k are positive integers; a and e can be simultaneously or individually zero; b, f, g and j can be individually, simultaneously or in any combination, zero; b cannot be zero unless a is zero; f and g cannot be zero unless e is zero; 200≧a+b+2c+4d+e+f+g+2h+2i+j+2k≧10; and R is alkyl, C 8 -C 30 , thereby to substantially disperse said bundles into individual fibers within the aqueous medium, and, passing said dispersion through a mat-forming screen to form the desired uniform glass fiber mat.
Claim 3
Dependent Claim 14 words
A method according to claim 1 wherein in said compounds a+b+2c+4d+e+f+g+2h+2i+2h is about 13.5.
Claim 4
Dependent Claim 18 words
A method according to claim 1 where in said compounds R is about C 12 -C 18 .
Claim 5
Dependent Claim 19 words
A method according to claim 1 wherein said fatty acids are a mixture of coco and tallow fatty acids.
Claim 6
Dependent Claim 18 words
A method according to claim 1 wherein said glass fibers are about 1/2 to 2 inches in length.
Claim 7
Dependent Claim 16 words
A method according to claim 1 wherein said glass fibers are about 1 inch in length.
Claim 8
Dependent Claim 16 words
A method according to claim 1 wherein said glass fibers are about 3-20 microns in diameter.
Claim 9
Dependent Claim 16 words
A method according to claim 1 wherein said glass fibers are about 15 microns in diameter.
Claim 10
Dependent Claim 14 words
A method according to claim 1 wherein said glass fiber consistency is about 0.05%.
Claim 11
Dependent Claim 18 words
A method according to claim 1 wherein said dispersant is present in a concentration of about 10-25 ppm.
Claim 12
Dependent Claim 18 words
A method according to claim 1 wherein said fiber dispersion is diluted before passing through said mat-forming machines.

References Cited (Backward Citations)

US2681354A Cited
US3573158A Cited
US3766003A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1984-05-04 1984-11-03 1985-05-05 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1988-05-04 1988-11-03 1989-05-05 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1992-05-04 1992-11-03 1993-05-05 $7700.00 Window Closed / Lapsed

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