US4255192A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Homogenous bonding of dispersed phase alloy
Assignee: Manufacturers Hanover Trust Co
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Filing: 1979-12-17
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Granted: 1981-03-10
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Expires: 1999-12-17
Abstract
Abstract Dispersed phase dental alloy made by mechanically blending mixtures of lathe cut dental amalgam alloy particles and spheroidal silver-copper alloy particles has superior properties as an amalgam when a mechanical blend of the mixture of alloy particles is treated prior to amalgamation with dilute aqueous mineral acid solutions or with methyl alcohol.
Inventors
- 👤 Charles F. Burns
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-04 02:37
CPC Classifications
A; A61; A61K; A61K6/00; A61K6/80; A61K6/84; A61K6/847; Y; Y10; Y10S; Y10S75/00; Y10S75/955
Claims Analysis
Total Claims: 10
Claim 1
Independent Claim
239 words
In a process for making a dental alloy mixture which will amalgamate to form a restoration with superior compressive strength and low creep properties by mechanically mixing lathe cut dental amalgam alloy particles and silver-copper alloy spheres, the improvement comprising treating a mechanical mixture of lathe cut dental amalgam alloy particles of minus 200 mesh, having the composition: silver 40--75%, tin 20--30%; copper 2--30%, and from 0 to 30% of one or more metals selected from the group consisting of indium, zinc, gold, mercury, manganese, cadmium and aluminum, and spheroidal silver-copper alloy of minus 325 mesh, having the composition: silver 54--72%; copper 24--40%, and varying amounts of one or more metals selected from the group consisting of nickel, zinc, tin or indium, the said mixture of alloys containing from about 20 to 50% by weight of the silver-copper alloy, with an effective amount of a treating solution selected from the group consisting of 5 volume % to 100 volume % hydrochloric acid, 5 volume % to 50 volume % sulfuric acid, 5 volume % to 20 volume % nitric acid and 5 volume % to 100 volume % methyl alcohol to aglommerate the mixture of alloy particles, separating the aglommerated mixture of alloy particles from the treating solution, washing the agglommerated alloy particles with water to remove the treating solution when the treating solution is one of the mineral acids, and finally drying the aglommerated mixture of alloy particles.
Claim 2
Dependent Claim
239 words
In a process for making a dental alloy mixture which will amalgamate to form a restoration with superior compressive strength and low creep properties by mechanically mixing lathe cut dental amalgam alloy particles and silver-copper alloy spheres, the improvement comprising treating a mechanical mixture of lathe cut dental amalgam alloy particles of minus 200 mesh, having the composition: silver 40--75%, tin 20--30%; copper 2--30%, and from 0 to 30% of one or more metals selected from the group consisting of indium, zinc, gold, mercury, manganese, cadmium and aluminum, and spheroidal silver-copper alloy of minus 325 mesh, having the composition: silver 54--72%; copper 24--40%, and varying amounts of one or more metals selected from the group consisting of nickel, zinc, tin or indium, the said mixture of alloys containing from about 20 to 50% by weight of the silver-copper alloy, with an effective amount of a treating solution selected from the group consisting of 5 volume % to 100 volume % hydrochloric acid, 5 volume % to 50 volume % sulfuric acid, 5 volume % to 20 volume % nitric acid and 5 volume % to 100 volume % methyl alcohol to aglommerate the mixture of alloy particles, separating the aglommerated mixture of alloy particles from the treating solution, washing the agglommerated alloy particles with water to remove the treating solution when the treating solution is one of the mineral acids, and finally drying the aglommerated mixture of alloy particles.
Claim 3
Dependent Claim
16 words
The process of claim 1 in which the treating solution is 10 volume % hydrochloric acid.
Claim 4
Dependent Claim
30 words
The process of claim 1 in which the effective amount of treating solution is within the range of 1 to 5 cc. of treating solution per gram of alloy mixture.
Claim 5
Dependent Claim
40 words
The process of claim 1 in which the concentration of the spheroidal silver-copper alloy in the mechanical mixture of alloys is one-third part by weight and the concentration of the lathe cut dental amalgam alloy is two-thirds parts be weight.
Claim 6
Dependent Claim
21 words
The process of claim 1 in which the spheroidal silver-copper alloy has the composition 72% weight silver and 28% weight copper.
Claim 7
Dependent Claim
21 words
The process of claim 1 in which the particle size of the lathe cut dental amalgam alloy is minus 400 mesh.
Claim 8
Dependent Claim
26 words
The process of claim 1 in which the composition of the lathe cut dental amalgam alloy is silver--70%, tin--25%, copper--3.5% and zinc--1.5%, all percentages by weight.
Claim 9
Dependent Claim
16 words
The process of claim 1 in which the spheroidal silver-copper alloy is minus 400 mesh size.
Claim 10
Dependent Claim
37 words
The dental amalgam prepared by triturating the dental alloy mixture of claim 1, which, after amalgamation, has a one-hour compressive strength of about 31,500 to 34,500 pounds per square inch, and a static creep of about 0.15%.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1984-03-09 | 1984-09-08 | 1985-03-10 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1988-03-09 | 1988-09-08 | 1989-03-10 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1992-03-09 | 1992-09-08 | 1993-03-10 | $7700.00 | Window Closed / Lapsed |