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US4254104A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for preparing stable oil-in-water emulsions

Assignee: Shiseido Co Ltd
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Filing: 1975-11-12
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Granted: 1981-03-03
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Expires: 1995-11-12
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Abstract

Abstract A process for preparing a stable oil-in-water emulsion which comprises: adding a hydrophilic nonionic surface active agent to a water-soluble solvent; adding an oil phase thereto to form an emulsion of the oil phase in the water-soluble solution; and adding a water phase to the resulting emulsion. Cosmetics including such oil-in-water emulsions are also disclosed.

Inventors

  • 👤 Takashi Suzuki

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-05 06:05
CPC Classifications
A; A61; A61Q; A61Q19/00; A61K; A61K8/00; A61K8/02; A61K8/04; A61K8/06; A61K8/062; A61K9/00; A61K9/0012; A61K9/0014; C; C09; C09K; C09K23/00; C09K23/34; C09K23/42; A61K2800/00; A61K2800/20; A61K2800/21; A61Q1/00; A61Q1/02; A61Q1/14; A61Q5/00; A61Q5/08

Claims Analysis

Total Claims: 4
Claim 1
Independent Claim 239 words
A process for preparing a stable oil-in-water emulsion which comprises: adding about 0.2 to about 10 weight parts of a hydrophilic nonionic surface active agent selected from the group consisting of (1) a compound of the formula R--X--CH.sub.2 --CH.sub.2 --O).sub.n H wherein R represents an alkane, alkene, aryl or chloestanol group containing 8 to 30 carbon atoms, X represents an ether or ester group, and n represents an integer of 15 to 120, (2) a compound of the formula ##STR3## wherein R and X are the same as defined above, and m and m' represent an integer of 1 to 30 and at least 15, respectively, and (3) an ethylene oxide adduct in which about 30 to about 100 moles of ethylene oxide is added to hydrogenated castor oil, to about 1 to about 90 weight parts of a water-soluble solvent capable of dissolving said surface active agent selected from the group consisting of (1) a lower monohydric alcohol having 1 to 7 carbon atoms, (2) a lower polyhydric alcohol having 3 to 6 carbon atoms, (3) polyethylene glycol having a molecular weight of about 60 to about 2000, and (4) a lower aliphatic amine having 2 or 3 carbon atoms; adding about 1 to about 90 weight parts of an oil thereto to form an emulsion of the oil in the water-soluble solvent; and adding about 5 to about 95 weight parts of water to the resulting emulsion.
Claim 2
Dependent Claim 239 words
A process for preparing a stable oil-in-water emulsion which comprises: adding about 0.2 to about 10 weight parts of a hydrophilic nonionic surface active agent selected from the group consisting of (1) a compound of the formula R--X--CH.sub.2 --CH.sub.2 --O).sub.n H wherein R represents an alkane, alkene, aryl or chloestanol group containing 8 to 30 carbon atoms, X represents an ether or ester group, and n represents an integer of 15 to 120, (2) a compound of the formula ##STR3## wherein R and X are the same as defined above, and m and m' represent an integer of 1 to 30 and at least 15, respectively, and (3) an ethylene oxide adduct in which about 30 to about 100 moles of ethylene oxide is added to hydrogenated castor oil, to about 1 to about 90 weight parts of a water-soluble solvent capable of dissolving said surface active agent selected from the group consisting of (1) a lower monohydric alcohol having 1 to 7 carbon atoms, (2) a lower polyhydric alcohol having 3 to 6 carbon atoms, (3) polyethylene glycol having a molecular weight of about 60 to about 2000, and (4) a lower aliphatic amine having 2 or 3 carbon atoms; adding about 1 to about 90 weight parts of an oil thereto to form an emulsion of the oil in the water-soluble solvent; and adding about 5 to about 95 weight parts of water to the resulting emulsion.
Claim 3
Dependent Claim 95 words
A process of claim 1, wherein said hydrophilic nonionic surface active agent is selected from the group consisting of polyoxyethylene (15-80 moles ethylene oxide) lanolin alcohol ether, polyoxyethylene (15-80 moles ethylene oxide) lanolin fatty acid ester, polyoxyethylene (15-60 moles ethylene oxide) cholesteryl ether, polyoxyethylene (15-60 moles ethylene oxide) cholestanyl ether, polyoxyethylene (20-80 moles ethylene oxide) polyoxypropylene (1-12 moles propylene oxide) cetanol ether, polyoxyethylene (20-80 moles ethylene oxide) polyoxypropylene (1-12 moles propylene oxide) cholestanyl ether, polyoxyethylene (20-80 moles ethylene oxide) polyoxypropylene (1-12 moles propylene oxide) cholesteryl ether, and polyoxyethylene (30-80 moles ethylene oxide) glycerol tri-12-hydroxystearate ether.
Claim 4
Dependent Claim 47 words
A process of claim 1, wherein said water-soluble solvent is selected from the group consisting of methanol, ethanol, propanol, isopropanol, benzyl alcohol, glycerin, ethylene glycol, diethylene glycol, triethylene glycol, 2,5-hexanediol, 2,3-butylene glycol, 2,4-heptanediol, hexylylene glycol, 1,5-pentanediol, 1,4-butanediol, propylene glycol, 1,3-butylene glycol, dipropylene glycol, monoethanolamine, di-ethanolamine, and triethanolamine.

References Cited (Backward Citations)

US2593112A Cited
US2677700A Cited
US3846546A Cited
US3824294A Cited
US3839212A Cited
US3876760A Cited
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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1984-03-02 1984-09-01 1985-03-03 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1988-03-02 1988-09-01 1989-03-03 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1992-03-02 1992-09-01 1993-03-03 $7700.00 Window Closed / Lapsed

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