US4252900A
Expired / Lapsed
US
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Recovery of starch from amylaceous roots and/or grains as aqueous slurries
Assignee: Equistar Chemicals LP
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Filing: 1979-06-25
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Granted: 1981-02-24
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Expires: 1999-06-25
Abstract
Abstract Starch is recovered from an amylaceous material such as manioc root or corn in the form of an aqueous slurry containing substantially all of the soluble components, e.g., carbohydrates and proteins, of the amylaceous material prior to processing. To accomplish such recovery, amylaceous material is milled in one or more steps in the presence of water to provide a slurry containing liberated starch particles and non-starch components. The initial aqueous starch slurry is then concentrated by removal of water therefrom. The water removed from the initial starch slurry contains soluble elements of the starch and is recycled to restore these elements to the starch recovery system.
Inventors
- 👤 Werner C. Muller
- 👤 Franklyn D. Miller
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-01 06:57
CPC Classifications
C; C12; C12P; C12P7/00; C12P7/02; C12P7/04; C12P7/06; C08; C08B; C08B30/00; C08B30/04; Y; Y02; Y02E; Y02E50/00; Y02E50/10
Claims Analysis
Total Claims: 29
Claim 1
Independent Claim
100 words
A process for the recovery of starch from at least one amylaceous material selected from the group consisting of amylaceous root and cereal grain which comprises: (a) milling the amylaceous material containing substantially the entire amount of water soluble components originally present therein in the presence of water to provide an aqueous slurry of starch particles and non-starch particles; (b) removing water from the starch slurry to concentrate the starch particle content therein; and, (c) recycling all of the water removed from the starch slurry to step (a) for use in milling amylaceous material in a subsequent starch recovery sequence.
Claim 2
Dependent Claim
100 words
A process for the recovery of starch from at least one amylaceous material selected from the group consisting of amylaceous root and cereal grain which comprises: (a) milling the amylaceous material containing substantially the entire amount of water soluble components originally present therein in the presence of water to provide an aqueous slurry of starch particles and non-starch particles; (b) removing water from the starch slurry to concentrate the starch particle content therein; and, (c) recycling all of the water removed from the starch slurry to step (a) for use in milling amylaceous material in a subsequent starch recovery sequence.
Claim 3
Dependent Claim
12 words
The process of claim 1 wherein the amylaceous root is manioc root.
Claim 4
Dependent Claim
11 words
The process of claim 1 wherein the amylaceous grain is corn.
Claim 5
Dependent Claim
35 words
The process of claim 1 wherein an amount of water is removed from the initial starch slurry to provide a concentrated aqueous starch slurry containing from about 20 to about 50 weight percent dry substance.
Claim 6
Dependent Claim
34 words
The process of claim 4 wherein an amount of water is removed from the initial starch slurry to provide a concentrated aqueous slurry containing from about 30 to about 40 weight percent dry substance.
Claim 7
Dependent Claim
32 words
The process of claim 1 wherein the process water contains about the same amount of soluble components extracted from previously processed amylaceous material as is contained in the amylaceous material undergoing processing.
Claim 8
Dependent Claim
31 words
The process of claim 1 wherein the concentrated aqueous starch slurry is introduced to a starch hydrolysis unit for the conversion of the starch to an aqueous solution of fermentable sugar.
Claim 9
Dependent Claim
47 words
The process of claim 7 wherein the aqueous solution of fermentable sugar contains substantially all of the soluble material of the aqueous starch slurry from which the fermentable sugar was obtained, said aqueous solution of fermentable sugar being introduced to a fermentation unit for conversion to ethanol.
Claim 10
Dependent Claim
131 words
A process for the recovery of starch from amylaceous root as an aqueous slurry, the starch being present in the root in adherent association with root fiber which comprises: (a) milling the fragmented root containing substantially the entire amount of water soluble components originally present therein at least once in the presence of water to separate starch from root fiber thus providing an aqueous slurry of starch particles and fiber particles; (b) separating the starch particles from the fiber particles to provide an initial substantially fiber-free aqueous starch slurry; and, (c) removing water from said initial starch slurry to provide a concentrated aqueous starch slurry with all of the removed water being recycled to step (a) as process water for use in milling fragmented root in a subsequent starch recovery sequence.
Claim 11
Dependent Claim
131 words
A process for the recovery of starch from amylaceous root as an aqueous slurry, the starch being present in the root in adherent association with root fiber which comprises: (a) milling the fragmented root containing substantially the entire amount of water soluble components originally present therein at least once in the presence of water to separate starch from root fiber thus providing an aqueous slurry of starch particles and fiber particles; (b) separating the starch particles from the fiber particles to provide an initial substantially fiber-free aqueous starch slurry; and, (c) removing water from said initial starch slurry to provide a concentrated aqueous starch slurry with all of the removed water being recycled to step (a) as process water for use in milling fragmented root in a subsequent starch recovery sequence.
Claim 12
Dependent Claim
12 words
The process of claim 9 wherein the amylaceous root is manioc root.
Claim 13
Dependent Claim
26 words
The process of claim 9 wherein the milling provides an aqueous starch slurry having an average particle size of from about 6 to about 30 microns.
Claim 14
Dependent Claim
35 words
The process of claim 9 wherein an amount of water is removed from the initial starch slurry to provide a concentrated aqueous starch slurry containing from about 20 to about 50 weight percent dry substance.
Claim 15
Dependent Claim
35 words
The process of claim 11 wherein an amount of water is removed from the initial starch slurry to provide a concentrated aqueous starch slurry containing from about 30 to about 40 weight percent dry substance.
Claim 16
Dependent Claim
25 words
The process of claim 9 wherein the fiber particles from which starch particles were removed is milled to separate still further amounts of starch therefrom.
Claim 17
Dependent Claim
30 words
The process of claim 9 wherein the process water contains about the same amount of soluble components extracted from previously processed root as is contained in the root undergoing processing.
Claim 18
Dependent Claim
31 words
The process of claim 9 wherein the concentrated aqueous starch slurry is introduced to a starch hydrolysis unit for the conversion of the starch to an aqueous solution of fermentable sugar.
Claim 19
Dependent Claim
47 words
The process of claim 16 wherein the aqueous solution of fermentable sugar contains substantially all of the soluble material of the aqueous starch slurry from which the fermentable sugar was obtained, said aqueous solution of fermentable sugar being introduced to a fermentation unit for conversion to ethanol.
Claim 20
Dependent Claim
145 words
A process for the recovery of starch from amylaceous grain as an aqueous slurry, the starch being present in the grain together with one or more water insoluble nonstarch components selected from the group consisting of protein, oil and cellulosic material, which comprises: (a) milling the grain containing substantially the entire amount of water soluble components originally present therein at least once in the presence of water to provide an aqueous slurry to starch particles and water insoluble non-starch components; (b) separating the starch particles from the water insoluble non-starch components to provide an initial aqueous starch slurry substantially free of water insoluble non-starch components; and, (c) removing water from said initial starch slurry to provide a concentrated aqueous starch slurry with all of the removed water being recycled to step (a) as process water for use in milling grain a subsequent starch recovery sequence.
Claim 21
Dependent Claim
145 words
A process for the recovery of starch from amylaceous grain as an aqueous slurry, the starch being present in the grain together with one or more water insoluble nonstarch components selected from the group consisting of protein, oil and cellulosic material, which comprises: (a) milling the grain containing substantially the entire amount of water soluble components originally present therein at least once in the presence of water to provide an aqueous slurry to starch particles and water insoluble non-starch components; (b) separating the starch particles from the water insoluble non-starch components to provide an initial aqueous starch slurry substantially free of water insoluble non-starch components; and, (c) removing water from said initial starch slurry to provide a concentrated aqueous starch slurry with all of the removed water being recycled to step (a) as process water for use in milling grain a subsequent starch recovery sequence.
Claim 22
Dependent Claim
26 words
The process of claim 18 wherein the amylaceous grain is corn having a germ component containing protein and oil and a bran component containing cellulosic material.
Claim 23
Dependent Claim
26 words
The process of claim 18 wherein the milling provides an aqueous starch slurry having an average particle size of from about 6 to about 30 microns.
Claim 24
Dependent Claim
35 words
The process of claim 18 wherein an amount of water is removed from the initial starch slurry to provide a concentrated aqueous starch slurry containing from about 20 to about 50 weight percent dry substance.
Claim 25
Dependent Claim
35 words
The process of claim 21 wherein an amount of water is removed from the initial starch slurry to provide a concentrated aqueous starch slurry containing from about 30 to about 40 weight percent dry substance.
Claim 26
Dependent Claim
25 words
The process of claim 18 wherein the fiber particles from which starch particles were removed is milled to separate still further amounts of starch therefrom.
Claim 27
Dependent Claim
30 words
The process of claim 18 wherein the process water contains about the same amount of soluble components extracted from previously processed root as is contained in the root undergoing processing.
Claim 28
Dependent Claim
31 words
The process of claim 18 wherein the concentrated aqueous starch slurry is introduced to a starch hydrolysis unit for the conversion of the starch to an aqueous solution of fermentable sugar.
Claim 29
Dependent Claim
47 words
The process of claim 25 wherein the aqueous solution of fermentable sugar contains substantially all of the soluble material of the aqueous starch slurry from which the fermentable sugar was obtained, said aqueous solution of fermentable sugar being introduced to a fermentation unit for conversion to ethanol.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1984-02-24 | 1984-08-25 | 1985-02-24 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1988-02-24 | 1988-08-25 | 1989-02-24 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1992-02-24 | 1992-08-25 | 1993-02-24 | $7700.00 | Window Closed / Lapsed |