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US4234531A Expired / Lapsed US ⏱️ 0.0 years remaining

Method for extruding a cross-linked material

Assignee: Societe Industrielle de Liaisons Electriques SA
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Filing: 1979-02-01
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Granted: 1980-11-18
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Expires: 1999-02-01
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Abstract

Abstract A method of extruding a cross-linked material, more particularly an insulating cross-linked material around an electrical cable. In an extrusion machine comprising a housing terminated with an extrusion head and provided with a filtering means adjacent the outlet end of said housing, the cross-linkable product is fed without addition of a cross-linking agent, said cross-linking agent being first introduced in said cross-linkable material downstream said filtering means. The cross-linkable material is kept in the housing at an elevated temperature to be in a fluid state, the cross-linking agent being introduced at a temperature slightly lower than its reaction temperature, whereby the extrudate may be at a temperature near the maximum temperature admissible for the extrusion of said material.

Inventors

  • 👤 Robert Jocteur

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-29 13:56
CPC Classifications
B; B29; B29C; B29C48/00; B29C48/25; B29C48/78; B29C48/80; B29C48/83; B29C48/832; B29C48/03; B29C48/06; B29C48/15; B29C48/285; B29C48/288; B29C48/2883; B29C48/29; B29C48/022; B29C48/05; B29K; B29K2101/00; B29K2101/10; B29K2105/00; B29K2105/0005; B29K2301/00; B29K2301/10

Claims Analysis

Total Claims: 13
Claim 1
Independent Claim 171 words
A method for continuously extruding in a closed environment an insulating material cross-linked by the separate addition of a cross-linking agent, which method comprises the following steps: (1) passing a cross-linkable insulating material through an extrusion machine provided adjacent its outlet end with a filtering means and at said outlet end with an extrusion head, said extrusion machine being heated to a temperature between about 200° and 220° C., said temperature being about the maximum temperature admissible for said material, so as to bring said material in a substantially fluid condition; (2) cooling the thus filtered material to a temperature between about 140° and 150° C. which temperature is slightly lower than the reaction temperature of the cross-linking agent; (3) injecting said cross-linking agent into said thus cooled material; and (4) conveniently mixing said cross-linkable material and said cross-linking agent; and thereafter (5)elevating the temperature of the mixture of step (4) to a temperature about the maximum temperature admissible for the extrusion of said extrudate before it leaves said extrusion head.
Claim 2
Independent Claim 171 words
A method for continuously extruding in a closed environment an insulating material cross-linked by the separate addition of a cross-linking agent, which method comprises the following steps: (1) passing a cross-linkable insulating material through an extrusion machine provided adjacent its outlet end with a filtering means and at said outlet end with an extrusion head, said extrusion machine being heated to a temperature between about 200° and 220° C., said temperature being about the maximum temperature admissible for said material, so as to bring said material in a substantially fluid condition; (2) cooling the thus filtered material to a temperature between about 140° and 150° C. which temperature is slightly lower than the reaction temperature of the cross-linking agent; (3) injecting said cross-linking agent into said thus cooled material; and (4) conveniently mixing said cross-linkable material and said cross-linking agent; and thereafter (5)elevating the temperature of the mixture of step (4) to a temperature about the maximum temperature admissible for the extrusion of said extrudate before it leaves said extrusion head.
Claim 3
Dependent Claim 17 words
The method of claim 1, wherein a cross-linking retarding agent is initially added to said cross-linkable material.
Claim 4
Dependent Claim 17 words
The method of claim 1, wherein a cross-linking retarding agent is initially added to said cross-linking agent.
Claim 5
Dependent Claim 16 words
The method of claim 1, wherein said cross-linking agent is in solution in a carrying liquid.
Claim 6
Dependent Claim 14 words
The method of claim 1, wherein said cross-linkable material is polyethylene or its derivates.
Claim 7
Dependent Claim 17 words
The method of claim 1, wherein said cross-linking agent is an organic peroxide such as dicumyl peroxide.
Claim 8
Dependent Claim 17 words
The method of claim 5, wherein said cross-linking agent is an organic peroxide such as dicumyl peroxide.
Claim 9
Dependent Claim 13 words
The method of claim 4, wherein said carrying liquid is a paraffinic oil.
Claim 10
Independent Claim 99 words
A method for continuously extruding a cross-linked insulating material in an extrusion machine comprising a housing and an extrusion head, said method comprising the steps of: introducing a cross-linkable material within said housing, forcing said material towards said extrusion head while heating same at a first elevated temperature, filtering said thus heated material at said first temperature, cooling said thus filtered material at a second temperature lower than said first temperature, injecting into said thus cooled material a cross-linking agent, and heating the thus obtained mixture at a third temperature higher than said second temperature and extruding said mixture.
Claim 11
Independent Claim 99 words
A method for continuously extruding a cross-linked insulating material in an extrusion machine comprising a housing and an extrusion head, said method comprising the steps of: introducing a cross-linkable material within said housing, forcing said material towards said extrusion head while heating same at a first elevated temperature, filtering said thus heated material at said first temperature, cooling said thus filtered material at a second temperature lower than said first temperature, injecting into said thus cooled material a cross-linking agent, and heating the thus obtained mixture at a third temperature higher than said second temperature and extruding said mixture.
Claim 12
Dependent Claim 21 words
The method of claim 9, wherein said first temperature is about 200° C. and said second temperature being about 150° C.
Claim 13
Dependent Claim 17 words
The method of claim 10, wherein said third temperature is between about 200° and about 230° C.

References Cited (Backward Citations)

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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1983-11-18 1984-05-19 1984-11-18 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1987-11-18 1988-05-19 1988-11-18 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1991-11-18 1992-05-19 1992-11-18 $7700.00 Window Closed / Lapsed

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