Claims Analysis
Total Claims: 10
Claim 1
Independent Claim
216 words
A process for regenerating spent oils, characterized by comprising the steps of: (a) Heating the oil in a first oven, (b) Sending the heated oil to a pre-distillation column and separating at the column head the water and the light hydrocarbons, (c) Recovering from the bottom of the pre-distillation column the oil which is sent to a solvent-extraction section to remove from the oil the major fraction of the impurities contained therein, (d) Heating the oil raffinate exiting the extraction section after having stripped the solvent therefrom in a second oven, (e) Feeding the oil from the heating stage to a stage of distillation under vacuum with a bottom temperature higher than 300° C., to separate from the column side the lubricating bases having the lower viscosity and deprived of impurities and discharging from the bottom the heavier lubricating bases in which the remaining impurities have been concentrated, (f) Subjecting the heavier lubricating fraction to a heat treatment at a temperature from 300° C. to 450° C. under adiabatic conditions for a time varying from 1 to 120 minutes, (g) Subjecting the heavier lubricating fraction, after the heat treatment, to a second extraction with solvent, and (h) Sending the heavy lubricating base raffinate and the other bases having a lower viscosity, separately, to a hydrofinishing stage.
Claim 2
Dependent Claim
216 words
A process for regenerating spent oils, characterized by comprising the steps of: (a) Heating the oil in a first oven, (b) Sending the heated oil to a pre-distillation column and separating at the column head the water and the light hydrocarbons, (c) Recovering from the bottom of the pre-distillation column the oil which is sent to a solvent-extraction section to remove from the oil the major fraction of the impurities contained therein, (d) Heating the oil raffinate exiting the extraction section after having stripped the solvent therefrom in a second oven, (e) Feeding the oil from the heating stage to a stage of distillation under vacuum with a bottom temperature higher than 300° C., to separate from the column side the lubricating bases having the lower viscosity and deprived of impurities and discharging from the bottom the heavier lubricating bases in which the remaining impurities have been concentrated, (f) Subjecting the heavier lubricating fraction to a heat treatment at a temperature from 300° C. to 450° C. under adiabatic conditions for a time varying from 1 to 120 minutes, (g) Subjecting the heavier lubricating fraction, after the heat treatment, to a second extraction with solvent, and (h) Sending the heavy lubricating base raffinate and the other bases having a lower viscosity, separately, to a hydrofinishing stage.
Claim 3
Dependent Claim
22 words
A process according to claim 1, wherein the solvent used in the extraction section is normal paraffin having a low molecular weight.
Claim 4
Dependent Claim
44 words
A process according to claim 1, wherein the solvent-extraction of the whole oil and of the heavier lubricating base takes place alternatingly in the same extraction section and, in such a case, the storage tanks necessary for this kind of process must be provided.
Claim 5
Dependent Claim
27 words
A process according to claim 1, characterized in that the oil in the first oven is heated to a temperature comprised between 180° C. and 230° C.
Claim 6
Dependent Claim
35 words
A process according to claim 1, wherein the residue coming from the solvent-extraction stage of the heavier lubricating base is recycled as a charge to the extraction column together with the whole oil upon predistillation.
Claim 7
Dependent Claim
30 words
A process according to claim 1, wherein the solvent extraction section operates at a temperature comprised between 30° C. and the critical temperature of the normal paraffin which is employed.
Claim 8
Dependent Claim
24 words
A process according to claim 1, wherein the extraction section operates under a pressure comprised between 25 kg/cm 2 and 50 kg/cm 2 .
Claim 9
Dependent Claim
36 words
A process according to claim 1, wherein the extraction of the oil coming from the predistillation stage is carried out with volume ratios of the normal paraffin per volume of oil of from 3 to 10.
Claim 10
Dependent Claim
33 words
A process according to claim 1, wherein the extraction of the heavier lubricating base is carried out with volume ratios of the normal paraffin per volume of oil variable from 5 to 20.