US4229281A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Process for extracting bitumen from tar sands
Assignee: Phillips Petroleum Co
•
Filing: 1978-08-14
•
Granted: 1980-10-21
•
Expires: 1998-08-14
Abstract
Abstract Bitumen is recovered from tar sand by extraction with a solvent. The bitumen solution is washed with water containing a cationic surfactant in order to remove sand fines therefrom.
Inventors
- 👤 Henry E. Alquist
- 👤 Allen M. Ammerman
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-30 11:31
CPC Classifications
C; C10; C10C; C10C3/00; C10C3/007; C10G; C10G1/00; C10G1/04; C10G1/045; C10G1/047
Claims Analysis
Total Claims: 9
Claim 1
Independent Claim
72 words
A process for recovering bitumen from tar sands wherein bitumen is extracted from the tar sands with a solvent which process comprises contacting the bitumen solution comprising said solvent, bitumen and sand fines with water containing about 0.01 to about 0.10 weight percent of a cationic surfactant to effect the removal of said sand fines from said bitumen solution, recovering the resulting bitumen solution thereafter and recovering bitumen from said bitumen solution.
Claim 2
Dependent Claim
72 words
A process for recovering bitumen from tar sands wherein bitumen is extracted from the tar sands with a solvent which process comprises contacting the bitumen solution comprising said solvent, bitumen and sand fines with water containing about 0.01 to about 0.10 weight percent of a cationic surfactant to effect the removal of said sand fines from said bitumen solution, recovering the resulting bitumen solution thereafter and recovering bitumen from said bitumen solution.
Claim 3
Dependent Claim
22 words
A process in accordance with claim 1 wherein said cationic surfactant comprises 80 percent methyldodecylbenzyl trimethylammonium chloride and 20 percent methyldodecylxylylene-bis-(trimethylammonium chloride).
Claim 4
Dependent Claim
15 words
A process in accordance with claim 1 wherein said solvent is an aromatic hydrocarbon solvent.
Claim 5
Dependent Claim
119 words
A process for recovering bitumen from tar sands comprising the steps of: (a) mixing the tar sands with an extractive solvent, (b) allowing the mixture of step (a) to settle into a fine sand-bitumen solvent phase and a coarse sand phase, (c) removing the fine sand-bitumen solvent phase, (d) contacting said fine sand-bitumen solvent phase with water containing a cationic surfactant wherein the amount of said cationic surfactant present in the water is the range of about 0.01 to about 0.10 weight percent and allowing the mixture to settle into a solvent phase, an interface zone where the fines collect, and an aqueous phase, and (e) removing the solvent phase and separating said phase into solvent and bitumen product.
Claim 6
Dependent Claim
119 words
A process for recovering bitumen from tar sands comprising the steps of: (a) mixing the tar sands with an extractive solvent, (b) allowing the mixture of step (a) to settle into a fine sand-bitumen solvent phase and a coarse sand phase, (c) removing the fine sand-bitumen solvent phase, (d) contacting said fine sand-bitumen solvent phase with water containing a cationic surfactant wherein the amount of said cationic surfactant present in the water is the range of about 0.01 to about 0.10 weight percent and allowing the mixture to settle into a solvent phase, an interface zone where the fines collect, and an aqueous phase, and (e) removing the solvent phase and separating said phase into solvent and bitumen product.
Claim 7
Dependent Claim
43 words
A process in accordance with claim 4 which further comprises diluting the solvent phase to be separated into solvent and bitumen product prior to said separation with a high boiling solvent in order to reduce the viscosity of the bitumen during solvent recovery.
Claim 8
Dependent Claim
15 words
A process in accordance with claim 4 wherein said solvent is an aromatic hydrocarbon solvent.
Claim 9
Dependent Claim
29 words
A process in accordance with claim 6 wherein said aromatic hydrocarbon solvent is toluene and the cationic surfactant comprises 80 percent methyldodecylbenzyl trimethylammonium chloride and 20 percent methyldodecylxylene-bis-(trimethylammonium chloride).
References Cited (Backward Citations)
US2825677A
Cited
US3117922A
Cited
US3330757A
Cited
US3422000A
Cited
US3459653A
Cited
US3547803A
Cited
US4017377A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1983-10-21 | 1984-04-21 | 1984-10-21 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1987-10-21 | 1988-04-21 | 1988-10-21 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1991-10-21 | 1992-04-21 | 1992-10-21 | $7700.00 | Window Closed / Lapsed |