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US4229210A Expired / Lapsed US ⏱️ 0.0 years remaining

Method for the preparation of thixotropic slurries

Assignee: Olin Corp
•
Filing: 1977-12-12
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Granted: 1980-10-21
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Expires: 1997-12-12
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Abstract

Abstract The invention relates to an improved method for the preparation and delivery of semi-solid thixotropic metal slurries for use in metal forming processes such as the rheocast and thixocast processes. The method includes inducing turbulent motion within the metal during solidification by electromagnetic or electrodynamic techniques under controlled temperature conditions so as to produce a highly fluid semi-solid slurry with a degenerate dendritic structure comprising solid spheroids dispersed in liquid. In the method of the preferred embodiment of the present invention, flow of the thixotropic metal slurry from the vibrating chamber is controlled by electromagnetic techniques and may be continuous or semi-continuous.

Inventors

  • 👤 Joseph Winter
  • 👤 Derek E. Tyler
  • 👤 Michael J. Pryor

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-01 04:26
CPC Classifications
B; B01; B01F; B01F23/00; B01F33/00; B01F33/45; B01F33/451; C; C22; C22C; C22C1/00; C22C1/12; Y; Y10; Y10S; Y10S164/00; Y10S164/90

Claims Analysis

Total Claims: 7
Claim 1
Independent Claim 200 words
A process for producing a thixotropic metal or alloy composition containing discrete degenerate dendritic primary solid particles homogeneously suspended in a secondary phase having a lower melting point than said primary solid particles which comprises the steps of: (1) heating a metal or alloy to produce at least a partially liquid mixture comprising between 20 and 80% volume fraction primary solid particles; (2) supplying a current in the range of 500 to 10,000 amps to an AC induction coil at a frequency in the range of from 60 to 10,000 cps to form an induced electromagnetic force field of sufficient intensity to vigorously agitate said partially liquid mixture; (3) placing said partially liquid mixture within said induced electromagnetic force field; (4) holding said partially liquid mixture within said induced electromagnetic force field for sufficient duration to vigorously agitate said partially liquid mixture so as to convert said primay solid particles to discrete degenerate dendrites of substantially spheroidal configuration; and (5) simultaneously cooling said partially liquid mixture during said holding step at a cooling rate determined so as to counteract the heating effect of the induced current of said electromagnetic force field and maintain said volume fraction of primary solid particles.
Claim 2
Dependent Claim 200 words
A process for producing a thixotropic metal or alloy composition containing discrete degenerate dendritic primary solid particles homogeneously suspended in a secondary phase having a lower melting point than said primary solid particles which comprises the steps of: (1) heating a metal or alloy to produce at least a partially liquid mixture comprising between 20 and 80% volume fraction primary solid particles; (2) supplying a current in the range of 500 to 10,000 amps to an AC induction coil at a frequency in the range of from 60 to 10,000 cps to form an induced electromagnetic force field of sufficient intensity to vigorously agitate said partially liquid mixture; (3) placing said partially liquid mixture within said induced electromagnetic force field; (4) holding said partially liquid mixture within said induced electromagnetic force field for sufficient duration to vigorously agitate said partially liquid mixture so as to convert said primay solid particles to discrete degenerate dendrites of substantially spheroidal configuration; and (5) simultaneously cooling said partially liquid mixture during said holding step at a cooling rate determined so as to counteract the heating effect of the induced current of said electromagnetic force field and maintain said volume fraction of primary solid particles.
Claim 3
Dependent Claim 26 words
A process according to claim 1 wherein said metal is heated above its liquidus temperature and thereafter cooled to produce said at least partially liquid mixture.
Claim 4
Dependent Claim 25 words
A process according to claim 1 wherein said metal is heated to a temperature below its liquidus to produce said at least partially liquid mixture.
Claim 5
Dependent Claim 33 words
A process according to claim 1 wherein said step of holding said partially liquid mixture within said induced electromagnetic force field is carried out by utilizing a second distinct induced electromagnetic force field.
Claim 6
Dependent Claim 33 words
A process according to claim 4 wherein said second electromagnetic induced field is of sufficient force to prevent flow of said at least partially liquid mixture from within said first electromagnetic induced field.
Claim 7
Dependent Claim 47 words
A process according to claim 4 wherein said second electromagnetic induced field is of sufficient force to provide continuous flow of said at least partially liquid mixture from within said first electromagnetic induced field at a rate sufficient to produce said discrete degenerate dendritic primary solid particles.

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1983-10-21 1984-04-21 1984-10-21 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1987-10-21 1988-04-21 1988-10-21 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1991-10-21 1992-04-21 1992-10-21 $7700.00 Window Closed / Lapsed

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