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US4222978A Expired / Lapsed US ⏱️ 0.0 years remaining

Method for producing polycrystalline translucent alumina having an excellent in-line transmission

Assignee: NGK Insulators Ltd
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Filing: 1979-05-14
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Granted: 1980-09-16
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Expires: 1999-05-14
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Abstract

Abstract Polycrystalline translucent alumina having an average grain size of alumina crystal grain being not smaller than 20μ and an average surface roughness of the fired body being not larger than 1/10 of the maximum grain size of alumina crystal grain and capable of being used for an envelope of a high pressure vapor discharge lamp, which is produced by shaping alumina composition powders consisting mainly of alumina into a given shape, primarily firing the shaped body under vacuum or in an atmosphere of hydrogen gas or dissociated ammonia gas at a temperature within 1,500° C. and then secondarily firing the primarily fired body at a temperature of 1,650°-1,900° C., at least the temperature from 1,400° C. to 1,700° C. being raised at a rate of not lower than 200° C./hr.

Inventors

  • 👤 Isao Oda
  • 👤 Koichiro Maekawa

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-28 19:28
CPC Classifications
C; C04; C04B; C04B35/00; C04B35/01; C04B35/10; C04B35/111; C04B35/115; H; H01; H01J; H01J61/00; H01J61/02; H01J61/30; H01J61/302; Y; Y10; Y10S; Y10S264/00; Y10S264/91

Claims Analysis

Total Claims: 3
Claim 1
Independent Claim 108 words
A method for producing a polycrystalline translucent alumina envelope for a high pressure vapor discharge lamp, which comprises shaping compounded alumina powders having a grain size not larger than 1μ and a purity of more than 99.5% into a given shape, primarily firing the shaped body under vacuum or in an atmosphere of hydrogen gas or dissociated ammonia gas at a temperature within the range 1,300°-1,500° C. and then secondarily firing the primarily fired body at a temperature of 1,650°-1,900° C., for a period of 1-15 hours at least the temperature from 1,400° C. to 1,700° C. being raised at a rate of not lower than 200° C./hr.
Claim 2
Independent Claim 108 words
A method for producing a polycrystalline translucent alumina envelope for a high pressure vapor discharge lamp, which comprises shaping compounded alumina powders having a grain size not larger than 1μ and a purity of more than 99.5% into a given shape, primarily firing the shaped body under vacuum or in an atmosphere of hydrogen gas or dissociated ammonia gas at a temperature within the range 1,300°-1,500° C. and then secondarily firing the primarily fired body at a temperature of 1,650°-1,900° C., for a period of 1-15 hours at least the temperature from 1,400° C. to 1,700° C. being raised at a rate of not lower than 200° C./hr.
Claim 3
Dependent Claim 56 words
The method as claimed in claim 1, wherein the compounded powders are prepared by adding 0.01-0.2% by weight of MgO, 0.01-0.2% by weight of La 2 O 3 and 0.01-0.2% by weight of Y 2 O 3 to alumina powders having a grain size of not larger than 1μ and a purity of more than 99.5%.

References Cited (Backward Citations)

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USRE27083E Cited
US3792142A Cited
US4031177A Cited
US3834915A Cited
GB1443741A Cited
US3935495A Cited
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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1983-09-16 1984-03-17 1984-09-16 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1987-09-16 1988-03-17 1988-09-16 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1991-09-16 1992-03-17 1992-09-16 $7700.00 Window Closed / Lapsed

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