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US4195524A Expired / Lapsed US ⏱️ 0.0 years remaining

Method and apparatus for collecting and storing environmental gases

Assignee: Sumitomo SHI Cryogenics of America Inc
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Filing: 1978-10-31
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Granted: 1980-04-01
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Expires: 1998-10-31
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Abstract

Abstract A method and apparatus to collect and store a sample of an environmental gas, e.g. air. A sample container or bottle is cooled below the condensation temperature of the environmental gas so that a partial vacuum is created in the container thus permitting environmental gas to be drawn into the bottle and condensed. Included in the apparatus are means to meter the quantity of environmental gas admitted to the bottle.

Inventors

  • 👤 Robert G. Hansen

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-01 22:22
CPC Classifications
G; G01; G01N; G01N1/00; G01N1/02; G01N1/22; G01N1/24

Claims Analysis

Total Claims: 13
Claim 1
Independent Claim 92 words
A method of collecting and storing a sample of an environmental gas, e.g. air, comprising the steps of: providing a sample bottle having a metering orifice for admitting the environmental gases; cooling said sample bottle below the temperature at which said environmental gas condenses to create a partial vacuum in said sample bottle thus drawing said environmental gas into said bottle; maintaining said temperature of said bottle to prevent evaporation or freezing of said collected sample; and continuing collection of said sample at a constant rate until the desired sample is obtained.
Claim 2
Independent Claim 92 words
A method of collecting and storing a sample of an environmental gas, e.g. air, comprising the steps of: providing a sample bottle having a metering orifice for admitting the environmental gases; cooling said sample bottle below the temperature at which said environmental gas condenses to create a partial vacuum in said sample bottle thus drawing said environmental gas into said bottle; maintaining said temperature of said bottle to prevent evaporation or freezing of said collected sample; and continuing collection of said sample at a constant rate until the desired sample is obtained.
Claim 3
Dependent Claim 11 words
A method according to claim 1 wherein said gas is air.
Claim 4
Dependent Claim 28 words
A method according to claim 2 wherein said bottle is cooled to and maintained at a temperature of less than 73 degrees Kelvin and above 65 degrees Kelvin.
Claim 5
Dependent Claim 35 words
A method according to claim 1 wherein said bottle is maintained at a temperature less than the saturation temperature corresponding to the critical pressure, but greater than the freezing temperature of the gas being sampled.
Claim 6
Dependent Claim 15 words
A method according to claim 1 wherein said collection continues until said bottle is full.
Claim 7
Independent Claim 90 words
An apparatus for collecting and storing a sample of environmental gas comprising in combination: a sample bottle or container having means for admitting and discharging a quantity of environmental gas; means to meter the quantity of environmental gas admitted to said sample bottle; and means to cool said sample bottle below the temperature at which said environmental gas condenses; whereby when said sample bottle is cooled below said condensation temperature a partial vacuum is created in said bottle thus permitting environmental gas to be drawn into said bottle and condensed.
Claim 8
Independent Claim 90 words
An apparatus for collecting and storing a sample of environmental gas comprising in combination: a sample bottle or container having means for admitting and discharging a quantity of environmental gas; means to meter the quantity of environmental gas admitted to said sample bottle; and means to cool said sample bottle below the temperature at which said environmental gas condenses; whereby when said sample bottle is cooled below said condensation temperature a partial vacuum is created in said bottle thus permitting environmental gas to be drawn into said bottle and condensed.
Claim 9
Dependent Claim 17 words
An apparatus according to claim 6 wherein said sample bottle is constructed from a lightweight structural metal.
Claim 10
Dependent Claim 24 words
An apparatus according to claim 6 including separate inlet and outlet conduits, said inlet conduit including a gas metering orifice at its inlet end.
Claim 11
Dependent Claim 24 words
An apparatus according to claim 6 wherein said means to cool said sample bottle includes a cryogenic refrigerator removably connected to said sample bottle.
Claim 12
Dependent Claim 22 words
An apparatus according to claim 6 wherein said sample bottle and a portion of said cooling means are surrounded by insulating means.
Claim 13
Dependent Claim 14 words
An apparatus according to claim 10 wherein said insulation is a lightweight synthetic foam.

References Cited (Backward Citations)

GB1113875A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1983-04-01 1983-10-01 1984-04-01 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1987-04-01 1987-10-01 1988-04-01 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1991-04-01 1991-10-01 1992-04-01 $7700.00 Window Closed / Lapsed

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