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US4194996A Expired / Lapsed US ⏱️ 0.0 years remaining

Phenol formaldehyde compression moulding composition comprising phenol formaldehyde-wood filler

Assignee: Uralsky Lesotekhnichesky Institut
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Filing: 1978-10-10
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Granted: 1980-03-25
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Expires: 1998-10-10
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Abstract

Abstract A compression-molding composition contains a phenol-formaldehyde resin, a filler, a curing agent, viz. hexamethylenetetramine, a curing accelerator such as calcium oxide or magnesium oxide, and a lubricant such as stearin or stearates. The filler comprises a product resulting from the treatment of crushed wood with an aqueous solution of phenol and formaldehyde at the boiling temperature of said solution in the presence of hydrochloric acid at a weight ratio between phenol, formaldehyde, water, hydrochloric acid, crushed wood equal to 0.15-0.80:0.045-0.864:6-15:0.0435-0.1086:1 respectively. Proportions of the components are as follows, parts by weight: -phenol-formaldehyde resin 15 to 45 -filler 47.5 to 75 -curing agent 7 to 9 -curing accelerator 0.5 to 1 -lubricant 0.6 to 0.9 - The compression-molding composition according to the present invention has an increased water-resistance (17 to 19 mg), heat-resistance (up to 182 DEG C.) along with other properties satisfying the requirements of modern standards. This enlarges the field of application of the compression-molding composition of this invention as compared to the prior art phenolic compression-molding compositions.

Inventors

  • 👤 Margarita D. Babina
  • 👤 Evgeny S. Dunjushkin
  • 👤 Galina I. Popova
  • 👤 Anatoly D. Sokolov
  • 👤 Jury M. Smirnov

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-04 19:34
CPC Classifications
C; C08; C08L; C08L61/00; C08L61/04; C08L61/06; C08G; C08G8/00; C08G8/04; C08G8/08; C08G8/10; C08L97/00; C08L97/02

Claims Analysis

Total Claims: 6
Claim 1
Independent Claim 122 words
A compression-moulding composition containing 15 to 45 parts by weight of a phenol-formaldehyde resin, 47.5 to 75 parts by weight of a filler comprising a product of the treatment of crushed wood with an aqueous solution of phenol and formaldehyde at the boiling temperature of said solution in the presence of hydrochloric acid at a weight ratio between phenol, formaldehyde, water, hydrochloric acid and crushed wood equal to 0.15-0.80:0.045-0.864:6-15:0.0435-0.1086:1 respectively, 7 to 9 parts by weight of a curing agent, i.e. hexamethylenetetramine, 0.5 to 1 part by weight of a curing accelerator selected from the group consisting of calcium oxide and magnesium oxide and 0.6 to 0.9 part by weight of a lubricant selected from the group consisting of stearin and stearates.
Claim 2
Dependent Claim 122 words
A compression-moulding composition containing 15 to 45 parts by weight of a phenol-formaldehyde resin, 47.5 to 75 parts by weight of a filler comprising a product of the treatment of crushed wood with an aqueous solution of phenol and formaldehyde at the boiling temperature of said solution in the presence of hydrochloric acid at a weight ratio between phenol, formaldehyde, water, hydrochloric acid and crushed wood equal to 0.15-0.80:0.045-0.864:6-15:0.0435-0.1086:1 respectively, 7 to 9 parts by weight of a curing agent, i.e. hexamethylenetetramine, 0.5 to 1 part by weight of a curing accelerator selected from the group consisting of calcium oxide and magnesium oxide and 0.6 to 0.9 part by weight of a lubricant selected from the group consisting of stearin and stearates.
Claim 3
Dependent Claim 24 words
A compression-moulding composition as claimed in claim 1, wherein a dye is present in an amount of from 1.1 to 1.5 part by weight.
Claim 4
Dependent Claim 15 words
A compression-moulding composition as claimed in claim 2, wherein nigrosine is used as the dye.
Claim 5
Dependent Claim 24 words
A compression-moulding composition as claimed in claim 1, wherein china clay is contained in an amount of from 3 to 4 parts by weight.
Claim 6
Dependent Claim 24 words
A compression-moulding composition as claimed in claim 2, wherein china clay is contained in an amount of from 3 to 4 parts by weight.

References Cited (Backward Citations)

DE1569463A1 Cited
GB1430343A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1983-03-25 1983-09-24 1984-03-25 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1987-03-25 1987-09-24 1988-03-25 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1991-03-25 1991-09-24 1992-03-25 $7700.00 Window Closed / Lapsed

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