US4181747A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Processed vegetable seed fiber for food products
Assignee: Staley Continental Inc
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Filing: 1978-12-04
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Granted: 1980-01-01
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Expires: 1998-12-04
Abstract
Abstract A processed vegetable seed fiber, particularly corn and soybean fiber, for use in food products is disclosed. Processing is accomplished by heating an aqueous slurry of the crude vegetable seed fiber to about 155 DEG -180 DEG F., and then maintaining the pH of the heated slurry in the range of about 2.5 to 5.0. The elevated temperature of the slurry is maintained for up to about 15 to 60 minutes while the slurry is agitated. The resulting acid-pasteurized slurry is then dewatered to obtain a fiber material at about 20-30% dry solids. Fresh water is then added to the dewatered fiber material to reslurry it to about 3-4% dry solids. The reslurried fiber material is agitated at a temperature up to about 140 DEG F. for about fifteen to thirty minutes, dewatered a second time, and then dried to about 10% moisture.
Inventors
- 👤 Hunter L. Kickle
- 👤 William J. Ball, Jr.
- 👤 Robert Von Schanefelt
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-24 22:55
CPC Classifications
A; A21; A21D; A21D2/00; A21D2/08; A21D2/36; A23; A23L; A23L33/00; A23L33/20; A23L33/21; A23L7/00; A23L7/10; A23L7/115
Claims Analysis
Total Claims: 21
Claim 1
Independent Claim
108 words
In a method of making pasteurized food fiber from crude fiber-containing vegetable seed hulls, the steps comprising: (a) mixing water and said vegetable hulls to form an aqueous slurry; (b) maintaining the pH of said aqueous slurry in the range of 2.5-5.0; (c) heating said slurry to a temperature of about 155° F.-180° F. for 15-60 minutes to acid-pasteurize said seed hulls; (d) dewatering said aqueous slurry of seed hulls; (e) washing said dewatered seed hulls with fresh water to further refine said seed hulls; (f) dewatering the washed seed hulls; and (g) drying said dewatered seed hulls to obtain refined, acid-pasteurized vegetable fiber suitable for human consumption.
Claim 2
Dependent Claim
108 words
In a method of making pasteurized food fiber from crude fiber-containing vegetable seed hulls, the steps comprising: (a) mixing water and said vegetable hulls to form an aqueous slurry; (b) maintaining the pH of said aqueous slurry in the range of 2.5-5.0; (c) heating said slurry to a temperature of about 155° F.-180° F. for 15-60 minutes to acid-pasteurize said seed hulls; (d) dewatering said aqueous slurry of seed hulls; (e) washing said dewatered seed hulls with fresh water to further refine said seed hulls; (f) dewatering the washed seed hulls; and (g) drying said dewatered seed hulls to obtain refined, acid-pasteurized vegetable fiber suitable for human consumption.
Claim 3
Dependent Claim
143 words
In a method of making pasteurized, light-colored food fiber from crude fiber-containing vegetable seed hulls having dark-colored hilums, the steps comprising: (a) mixing water and said vegetable seed hulls to form an aqueous slurry; (b) adjusting the pH of said aqueous slurry to 2.5-5.0; (c) heating said slurry to a temperature of about 155° F.-180+ F. for 15-60 minutes to acid-pasteurize said seed hulls and substantially lighten the dark-colored hilums of said seed hulls; (d) dewatering said aqueous slurry of seed hulls; (e) washing said dewatered seed hulls with fresh water to increase the fiber content of the seed hulls by decreasing the content of non-fiber materials therein; (f) dewatering the washed seed hulls; and (g) drying said dewatered seed hulls to obtain an acid-pasteurized vegetable fiber suitable for human consumption which is lighter in overall color than the crude fiber-containing seed hulls.
Claim 4
Dependent Claim
143 words
In a method of making pasteurized, light-colored food fiber from crude fiber-containing vegetable seed hulls having dark-colored hilums, the steps comprising: (a) mixing water and said vegetable seed hulls to form an aqueous slurry; (b) adjusting the pH of said aqueous slurry to 2.5-5.0; (c) heating said slurry to a temperature of about 155° F.-180+ F. for 15-60 minutes to acid-pasteurize said seed hulls and substantially lighten the dark-colored hilums of said seed hulls; (d) dewatering said aqueous slurry of seed hulls; (e) washing said dewatered seed hulls with fresh water to increase the fiber content of the seed hulls by decreasing the content of non-fiber materials therein; (f) dewatering the washed seed hulls; and (g) drying said dewatered seed hulls to obtain an acid-pasteurized vegetable fiber suitable for human consumption which is lighter in overall color than the crude fiber-containing seed hulls.
Claim 5
Dependent Claim
133 words
In a method of pasteurizing soybean hulls having dark-colored seed hilums, the steps comprising: (a) preparing an aqueous slurry containing about 3-10% dry solids of soybean hulls; (b) maintaining said slurry at a pH in the range of 2.5-5.0 and at a temperature of about 155° F.-180° F. for 15-60 minutes to acid-pasteurize said soybean hulls, and to change the seed hilums of said soybean hulls from dark-colored to light-colored; (c) dewatering said slurry of soybean hulls; (d) washing said dewatered soybean hulls with fresh water to increase the fiber content of the seed hulls by decreasing the content of non-fiber materials therein; (e) dewatering the washed soybean hulls; and (f) drying said dewatered soybean hulls to obtain light-colored pasteurized soybean hulls having a total bacteria standard plate count less than 50,000 max./gram.
Claim 6
Dependent Claim
133 words
In a method of pasteurizing soybean hulls having dark-colored seed hilums, the steps comprising: (a) preparing an aqueous slurry containing about 3-10% dry solids of soybean hulls; (b) maintaining said slurry at a pH in the range of 2.5-5.0 and at a temperature of about 155° F.-180° F. for 15-60 minutes to acid-pasteurize said soybean hulls, and to change the seed hilums of said soybean hulls from dark-colored to light-colored; (c) dewatering said slurry of soybean hulls; (d) washing said dewatered soybean hulls with fresh water to increase the fiber content of the seed hulls by decreasing the content of non-fiber materials therein; (e) dewatering the washed soybean hulls; and (f) drying said dewatered soybean hulls to obtain light-colored pasteurized soybean hulls having a total bacteria standard plate count less than 50,000 max./gram.
Claim 7
Dependent Claim
76 words
A substantially dry, pasteurized food fiber derived from crude soybean hulls having dark-colored hilums resulting from the method of claim 3, containing no more than 2% by weight fat, less than 15% protein, and a minimum of 45% crude fiber, said food fiber material having no detectible level of Salmonella, Coliforms and coagulase positive Staphylococci bacteria, said fiber having a water-holding capacity of about 3.0 to 4.5 grams water per gram of said fiber sample tested.
Claim 8
Dependent Claim
34 words
The method of claim 1, in which the seed hulls are selected from the group consisting of soybean hulls, corn hulls, rice hulls, wheat hulls, rye hulls, barley hulls, oat hulls and pea hulls.
Claim 9
Dependent Claim
16 words
The method of claim 2, in which the pH is adjusted to about 3.5 during heating.
Claim 10
Dependent Claim
16 words
The method of claim 3, in which the pH is maintained to about 3.5 during heating.
Claim 11
Dependent Claim
20 words
The method of claim 2, in which the heating temperature is maintained at about 160° F .-170° F. during pasteurizing.
Claim 12
Dependent Claim
24 words
The method of claim 3, in which the slurry of soybean hulls is maintained at a temperature of about 160° F.-170° F. during pasteurizing.
Claim 13
Dependent Claim
18 words
The method of claim 3, in which the pH is maintained at about 4.0-4.5 with concentrated sulfuric acid.
Claim 14
Dependent Claim
31 words
The method of claim 2, in which the pH is adjusted with an acid selected from the group consisting of hydrochloric, sulfuric, tartaric, acetic, ascorbic, citric, itaconic, phosphoric and fumaric acids.
Claim 15
Dependent Claim
44 words
The method of claim 3, in which the soybean hulls are initially slurried in water at a level of about 5-6% solids, said soybean hulls then being washed as a slurry of about 3-4% solids with added fresh water after the first dewatering step.
Claim 16
Dependent Claim
31 words
The method of claim 2, in which the washing of said dewatered seed hulls with fresh water is conducted at a temperature below 155° F. but higher than about 130° F.
Claim 17
Dependent Claim
25 words
The method of claim 3, in which the fresh water wash is conducted at a temperature of about 130° F.-155° F. for about 30 minutes.
Claim 18
Dependent Claim
12 words
The acid-pasteurized, light-colored soybean hulls resulting from the method of claim 14.
Claim 19
Dependent Claim
31 words
The method of claim 1, in which the crude fiber containing vegetable seed hulls comprise corn bran, and the pH of the aqueous slurry is maintained in the range of 3.5-5.0.
Claim 20
Dependent Claim
24 words
The method of claim 16, in which the solids level of said aqueous slurry of corn bran is in the range of about 2.5-10%.
Claim 21
Dependent Claim
14 words
The method of claim 1, in which the vegetable seed hulls comprise corn bran.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1982-12-31 | 1983-07-02 | 1984-01-01 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1986-12-31 | 1987-07-02 | 1988-01-01 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1990-12-31 | 1991-07-02 | 1992-01-01 | $7700.00 | Window Closed / Lapsed |