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US4178161A Expired / Lapsed US ⏱️ 0.0 years remaining

Manufacture of rigidized convoluted foam from flexible polyurethane foam and resultant product

Assignee: GFC FOAM Corp A CORP OF DE
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Filing: 1978-07-26
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Granted: 1979-12-11
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Expires: 1998-07-26
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Abstract

Abstract A rigidized convoluted foam suitable as a self-standing filter is made by passing a sheet of air-permeable flexible polyurethane foam through a convoluting machine to obtain two unnested sheets of convoluted foam, each sheet being convoluted on only one side. The two sheets are nested and impregnated from the flat surface of each sheet almost to the closest valley surface with a thermosetting melamine, urea, or benzoguanamine resin in an amount to not appreciably impair the permeability of the foam and to increase the rigidity of the foam sufficiently so that each unnested sheet will be self-standing. After the resin has reacted, the nested sheets are separated.

Inventors

  • 👤 Bernard Rudner
  • 👤 David Reich
  • 👤 Edward Galica

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-27 13:04
CPC Classifications
B; B29; B29C; B29C67/00; B29C67/20; B01; B01D; B01D39/00; B01D39/14; B01D39/16; B01D39/1669; B01D39/1676; C; C08; C08J; C08J9/00; C08J9/36; C08J9/40; C08J9/42; C08J2375/00; C08J2375/04; C08J2461/00; Y; Y10; Y10S; Y10S264/00; Y10S264/48; Y10S55/00; Y10S55/13; Y10S55/42

Claims Analysis

Total Claims: 26
Claim 1
Independent Claim 228 words
A process for the manufacture of a convoluted polyurethane foam self-standing filter which comprises the steps of: (a) passing a sheet of air-permeable flexible polyurethane foam that is capable of being impregnated with a thermosetting resin, said sheet having a thickness of from about 11/4 inches to about 8 inches, through a convoluting machine whereby two unnested sheets of convoluted foam are provided, each of said sheets being convoluted on only one side; (b) nesting said two unnested sheets of convoluted foam; (c) impregnating one of said nested sheets, by means of immersion, reverse-roll coating, or gravure roll coating, from the flat surface of the sheet almost to the closest valley surface of the sheet with a thermosetting melamine, urea, or benzoguanamine resin, and a cross-linker, the combined dry weight of said thermosetting resin and said cross-linker after reaction being from about 10 percent to about 300 percent of the dry weight of said polyurethane foam and being an amount to not appreciably impair said foam permeability and to increase the rigidity of said polyurethane foam sufficiently that said unnested sheet will be self-standing; (d) reacting said thermosetting resin and said cross-linker without separating said nested sheets; (e) repeating steps (c) and (d) on the other of said nested sheets; and, (f) separating said nested sheets, thereby providing convoluted polyurethane foam which is rigid enough to be self-standing.
Claim 2
Dependent Claim 228 words
A process for the manufacture of a convoluted polyurethane foam self-standing filter which comprises the steps of: (a) passing a sheet of air-permeable flexible polyurethane foam that is capable of being impregnated with a thermosetting resin, said sheet having a thickness of from about 11/4 inches to about 8 inches, through a convoluting machine whereby two unnested sheets of convoluted foam are provided, each of said sheets being convoluted on only one side; (b) nesting said two unnested sheets of convoluted foam; (c) impregnating one of said nested sheets, by means of immersion, reverse-roll coating, or gravure roll coating, from the flat surface of the sheet almost to the closest valley surface of the sheet with a thermosetting melamine, urea, or benzoguanamine resin, and a cross-linker, the combined dry weight of said thermosetting resin and said cross-linker after reaction being from about 10 percent to about 300 percent of the dry weight of said polyurethane foam and being an amount to not appreciably impair said foam permeability and to increase the rigidity of said polyurethane foam sufficiently that said unnested sheet will be self-standing; (d) reacting said thermosetting resin and said cross-linker without separating said nested sheets; (e) repeating steps (c) and (d) on the other of said nested sheets; and, (f) separating said nested sheets, thereby providing convoluted polyurethane foam which is rigid enough to be self-standing.
Claim 3
Dependent Claim 51 words
The process of claim 1 wherein the melamine resin conforms to the generic formula ##STR8## wherein A,B,D,E,F and G are hydrogen, with the proviso that at least one of A,B,D,E,F and G is ##STR9## wherein R and R' are hydrogen or an alkyl radical containing from one to four carbon atoms.
Claim 4
Dependent Claim 13 words
The process of claim 2 wherein the melamine resin is tri(methoxymethyl) trimethylol melamine.
Claim 5
Dependent Claim 11 words
The process of claim 2 wherein the melamine resin is tris-(methoxymethyl)-melamine.
Claim 6
Dependent Claim 13 words
The process of claim 1 wherein the cross-linker is an ethylene-acrylic acid copolymer.
Claim 7
Dependent Claim 13 words
The process of claim 1 wherein the cross-linker is a butene-maleic anhydride copolymer.
Claim 8
Dependent Claim 53 words
The process of claim 1 wherein the urea resin conforms to the generic formula ##STR10## wherein one of L and M are hydrogen, with the proviso that at least one of L and M is ##STR11## wherein R and R' are hydrogen or an alkyl radical containing from one to four carbon atoms.
Claim 9
Dependent Claim 13 words
The process of claim 7 wherein the urea resin is a urea-formaldehyde resin.
Claim 10
Dependent Claim 13 words
The process of claim 1 wherein the urea resin is a glyoxal-urea-formaldehyde resin.
Claim 11
Dependent Claim 50 words
The process of claim 1 wherein the benzoguanamine resin conforms to the generic formula ##STR12## wherein A,B,G and F are hydrogen, with the proviso that at least one of A,B,G and F is ##STR13## wherein R and R' are hydrogen or an alkyl radical from one to four carbon atoms.
Claim 12
Dependent Claim 13 words
The process of claim 10 wherein the benzoguanamine resin is a benzoguanamine-formaldehyde-methanol resin.
Claim 13
Dependent Claim 8 words
The product of the process of claim 1.
Claim 14
Dependent Claim 210 words
A process for the manufacture of a convoluted polyurethane foam self-standing filter which comprises the steps of: (a) passing a sheet of air-permeable flexible polyurethane foam that is capable of being impregnated with a thermosetting resin, said sheet having a thickness of from about 11/4 inches to about 8 inches, through a convoluting machine whereby two unnested sheets of convoluted foam are provided, each of said sheets being convoluted on only one side, (b) nesting said two unnested sheets of convoluted foam; (c) impregnating each of said nested sheets, by means of immersion, reverse-roll coating, or gravure roll coating, from the flat surface of the sheet almost to the closest valley surface of the sheet with a thermosetting melamine, urea, or benzoguanamine resin, and a cross-linker, the combined dry weight of said thermosetting resin and said cross-linker after reaction being from about 10 percent to about 300 percent of the dry weight of said polyurethane foam and being an amount to not appreciably impair said foam permeability and to increase the rigidity of said polyurethane foam sufficiently that each unnested sheet will be self-standing; (d) reacting said thermosetting resin and said cross-linker; and (e) separating said nested sheets, thereby providing convoluted polyurethane foam which is rigid enough to be self-standing.
Claim 15
Dependent Claim 210 words
A process for the manufacture of a convoluted polyurethane foam self-standing filter which comprises the steps of: (a) passing a sheet of air-permeable flexible polyurethane foam that is capable of being impregnated with a thermosetting resin, said sheet having a thickness of from about 11/4 inches to about 8 inches, through a convoluting machine whereby two unnested sheets of convoluted foam are provided, each of said sheets being convoluted on only one side, (b) nesting said two unnested sheets of convoluted foam; (c) impregnating each of said nested sheets, by means of immersion, reverse-roll coating, or gravure roll coating, from the flat surface of the sheet almost to the closest valley surface of the sheet with a thermosetting melamine, urea, or benzoguanamine resin, and a cross-linker, the combined dry weight of said thermosetting resin and said cross-linker after reaction being from about 10 percent to about 300 percent of the dry weight of said polyurethane foam and being an amount to not appreciably impair said foam permeability and to increase the rigidity of said polyurethane foam sufficiently that each unnested sheet will be self-standing; (d) reacting said thermosetting resin and said cross-linker; and (e) separating said nested sheets, thereby providing convoluted polyurethane foam which is rigid enough to be self-standing.
Claim 16
Dependent Claim 51 words
The process of claim 13 wherein the melamine resin conforms to th generic formula ##STR14## wherein A,B,D,E,F and G are hydrogen, with the proviso that at least one of A,B,D,E,F and G is ##STR15## wherein R and R' are hydrogen or an alkyl radical containing from one to four carbon atoms.
Claim 17
Dependent Claim 13 words
The process of claim 14 wherein the melamine resin is tri(methoxymethyl) trimethylol melamine.
Claim 18
Dependent Claim 11 words
The process of claim 14 wherein the melamine resin is tris-(methoxymethyl)-melamine.
Claim 19
Dependent Claim 13 words
The process of claim 13 wherein the cross-linker is an ethylene-acrylic acid copolymer.
Claim 20
Dependent Claim 13 words
The process of claim 13 wherein the cross-linker is a butene-maleic anhydride copolymer.
Claim 21
Dependent Claim 53 words
The process of claim 13 wherein the urea resin conforms to the generic formula ##STR16## wherein one of L and M are hydrogen, with the proviso that at least one of L and M is ##STR17## wherein R and R' are hydrogen or an alkyl radical containing from one to four carbon atoms.
Claim 22
Dependent Claim 13 words
The process of claim 19 wherein the urea resin is a urea-formaldehyde resin.
Claim 23
Dependent Claim 13 words
The process of claim 13 wherein the urea resin is a glyoxal-urea-formaldehyde resin.
Claim 24
Dependent Claim 50 words
The process of claim 13 wherein the benzoguanamine resin conforms to the generic formula ##STR18## wherein A,B,G and F are hydrogen, with the proviso that at least one of A,B,G and F is ##STR19## wherein R and R' are hydrogen or an alkyl radical from one to four carbon atoms.
Claim 25
Dependent Claim 13 words
The process of claim 22 wherein the benzoguanamine resin is a benzoguanamine-formaldehyde-methanol resin.
Claim 26
Dependent Claim 8 words
The product of the process of claim 13.

References Cited (Backward Citations)

CA795294A Cited
GB977929A Cited
US3269887A Cited
US3558393A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1982-12-10 1983-06-11 1983-12-11 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1986-12-10 1987-06-11 1987-12-11 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1990-12-10 1991-06-11 1991-12-11 $7700.00 Window Closed / Lapsed

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