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US4175109A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for extracting tungsten from alkali metal tungstate solutions

Assignee: GTE Sylvania Inc
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Filing: 1978-08-03
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Granted: 1979-11-20
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Expires: 1998-08-03
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Abstract

Abstract A tungsten extraction process wherein tungsten values are extracted from an aqueous alkali metal tungstate solution by an organic extractant, then stripped from the extractant is improved by using an organic solution consisting essentially of from about 6 to about 10 percent by volume an extractant that is a mixture of trialkyl amines wherein the major constituent is tri-isooctyl amine and from about 90 to about 94 percent by volume of a solvent that is a mixture of alkyl benzenes having molecular weights of either 120, 134 or 148.

Inventors

  • 👤 Tai K. Kim

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-03 07:06
CPC Classifications
C; C01; C01G; C01G41/00; C01G41/003; C22; C22B; C22B3/00; C22B3/20; C22B3/26; C22B3/28; C22B3/282; Y; Y02; Y02P; Y02P10/00; Y02P10/20; Y10; Y10S; Y10S423/00; Y10S423/09; Y10S423/14

Claims Analysis

Total Claims: 3
Claim 1
Independent Claim 154 words
In a process wherein tungsten values are extracted from an aqueous alkali metal tungstate solution containing impurities by an organic extractant solution containing an amine extractant and thereafter the tungste values are removed from the organic extractant solution by stripping with aqueous ammonia, wherein the improvement comprises providing, as an extractant, an organic extraction solution consisting essentially of from about 6 to about 10 percent by volume of a mixture of tri-alkyl amines having alkyl chains of about 6 to 10 carbon atoms with trisooctyl amine being the major component in said mixture and from about 90 to 94 percent by volume of an aromatic solvent consisting essentially of a mixture of alkyl benzenes wherein the alkyl benzenes constituting the mixture of alkyl benzenes have molecular weights of 120, 134 or 148 and the total number of carbon atoms in the alkyl chains attached to the benzene ring are either 3, 4 or 5.
Claim 2
Dependent Claim 154 words
In a process wherein tungsten values are extracted from an aqueous alkali metal tungstate solution containing impurities by an organic extractant solution containing an amine extractant and thereafter the tungste values are removed from the organic extractant solution by stripping with aqueous ammonia, wherein the improvement comprises providing, as an extractant, an organic extraction solution consisting essentially of from about 6 to about 10 percent by volume of a mixture of tri-alkyl amines having alkyl chains of about 6 to 10 carbon atoms with trisooctyl amine being the major component in said mixture and from about 90 to 94 percent by volume of an aromatic solvent consisting essentially of a mixture of alkyl benzenes wherein the alkyl benzenes constituting the mixture of alkyl benzenes have molecular weights of 120, 134 or 148 and the total number of carbon atoms in the alkyl chains attached to the benzene ring are either 3, 4 or 5.
Claim 3
Dependent Claim 19 words
An improvement according to claim 1 wherein the amine constitutes about 8 percent by volume of the extracting solution.

References Cited (Backward Citations)

US3052516A Cited
US3158438A Cited
US3804941A Cited
US3770869A Cited
SU456791A1 Cited
US4092400A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1982-11-19 1983-05-21 1983-11-20 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1986-11-19 1987-05-21 1987-11-20 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1990-11-19 1991-05-21 1991-11-20 $7700.00 Window Closed / Lapsed

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