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US4155729A Expired / Lapsed US ⏱️ 0.0 years remaining

Liquid flash between expanders in gas separation

Assignee: Phillips Petroleum Co
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Filing: 1977-10-20
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Granted: 1979-05-22
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Expires: 1997-10-20
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Abstract

Abstract In the separation of low boiling gases such as ethane and heavier from natural gas utilizing two expanders in series, liquid condensed before expansion is not passed to the fractionator but is flashed and the resulting vapor combined with the expanded vapor from the first expander. This results in both increased work output from the second expander and simplified design of the downstream fractionator column since it reduces the amount of lighter materials introduced into the lower section thereof.

Inventors

  • 👤 Michael L. Gray
  • 👤 Robert M. Bellinger

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-30 13:18
CPC Classifications
F; F25; F25J; F25J3/00; F25J3/02; F25J3/0204; F25J3/0209; F25J3/0228; F25J3/0233; F25J3/0238; F25J2200/00; F25J2200/02; F25J2200/70; F25J2205/00; F25J2205/02; F25J2205/04; F25J2235/00; F25J2235/60; F25J2240/00; F25J2240/02; F25J2270/00; F25J2270/12; F25J2270/60

Claims Analysis

Total Claims: 10
Claim 1
Independent Claim 304 words
A process comprising: (a) passing a first fluid stream to a first expander inlet separation zone; (b) withdrawing a vapor stream from an upper portion of said first expander inlet separation zone and passing said vapor stream to a first expansion zone where said vapor stream is expanded to cool said vapor stream and produce external work; (c) withdrawing a thus cooled expanded fluid stream from said first expansion zone; (d) withdrawing a liquid stream from a lower portion of said first expander inlet separation zone and passing said liquid stream into a flash separation zone operated at a lower pressure than said first expander inlet separation zone; (e) withdrawing a flashed vapor stream from an upper portion of said flash separation zone; (f) combining said expanded fluid stream of (c) and said flashed vapor stream of (e); (g) withdrawing a liquid stream from a lower portion of said flash separation zone; (h) passing said thus withdrawn liquid stream of (g) to a fractionation zone; (i) passing said combined stream of (f) to a second expander inlet separation zone; (j) withdrawing a vapor stream from an upper portion of said second expander inlet separation zone and passing said vapor stream to a second expansion zone where said vapor stream is expanded to cool said vapor stream and produce external work; (k) withdrawing a thus cooled expanded fluid stream from said second expansion zone and passing said thus cooled fluid stream to a point near an upper portion of said fractionation zone; (l) withdrawing liquid from a lower portion of said second expander inlet separation zone; (m) passing the thus withdrawn liquid of (l) to said fractionation zone; (n) withdrawing a vaporous product from an upper portion of said fractionation zone; and (o) withdrawing a liquid product from the bottom portion of said fractionation zone.
Claim 2
Dependent Claim 304 words
A process comprising: (a) passing a first fluid stream to a first expander inlet separation zone; (b) withdrawing a vapor stream from an upper portion of said first expander inlet separation zone and passing said vapor stream to a first expansion zone where said vapor stream is expanded to cool said vapor stream and produce external work; (c) withdrawing a thus cooled expanded fluid stream from said first expansion zone; (d) withdrawing a liquid stream from a lower portion of said first expander inlet separation zone and passing said liquid stream into a flash separation zone operated at a lower pressure than said first expander inlet separation zone; (e) withdrawing a flashed vapor stream from an upper portion of said flash separation zone; (f) combining said expanded fluid stream of (c) and said flashed vapor stream of (e); (g) withdrawing a liquid stream from a lower portion of said flash separation zone; (h) passing said thus withdrawn liquid stream of (g) to a fractionation zone; (i) passing said combined stream of (f) to a second expander inlet separation zone; (j) withdrawing a vapor stream from an upper portion of said second expander inlet separation zone and passing said vapor stream to a second expansion zone where said vapor stream is expanded to cool said vapor stream and produce external work; (k) withdrawing a thus cooled expanded fluid stream from said second expansion zone and passing said thus cooled fluid stream to a point near an upper portion of said fractionation zone; (l) withdrawing liquid from a lower portion of said second expander inlet separation zone; (m) passing the thus withdrawn liquid of (l) to said fractionation zone; (n) withdrawing a vaporous product from an upper portion of said fractionation zone; and (o) withdrawing a liquid product from the bottom portion of said fractionation zone.
Claim 3
Dependent Claim 12 words
A process according to claim 1 wherein said feed is natural gas.
Claim 4
Dependent Claim 19 words
A method according to claim 2 wherein said natural gas has been treated to remove acid gases and water.
Claim 5
Dependent Claim 20 words
A method according to claim 3 wherein said natural gas comprises methane and smaller amounts of higher molecular weight hydrocarbons.
Claim 6
Dependent Claim 22 words
A method according to claim 4 wherein said natural gas comprises predominantly methane with smaller amounts of ethane, propane, butanes, and nitrogen.
Claim 7
Dependent Claim 52 words
A method according to claim 1 wherein said vaporous product withdrawn from the upper portion of said fractionation zone is predominantly methane and nitrogen and said liquid product recovered from the bottom portion of said fractionation zone is ethane and higher molecular weight hydrocarbons with only a minor amount of methane present.
Claim 8
Dependent Claim 39 words
A method according to claim 6 wherein said feed is introduced at a pressure within the range of 3.45 to 6.03 MPa and said fractionation zone is operated at a pressure within the range of 0.689 to 2.4 MPa.
Claim 9
Dependent Claim 71 words
A method according to claim 1 wherein said feed comprises about 2 percent nitrogen, 71 percent methane, 15 percent ethane, 8 percent propane, 1 percent isobutane, 2 percent n-butane, and 1 percent C 5 + hydrocarbons, said feed is at a pressure of about 5 MPa, said fractionator is operated at a pressure of about 1.4 MPa, and the pressure between said first and second expansion zones is about 3 MPa.
Claim 10
Dependent Claim 25 words
A method according to claim 1 wherein said stream of (m) is introduced to said fractionation column at a point below said stream of (k).

References Cited (Backward Citations)

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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1982-05-21 1982-11-20 1983-05-22 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1986-05-21 1986-11-20 1987-05-22 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1990-05-21 1990-11-20 1991-05-22 $7700.00 Window Closed / Lapsed

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