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US4153766A Expired / Lapsed US ⏱️ 0.0 years remaining

Continuous process for the production of ethylene terephthalate polyesters

Assignee: Kanebo Ltd
•
Filing: 1976-10-26
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Granted: 1979-05-08
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Expires: 1996-10-26
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Abstract

Abstract In a continuous process for the production of ethylene terephthalate polyesters, when the control value for the viscosity which relates to the degree of the polymerization in a polymerization vessel exceeds a predetermined value, a desired command value of the viscosity at the output of the preceding polymerization vessel is automatically revised.

Inventors

  • 👤 Tohru Koide
  • 👤 Tabashi Ezawa
  • 👤 Hideki Onoda
  • 👤 Chiharu Masaki
  • 👤 Tohru Morita

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-28 13:15
CPC Classifications
B; B01; B01J; B01J19/00; B01J19/0006; C; C08; C08G; C08G63/00; C08G63/78; C08G63/785; B01J2219/00; B01J2219/00049; B01J2219/00162; B01J2219/00164

Claims Analysis

Total Claims: 5
Claim 1
Independent Claim 251 words
A continuous process for the production of ethylene terephthalate polyesters which comprises passing a polyester-forming fusion melt predominantly comprised of bis-2-hydroxethyl terephthalate and/or its low polymers sequentially through a series of reduced pressure polymerization vessles while controlling the degree of polymerization of the product by a controlling system, characterized in that, the viscosity of material leaving each of said vessels except for the first vessel is controlled in cascade by the steps of: measuring melt viscosities of material entering and leaving a downstream vessel at predetermined time intervals; storing the values so measured in a memory and calculating a resultant sum wherein said resultant sum is calculated by adding a value which corresponds to a difference between a set point and a measured value for the melt viscosity of the material leaving said downstream vessel at one of said time intervals to a value which corresponds to a difference between a set point and a measured value for the melt viscosity of material entering said downstream vessel at a predetermined time interval prior to said one time interval; resetting the set point for pressure control of a melt viscosity of the material in said downstream vessel in response to the resultant sum; and controlling the melt viscosity by adjusting pressure of the preceding upstream vessel by automatically resetting, for the preceding upstream vessel, the set point for a melt viscosity of the material leaving said upstream vessel, when the reset set point for said downstream vessel falls outside a predetermined range.
Claim 2
Dependent Claim 251 words
A continuous process for the production of ethylene terephthalate polyesters which comprises passing a polyester-forming fusion melt predominantly comprised of bis-2-hydroxethyl terephthalate and/or its low polymers sequentially through a series of reduced pressure polymerization vessles while controlling the degree of polymerization of the product by a controlling system, characterized in that, the viscosity of material leaving each of said vessels except for the first vessel is controlled in cascade by the steps of: measuring melt viscosities of material entering and leaving a downstream vessel at predetermined time intervals; storing the values so measured in a memory and calculating a resultant sum wherein said resultant sum is calculated by adding a value which corresponds to a difference between a set point and a measured value for the melt viscosity of the material leaving said downstream vessel at one of said time intervals to a value which corresponds to a difference between a set point and a measured value for the melt viscosity of material entering said downstream vessel at a predetermined time interval prior to said one time interval; resetting the set point for pressure control of a melt viscosity of the material in said downstream vessel in response to the resultant sum; and controlling the melt viscosity by adjusting pressure of the preceding upstream vessel by automatically resetting, for the preceding upstream vessel, the set point for a melt viscosity of the material leaving said upstream vessel, when the reset set point for said downstream vessel falls outside a predetermined range.
Claim 3
Dependent Claim 23 words
A continuous process for the production of ethylene terephthalate polyesters according to claim 1, wherein said controlling system is a programmed digital computer.
Claim 4
Dependent Claim 32 words
A continuous process for the production of ethylene terephthalate polyesters according to claim 1, wherein said controlling system is an analog computer including at least an adder, an integrator and a differentiator.
Claim 5
Dependent Claim 35 words
A continuous process for the production of ethylene terephthalate polyesters according to claim 1, wherein the set point controls the degree of vacuum in said vessels and thereby the degree to polymerization of the product.

References Cited (Backward Citations)

US3475392A Cited
US3438942A Cited
US3503937A Cited
US3502622A Cited
UST861005I4 Cited
US3878379A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1982-05-07 1982-11-06 1983-05-08 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1986-05-07 1986-11-06 1987-05-08 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1990-05-07 1990-11-06 1991-05-08 $7700.00 Window Closed / Lapsed

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