US4153649A
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Phosphate ester-type reaction product and method of preparing same
Assignee: Schlumberger Technology Corp
•
Filing: 1977-07-15
•
Granted: 1979-05-08
•
Expires: 1997-07-15
Abstract
Abstract The reaction product of a hydroxy ether and a pentavalent phosphorus compound with a short chain and/or long chain alcohol can be employed to gel organic liquids by mixing the reaction product with an organic liquid in the presence of a multivalent metal cation.
Inventors
- 👤 Thomas J. Griffin, Jr.
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-05 13:34
CPC Classifications
C; C09; C09K; C09K8/00; C09K8/60; C09K8/62; C09K8/64; C07; C07F; C07F9/00; C07F9/02; C07F9/06; C07F9/08; C09K3/00; Y; Y10; Y10S; Y10S507/00; Y10S507/922; Y10T; Y10T137/00; Y10T137/0318; Y10T137/0391
Claims Analysis
Total Claims: 60
Claim 1
Independent Claim
301 words
An organic phosphate ester composition having as a property the ability to increase the viscosity of kerosene when admixed in kerosene with sodium aluminate, said composition being prepared by the process which comprises the reaction of: A. a pentavalent phosphorus compound selected from the group consisting of P 2 O 5 and a mixture of P 2 O 5 with polyphosphoric acid; B. a hydroxy ether of the formula ROR 1 OH wherein R is a C 1 to C 6 alkyl group, R 1 is a C 2 or C 3 alkylene group and the total carbon atoms of R and R 1 range from 3 to about 8; and C. when the total carbon atoms of R and R 1 and is 3 or 4, a long chain substantially unsubstituted monohydric aliphatic alcohol containing at least 5 carbon atoms, but when the total carbon atoms of R and R 1 is 5 to 8, an alcohol selected from the group consisting of a long chain substantially unsubstituted monohydric aliphatic alcohol containing at least 5 carbon atoms, a short chain substantially unsubstituted monohydric aliphatic alcohol containing from 1 to 4 carbon atoms and a mixture of said alcohols, the individual mole ratios of the hydroxy ether, the long chain alcohol and the short chain alcohol to total P 2 O 5 being within the ranges of 0.4:1 to 4.5:1; 0:1 to 4.0:1 and 0:1 to 5.0:1 respectively, said reaction being conducted at temperature ranging from about 70° to about 90° C. for a period of time of from about 1.5 to about 6 hours, and said pentavalent phosphorus compound, hydroxy ether, and alcohol or alcohols being provided in molar ratios and admixed in a sequence effective to provide a reaction product suitable for use in increasing the viscosity of kerosene.
Claim 2
Dependent Claim
301 words
An organic phosphate ester composition having as a property the ability to increase the viscosity of kerosene when admixed in kerosene with sodium aluminate, said composition being prepared by the process which comprises the reaction of: A. a pentavalent phosphorus compound selected from the group consisting of P 2 O 5 and a mixture of P 2 O 5 with polyphosphoric acid; B. a hydroxy ether of the formula ROR 1 OH wherein R is a C 1 to C 6 alkyl group, R 1 is a C 2 or C 3 alkylene group and the total carbon atoms of R and R 1 range from 3 to about 8; and C. when the total carbon atoms of R and R 1 and is 3 or 4, a long chain substantially unsubstituted monohydric aliphatic alcohol containing at least 5 carbon atoms, but when the total carbon atoms of R and R 1 is 5 to 8, an alcohol selected from the group consisting of a long chain substantially unsubstituted monohydric aliphatic alcohol containing at least 5 carbon atoms, a short chain substantially unsubstituted monohydric aliphatic alcohol containing from 1 to 4 carbon atoms and a mixture of said alcohols, the individual mole ratios of the hydroxy ether, the long chain alcohol and the short chain alcohol to total P 2 O 5 being within the ranges of 0.4:1 to 4.5:1; 0:1 to 4.0:1 and 0:1 to 5.0:1 respectively, said reaction being conducted at temperature ranging from about 70° to about 90° C. for a period of time of from about 1.5 to about 6 hours, and said pentavalent phosphorus compound, hydroxy ether, and alcohol or alcohols being provided in molar ratios and admixed in a sequence effective to provide a reaction product suitable for use in increasing the viscosity of kerosene.
Claim 3
Dependent Claim
11 words
The reaction product of claim 1 wherein each alcohol is unsubstituted.
Claim 4
Dependent Claim
45 words
The reaction product of claim 2 wherein the individual mole ratios of the hydroxy ether, the long chain alcohol and the short chain alcohol to P 2 O 5 are within the ranges of 0.8:1 to 1.8:1; 0:1 to 1.4:1; and 0.9:1 to 2.0:1 respectively.
Claim 5
Dependent Claim
37 words
The reaction product of claim 3 wherein the total mole ratio of the hydroxy ether, the long chain alcohol and the short chain alcohol to total P 2 O 5 ranges from about 2.8:1 to about 7.0:1.
Claim 6
Dependent Claim
17 words
The reaction product of claim 1 wherein the pentavalent phosphorus compound is P 2 O 5 .
Claim 7
Dependent Claim
20 words
The reaction product of claim 1 wherein the long chain monohydric alcohol contains from 5 to about 12 carbon atoms.
Claim 8
Dependent Claim
19 words
The reaction product of claim 6 wherein the short chain alcohol is a primary, unsubstituted, straight chain, saturated alcohol.
Claim 9
Dependent Claim
25 words
The reaction product of claim 7 wherein the short chain alcohol is ethanol, methanol, or a mixture thereof, and the long chain alcohol is unsubstituted.
Claim 10
Dependent Claim
13 words
The reaction product of claim 8 wherein the short chain alcohol is methanol.
Claim 11
Dependent Claim
35 words
The reaction product of claim 1 wherein the total mole ratio of the hydroxy ether, the long chain alcohol and the short chain alcohol to total P 2 O 5 is about 3.64 to 1.
Claim 12
Dependent Claim
30 words
The reaction product of claim 1 wherein the reaction temperature ranges from about 80° to about 90° C. and the reaction time ranges from about 1.5 to about 3 hours.
Claim 13
Dependent Claim
46 words
The reaction product of claim 1 werein when the total carbon atoms of R and R 1 is 3 or 4 there is also reacted a short chain substantially unsubstituted monohydric aliphatic alcohol containing from 1 to 4 carbon atoms or a mixture of said alcohols.
Claim 14
Dependent Claim
34 words
The reaction product of claim 12 wherein the long chain alcohol is unsubstituted and contains from 5 to 12 carbon atoms, and wherein the short chain alcohol is methanol, ethanol, or a mixture thereof.
Claim 15
Dependent Claim
334 words
An organic phosphate ester composition prepared by the process which comprises the reaction of: A. a pentavalent phosphorus compound, selected from the group consisting of P 2 O 5 and a mixture of P 2 O 5 with polyphosphoric acid; B. a hydroxy ether of the formula ROR 1 OH wherein R is a C 1 to C 6 alkyl group, R 1 is a C 2 or C 3 alkylene group and the total carbon atoms of R and R 1 range from 3 to about 8; and C. when the total carbon atoms of R and R 1 is 3 or 4 a long chain substantially unsubstituted monohydric aliphatic alcohol containing at least 5 carbon atoms and a short chain substantially unsubstituted monohydric aliphatic alcohol containing from one to four carbon atoms; when the total carbon atoms of R and R 1 is five to eight a short chain substantially unsubstituted monohydric aliphatic alcohol containing from one to four carbon atoms; the individual mole ratios of the hydroxy ether, the long chain alcohol and the short chain alcohol to total P 2 O 5 being within the ranges of 0.4:1 to 4.5:1; 0:1 to 4.0:1 and 0:1 to 5:1 respectively, and the total mole ratio of said three components to total P 2 O 5 being from about 2.8:1 to about 7.0:1, said reaction being conducted by first reacting the phosphorus compound with the hydroxy ether, and when the total carbon atoms of R and R 1 is 3 or 4, also with the long chain alcohol for a period of time of from about 5 to about 30 minutes at a temperature of from about 70° to about 90° C., cooling the reaction mixture to below 70° C., adding the short chain alcohol to the reaction mixture and reacting the mixture at a temperature of from about 70° to about 90° C. for a period of time to provide a total reaction time of from about 1.5 to about 6 hours.
Claim 16
Dependent Claim
334 words
An organic phosphate ester composition prepared by the process which comprises the reaction of: A. a pentavalent phosphorus compound, selected from the group consisting of P 2 O 5 and a mixture of P 2 O 5 with polyphosphoric acid; B. a hydroxy ether of the formula ROR 1 OH wherein R is a C 1 to C 6 alkyl group, R 1 is a C 2 or C 3 alkylene group and the total carbon atoms of R and R 1 range from 3 to about 8; and C. when the total carbon atoms of R and R 1 is 3 or 4 a long chain substantially unsubstituted monohydric aliphatic alcohol containing at least 5 carbon atoms and a short chain substantially unsubstituted monohydric aliphatic alcohol containing from one to four carbon atoms; when the total carbon atoms of R and R 1 is five to eight a short chain substantially unsubstituted monohydric aliphatic alcohol containing from one to four carbon atoms; the individual mole ratios of the hydroxy ether, the long chain alcohol and the short chain alcohol to total P 2 O 5 being within the ranges of 0.4:1 to 4.5:1; 0:1 to 4.0:1 and 0:1 to 5:1 respectively, and the total mole ratio of said three components to total P 2 O 5 being from about 2.8:1 to about 7.0:1, said reaction being conducted by first reacting the phosphorus compound with the hydroxy ether, and when the total carbon atoms of R and R 1 is 3 or 4, also with the long chain alcohol for a period of time of from about 5 to about 30 minutes at a temperature of from about 70° to about 90° C., cooling the reaction mixture to below 70° C., adding the short chain alcohol to the reaction mixture and reacting the mixture at a temperature of from about 70° to about 90° C. for a period of time to provide a total reaction time of from about 1.5 to about 6 hours.
Claim 17
Dependent Claim
52 words
The reaction product of claim 14 wherein when the total carbon atoms of R and R 1 is five to eight there is also reacted with the pentavalent phosphorus compound and the hydroxy ether a long chain monohydric alcohol containing at least 5 carbon atoms prior to reacting the short chain alcohol.
Claim 18
Dependent Claim
17 words
The reaction product of claim 14 wherein the long chain alcohol has 5 to 12 carbon atoms.
Claim 19
Dependent Claim
17 words
The reaction product of claim 14 wherein the pentavalent phosphorus compound is P 2 O 5 .
Claim 20
Dependent Claim
19 words
The reaction product of claim 14 wherein the short chain alcohol is a primary, unsubstituted, straight chain, saturated alcohol.
Claim 21
Dependent Claim
25 words
The reaction product of claim 18 wherein the short chain alcohol is ethanol, methanol, or a mixture thereof, and the long chain alcohol is unsubstituted.
Claim 22
Dependent Claim
13 words
The reaction product of claim 19 wherein the short chain alcohol is methanol.
Claim 23
Dependent Claim
13 words
The reaction product of claim 19 wherein the short chain alcohol is ethanol.
Claim 24
Dependent Claim
11 words
The reaction product of claim 14 wherein each alcohol is unsubstituted.
Claim 25
Dependent Claim
38 words
The reaction product of claim 22 wherein the long chain alcohol has 5 to 12 carbon atoms; the pentavalent phosphorus compound is P 2 O 5 ; and the short chain alcohol is primary, straight chain, and saturated.
Claim 26
Dependent Claim
52 words
The reaction product of claim 23 wherein said hydroxy ether is selected from the group consisting of ethylene glycol monomethyl ether, ethylene glycol monoethyl ether, ethylene glycol mono-n-butyl ether, ethylene glycol mono-n-hexyl ether, ethylene glycol monoisobutyl ether, propylene glycol monomethyl ether, propylene glycol monoisobutyl ether, propylene glycol monomethyl ether and mixtures thereof.
Claim 27
Dependent Claim
45 words
The reaction product of claim 24 wherein the individual mole ratios of the hydroxy ether, the long chain alcohol and the short chain alcohol to P 2 O 5 are within the ranges of 0.8:1 to 1.8:1; 0:1 to 1.4:1; and 0.9:1 to 2.0:1 respectively.
Claim 28
Dependent Claim
18 words
The reaction product of claim 25 wherein the short chain alcohol is methanol, ethanol, or a mixture thereof.
Claim 29
Dependent Claim
30 words
The reaction product of claim 26 wherein the total mole ratio of the short chain alcohol, hydroxy ether and long chain alcohol to P 2 O 5 is about 3.64:1.
Claim 30
Dependent Claim
13 words
The reaction product of claim 27 wherein the short chain alcohol is methanol.
Claim 31
Independent Claim
298 words
A method of preparing an organic phosphate ester composition, said ester composition having as a property the ability to increase the viscosity of kerosene when admixed in kerosene with sodium aluminate, which comprises reacting: A. a pentavalent phosphorus compound selected from the group consisting of P 2 O 5 and a mixture of P 2 O 5 with polyphosphoric acid; B. a hydroxy ether of the formula ROR 1 OH wherein R is a C 1 to C 6 alkyl group, R 1 is a C 2 or C 3 alkylene group and the total carbon atoms of R and R 1 range from 3 to about 8; and C. when the total carbon atoms of R and R 1 is 3 or 4, a long chain substantially unsubstituted monohydric aliphatic alcohol containing at least 5 carbon atoms, but when the total carbon atoms of R and R 1 is 5 to 8, an alcohol selected from the group consisting of a long chain substantially unsubstituted monohydric aliphatic alcohol containing at least 5 carbon atoms, a short chain substantially unsubstituted monohydric aliphatic alcohol containing from 1 to 4 carbon atoms or a mixture of said alcohols, the individual mole ratios of the hydroxy ether, the long chain alcohol and the short chain alcohol to total P 2 O 5 are within the ranges of 0.4:1 to 4.5:1; 0:1 to 4.0:1 and 0:1 to 5.0:1 respectively, said reaction being conducted at temperature ranging from about 70° to about 90° C. for a period of time of from about 1.5 to about 6 hours, and said pentavalent phosphorus compound, hydroxy ether, and alcohol or alcohols being provided in molar ratios and admixed in a sequence effective to provide a reaction product suitable for use in increasing the viscosity of kerosene.
Claim 32
Independent Claim
298 words
A method of preparing an organic phosphate ester composition, said ester composition having as a property the ability to increase the viscosity of kerosene when admixed in kerosene with sodium aluminate, which comprises reacting: A. a pentavalent phosphorus compound selected from the group consisting of P 2 O 5 and a mixture of P 2 O 5 with polyphosphoric acid; B. a hydroxy ether of the formula ROR 1 OH wherein R is a C 1 to C 6 alkyl group, R 1 is a C 2 or C 3 alkylene group and the total carbon atoms of R and R 1 range from 3 to about 8; and C. when the total carbon atoms of R and R 1 is 3 or 4, a long chain substantially unsubstituted monohydric aliphatic alcohol containing at least 5 carbon atoms, but when the total carbon atoms of R and R 1 is 5 to 8, an alcohol selected from the group consisting of a long chain substantially unsubstituted monohydric aliphatic alcohol containing at least 5 carbon atoms, a short chain substantially unsubstituted monohydric aliphatic alcohol containing from 1 to 4 carbon atoms or a mixture of said alcohols, the individual mole ratios of the hydroxy ether, the long chain alcohol and the short chain alcohol to total P 2 O 5 are within the ranges of 0.4:1 to 4.5:1; 0:1 to 4.0:1 and 0:1 to 5.0:1 respectively, said reaction being conducted at temperature ranging from about 70° to about 90° C. for a period of time of from about 1.5 to about 6 hours, and said pentavalent phosphorus compound, hydroxy ether, and alcohol or alcohols being provided in molar ratios and admixed in a sequence effective to provide a reaction product suitable for use in increasing the viscosity of kerosene.
Claim 33
Dependent Claim
10 words
The method of claim 29 wherein each alcohol is unsubstituted.
Claim 34
Dependent Claim
44 words
The method of claim 30 wherein the individual mole ratios of the hydroxy ether, the long chain alcohol and the short chain alcohol to P 2 O 5 are within the ranges of 0.8:1 to 1.8:1; 0:1 to 1.4:1; and 0.9:1 to 2.0:1 respectively.
Claim 35
Dependent Claim
36 words
The method of claim 31 wherein the total mole ratio of the hydroxy ether, the long chain alcohol and the short chain alcohol to total P 2 O 5 ranges from about 2.8:1 to about 7.0:1.
Claim 36
Dependent Claim
16 words
The method of claim 29 wherein the pentavalent phosphorus compound is P 2 O 5 .
Claim 37
Dependent Claim
19 words
The method of claim 29 wherein the long chain monohydric alcohol contains from 5 to about 12 carbon atoms.
Claim 38
Dependent Claim
18 words
The method of claim 34 wherein the short chain alcohol is a primary, unsubstituted, straight chain, saturated alcohol.
Claim 39
Dependent Claim
24 words
The method of claim 35 wherein the short chain alcohol is ethanol, methanol, or a mixture thereof, and the long chain alcohol is unsubstituted.
Claim 40
Dependent Claim
12 words
The method of claim 36 wherein the short chain alcohol is methanol.
Claim 41
Dependent Claim
34 words
The method of claim 29 wherein the total mole ratio of the hydroxy ether, the long chain alcohol and the short chain alcohol to total P 2 O 5 is about 3.64 to 1.
Claim 42
Dependent Claim
29 words
The method of claim 29 wherein the reaction temperature ranges from about 80° to about 90° C. and the reaction time ranges from about 1.5 to about 3 hours.
Claim 43
Dependent Claim
45 words
The method of claim 29 wherein when the total carbon atoms of R and R 1 is 3 or 4 there is also reacted a short chain substantially unsubstituted monohydric aliphatic alcohol containing from 1 to 4 carbon atoms or a mixture of said alcohols.
Claim 44
Dependent Claim
33 words
The method of claim 40 wherein the long chain alcohol is unsubstituted and contains from 5 to 12 carbon atoms, and wherein the short chain alcohol is methanol, ethanol, or a mixture thereof.
Claim 45
Independent Claim
331 words
A method of preparing an organic phosphate ester composition comprising reacting: A. a pentavalent phosphorus compound, selected from the group consisting of P 2 O 5 and a mixture of P 2 O 5 with polyphosphoric acid; B. a hydroxy ether of the formula ROR 1 OH wherein R is a C 1 to C 6 alkyl group, R 1 is a C 2 or C 3 alkylene group and the total carbon atoms of R and R 1 range from 3 to about 8; and C. when the total carbon atoms of R and R 1 is 3 or 4 a long chain substantially unsubstituted monohydric aliphatic alcohol containing at least 5 carbon atoms and a short chain substantially unsubstituted monohydric aliphatic alcohol containing from one to four carbon atoms; when the total carbon atoms of R and R 1 is five to eight a short chain substantially unsubstituted monohydric aliphatic alcohol containing from one to four carbon atoms; the individual mole ratios of the hydroxy ether, the long chain alcohol and the short chain alcohol to total P 2 O 5 being within the ranges of 0.4:1 to 4.5:1; 0:1 to 4.0:1 and 0:1 to 5:1 respectively, and the total mole ratio of said three components to total P 2 O 5 being from about 2.8:1 to about 7.0:1, said reaction being conducted by first reacting the phosphorus compound with the hydroxy ether, and when the total carbon atoms of R and R 1 is 3 or 4, also with the long chain alcohol for a period of time of from about 5 to about 30 minutes at a temperature of from about 70° to about 90° C., cooling the reaction mixture to below 70° C., adding the short chain alcohol to the reaction mixture and reacting the mixture at a temperature of from about 70° to about 90° C. for a period of time to provide a total reaction time of from about 1.5 to about 6 hours.
Claim 46
Independent Claim
331 words
A method of preparing an organic phosphate ester composition comprising reacting: A. a pentavalent phosphorus compound, selected from the group consisting of P 2 O 5 and a mixture of P 2 O 5 with polyphosphoric acid; B. a hydroxy ether of the formula ROR 1 OH wherein R is a C 1 to C 6 alkyl group, R 1 is a C 2 or C 3 alkylene group and the total carbon atoms of R and R 1 range from 3 to about 8; and C. when the total carbon atoms of R and R 1 is 3 or 4 a long chain substantially unsubstituted monohydric aliphatic alcohol containing at least 5 carbon atoms and a short chain substantially unsubstituted monohydric aliphatic alcohol containing from one to four carbon atoms; when the total carbon atoms of R and R 1 is five to eight a short chain substantially unsubstituted monohydric aliphatic alcohol containing from one to four carbon atoms; the individual mole ratios of the hydroxy ether, the long chain alcohol and the short chain alcohol to total P 2 O 5 being within the ranges of 0.4:1 to 4.5:1; 0:1 to 4.0:1 and 0:1 to 5:1 respectively, and the total mole ratio of said three components to total P 2 O 5 being from about 2.8:1 to about 7.0:1, said reaction being conducted by first reacting the phosphorus compound with the hydroxy ether, and when the total carbon atoms of R and R 1 is 3 or 4, also with the long chain alcohol for a period of time of from about 5 to about 30 minutes at a temperature of from about 70° to about 90° C., cooling the reaction mixture to below 70° C., adding the short chain alcohol to the reaction mixture and reacting the mixture at a temperature of from about 70° to about 90° C. for a period of time to provide a total reaction time of from about 1.5 to about 6 hours.
Claim 47
Dependent Claim
51 words
The method of claim 42 wherein when the total carbon atoms of R and R 1 is five to eight there is also reacted with the pentavalent phosphorus compound and the hydroxy ether a long chain monohydric alcohol containing at least 5 carbon atoms prior to reacting the short chain alcohol.
Claim 48
Dependent Claim
16 words
The method of claim 42 wherein the long chain alcohol has 5 to 12 carbon atoms.
Claim 49
Dependent Claim
16 words
The method of claim 42 wherein the pentavalent phosphorus compound is P 2 O 5 .
Claim 50
Dependent Claim
18 words
The method of claim 42 wherein the short chain alcohol is a primary, unsubstituted, straight chain, saturated alcohol.
Claim 51
Dependent Claim
24 words
The method of claim 46 wherein the short chain alcohol is ethanol, methanol, or a mixture thereof, and the long chain alcohol is unsubstituted.
Claim 52
Dependent Claim
12 words
The method of claim 47 wherein the short chain alcohol is methanol.
Claim 53
Dependent Claim
12 words
The method of claim 47 wherein the short chain alcohol is ethanol.
Claim 54
Dependent Claim
10 words
The method of claim 42 wherein each alcohol is unsubstituted.
Claim 55
Dependent Claim
37 words
The method of claim 50 wherein the long chain alcohol has 5 to 12 carbon atoms; the pentavalent phosphorus compound is P 2 O 5 ; and the short chain alcohol is primary, straight chain, and saturated.
Claim 56
Dependent Claim
51 words
The method of claim 51 wherein said hydroxy ether is selected from the group consisting of ethylene glycol monomethyl ether, ethylene glycol monoethyl ether, ethylene glycol mono-n-butyl ether, ethylene glycol mono-n-hexyl ether, ethylene glycol monoisobutyl ether, propylene glycol monomethyl ether, propylene glycol monoisobutyl ether, propylene glycol monomethyl ether and mixtures thereof.
Claim 57
Dependent Claim
44 words
The method of claim 52 wherein the individual mole ratios of the hydroxy ether, the long chain alcohol and the short chain alcohol to P 2 O 5 are within the ranges of 0.8:1 to 1.8:1; 0:1 to 1.4:1; and 0.9:1 to 2.0:1 respectively.
Claim 58
Dependent Claim
17 words
The method of claim 53 wherein the short chain alcohol is methanol, ethanol, or a mixture thereof.
Claim 59
Dependent Claim
29 words
The method of claim 54 wherein the total mole ratio of the short chain alcohol, hydroxy ether and long chain alcohol to P 2 O 5 is about 3.64:1.
Claim 60
Dependent Claim
12 words
The method of claim 55 wherein the short chain alcohol is methanol.
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