US4141715A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Method and apparatus for producing a nitrate fertilizer
Assignee: NI-LECTRA Corp 3629 N DIXIE DRIVE DAYTON OH 45414 A CORP OF OH
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Filing: 1977-04-11
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Granted: 1979-02-27
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Expires: 1997-04-11
Abstract
Abstract Pressurized air is directed into a generally spherical combustion chamber to rotate an electrical arc within a circular aperture formed within an electrode element disposed within the center portion of the chamber. The air is directed through the aperture and the whirling arc to produce a nitrogen dioxide gas which is immediately aspirated into a recirculating flow of water. The water is directed through an elongated tube forming an absorption coil where the gas is absorbed into the water to form a dilute acid solution usable as a nitrate fertilizer.
Inventors
- 👤 Harold G. Wyse
- 👤 Millard S. Smith
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-04 11:29
CPC Classifications
B; B01; B01J; B01J19/00; B01J19/08; B01J19/087; B01J19/088; C; C05; C05C; C05C11/00
Claims Analysis
Total Claims: 17
Claim 1
Independent Claim
150 words
A method adapted for efficiently producing a nitrate fertilizer, comprising the steps of forming a first electrode element defining a circular aperture of predetermined diameter, arranging said first electrode element concentrically within the center of a generally spherical air combustion chamber having a diameter larger than the diameter of said aperture, arranging a second electrode element within the center of said aperture, supplying an electrical voltage across said electrode elements to produce an electrical plasma arc therebetween, producing a spiral flow of air within said spherical chamber to effect rotation of the arc within the aperture, directing the spiral flow of air through the aperture for efficiently generating a nitrogen dioxide gas, introducing the gas from the combustion chamber directly into a flow of water, and directing the water and gas through an elongated tube forming an absorption coil to produce a dilute acid solution usable as a nitrate fertilizer.
Claim 2
Independent Claim
150 words
A method adapted for efficiently producing a nitrate fertilizer, comprising the steps of forming a first electrode element defining a circular aperture of predetermined diameter, arranging said first electrode element concentrically within the center of a generally spherical air combustion chamber having a diameter larger than the diameter of said aperture, arranging a second electrode element within the center of said aperture, supplying an electrical voltage across said electrode elements to produce an electrical plasma arc therebetween, producing a spiral flow of air within said spherical chamber to effect rotation of the arc within the aperture, directing the spiral flow of air through the aperture for efficiently generating a nitrogen dioxide gas, introducing the gas from the combustion chamber directly into a flow of water, and directing the water and gas through an elongated tube forming an absorption coil to produce a dilute acid solution usable as a nitrate fertilizer.
Claim 3
Independent Claim
215 words
A method adapted for efficiently producing a nitrate fertilizer, comprising the steps of forming a plurality of air combustion units each having a generally flat first electrode element defining a circular aperture, arranging the first electrode element of each combustion unit within a corresponding circular air combustion chamber having a diameter larger than the diameter of the aperture, arranging a second electrode element substantially within the center of the aperture of said first electrode element of each unit, supplying an electrical voltage across the electrode elements of each unit to produce an electrical arc therebetween, producing a spiral flow of air within the chamber of each unit to effect rotation of the arc within the aperture, directing the flow of air within each unit through the rotating arc within the corresponding aperture for generating a nitrogen dioxide gas, connecting the units in series with the air and gas exhausted from the first unit being directed through the second unit, directing the gas from the series connected combustion units into a flow of water, directing the water and gas through an elongated tube to produce a dilute acid solution usable as a nitrate fertilizer, and recirculating the solution within the tube while gas is being directed into the solution to increase the concentration of the solution.
Claim 4
Independent Claim
215 words
A method adapted for efficiently producing a nitrate fertilizer, comprising the steps of forming a plurality of air combustion units each having a generally flat first electrode element defining a circular aperture, arranging the first electrode element of each combustion unit within a corresponding circular air combustion chamber having a diameter larger than the diameter of the aperture, arranging a second electrode element substantially within the center of the aperture of said first electrode element of each unit, supplying an electrical voltage across the electrode elements of each unit to produce an electrical arc therebetween, producing a spiral flow of air within the chamber of each unit to effect rotation of the arc within the aperture, directing the flow of air within each unit through the rotating arc within the corresponding aperture for generating a nitrogen dioxide gas, connecting the units in series with the air and gas exhausted from the first unit being directed through the second unit, directing the gas from the series connected combustion units into a flow of water, directing the water and gas through an elongated tube to produce a dilute acid solution usable as a nitrate fertilizer, and recirculating the solution within the tube while gas is being directed into the solution to increase the concentration of the solution.
Claim 5
Dependent Claim
193 words
Apparatus for producing a nitrate fertilizer, comprising at least one air combustion unit including a body defining a substantially spherical combustion chamber, a generally flat first electrode plate disposed within the center of said chamber and defining a substantially circular aperture having a diameter smaller than the diameter of said chamber, a second electrode element projecting into said chamber generally perpendicular to said first electrode plate and disposed substantially within the center of said aperture, means defining an in let passage within said body on one side of said electrode plate for introducing a flow of pressurized air into said spherical chamber and for directing all of the flow of air through said aperture, means defining an exhaust passage for said spherical chamber on the opposite side of said electrode plate, means for supplying a high voltage to said electrode plate and electrode element to produce an electrical arc therebetween, the flow of air through said aperture and the arc within said aperture being effective to generate a nitrogen dioxide gas, and means for introducing the gas into a supply of water to produce a dilute acid solution usable as a nitrate fertilizer.
Claim 6
Dependent Claim
193 words
Apparatus for producing a nitrate fertilizer, comprising at least one air combustion unit including a body defining a substantially spherical combustion chamber, a generally flat first electrode plate disposed within the center of said chamber and defining a substantially circular aperture having a diameter smaller than the diameter of said chamber, a second electrode element projecting into said chamber generally perpendicular to said first electrode plate and disposed substantially within the center of said aperture, means defining an in let passage within said body on one side of said electrode plate for introducing a flow of pressurized air into said spherical chamber and for directing all of the flow of air through said aperture, means defining an exhaust passage for said spherical chamber on the opposite side of said electrode plate, means for supplying a high voltage to said electrode plate and electrode element to produce an electrical arc therebetween, the flow of air through said aperture and the arc within said aperture being effective to generate a nitrogen dioxide gas, and means for introducing the gas into a supply of water to produce a dilute acid solution usable as a nitrate fertilizer.
Claim 7
Dependent Claim
30 words
Apparatus as defined in claim 3 wherein said inlet passage is disposed adjacent to and generally parallel to said first electrode element and is offset radially outwardly from said aperture.
Claim 8
Independent Claim
116 words
A method adapted for efficiently producing a nitrate fertilizer, comprising the steps of forming a generally flat first electrode plate defining a circular aperture of predetermined diameter, arranging said electrode plate concentrically within the center of a generally spherical air combustion chamber having a diameter larger than the diameter of said aperture, arranging a second electrode element within the center of said aperture, supplying an electrical voltage across said electrode plate and the electrode element to produce an electrical plasma arc therebetween, introducing a flow of air into the spherical chamber on one side of the electrode plate, and directing all of the flow of air through the aperture for efficiently generating a nitrogen dioxide gas.
Claim 9
Independent Claim
116 words
A method adapted for efficiently producing a nitrate fertilizer, comprising the steps of forming a generally flat first electrode plate defining a circular aperture of predetermined diameter, arranging said electrode plate concentrically within the center of a generally spherical air combustion chamber having a diameter larger than the diameter of said aperture, arranging a second electrode element within the center of said aperture, supplying an electrical voltage across said electrode plate and the electrode element to produce an electrical plasma arc therebetween, introducing a flow of air into the spherical chamber on one side of the electrode plate, and directing all of the flow of air through the aperture for efficiently generating a nitrogen dioxide gas.
Claim 10
Dependent Claim
57 words
A method as defined in claim 5 including the step of aspirating the nitrogen dioxide into a flow of water within a tube to form a dilute acid solution, directing the solution through the tube and into a storage vessel, and recirculating the solution from the vessel into the tube for increasing the concentration of the solution.
Claim 11
Independent Claim
174 words
A method adapted for efficiently producing a nitrate fertilizer, comprising the steps of forming a plurality of air combustion units each having a generally flat first electrode plate defining a circular aperture, arranging the first electrode plate of each combustion unit within a corresponding generally spherical air combustion chamber having a diameter larger than the diameter of the aperture, arranging a second electrode element substantially within the center of the aperture of said first electrode plate of each unit, supplying an electrical voltage across the electrode plate and electrode element of each unit to produce an electrical arc therebetween, introducing a spiral flow of air within the chamber of each unit on one side of the electrode plate to effect rotation of the arc within the aperture, directing all of the spiral flow of air within each unit through the rotating arc within the corresponding aperture for generating a nitrogen dioxide gas, and connecting the units in series with the air and gas exhausted from the first unit being directed through the second unit.
Claim 12
Independent Claim
174 words
A method adapted for efficiently producing a nitrate fertilizer, comprising the steps of forming a plurality of air combustion units each having a generally flat first electrode plate defining a circular aperture, arranging the first electrode plate of each combustion unit within a corresponding generally spherical air combustion chamber having a diameter larger than the diameter of the aperture, arranging a second electrode element substantially within the center of the aperture of said first electrode plate of each unit, supplying an electrical voltage across the electrode plate and electrode element of each unit to produce an electrical arc therebetween, introducing a spiral flow of air within the chamber of each unit on one side of the electrode plate to effect rotation of the arc within the aperture, directing all of the spiral flow of air within each unit through the rotating arc within the corresponding aperture for generating a nitrogen dioxide gas, and connecting the units in series with the air and gas exhausted from the first unit being directed through the second unit.
Claim 13
Dependent Claim
253 words
Apparatus for producing a nitrate fertilizer, comprising at least one air combustion unit including a body defining a combustion chamber having a circular configuration, a generally flat first electrode element disposed within said chamber and defining a substantially circular and concentric aperture having a diameter smaller than the diameter of said chamber, a second electrode element projecting into said chamber and disposed concentrically with said aperture, means defining an inlet passage within said body on one side of said first electrode element for introducing pressurized air into said chamber and for causing a spiral flow of air through said aperture, means defining an exhaust passage for said chamber on the opposite side of said first electrode element to assure that all of the air flowing through said inlet passage into said chamber passes through said aperture, means for supplying a high voltage to said electrode elements to produce an electrical arc therebetween, said spiral flow of air through said aperture being effective to rotate the arc within said aperture for subjecting a high proportion of said air flow to the arc for efficiently generating a nitrogen dioxide gas, means defining a water storage chamber, an absorption coil of tubing having substantial length, means for recirculating water from said storage chamber through said tubing forming said coil, and means for introducing the gas generated by said combustion unit directly into the water flowing within said tubing forming said coil to provide substantial gas-water exposure time for the nitrogen oxides to dissolve into the water.
Claim 14
Dependent Claim
253 words
Apparatus for producing a nitrate fertilizer, comprising at least one air combustion unit including a body defining a combustion chamber having a circular configuration, a generally flat first electrode element disposed within said chamber and defining a substantially circular and concentric aperture having a diameter smaller than the diameter of said chamber, a second electrode element projecting into said chamber and disposed concentrically with said aperture, means defining an inlet passage within said body on one side of said first electrode element for introducing pressurized air into said chamber and for causing a spiral flow of air through said aperture, means defining an exhaust passage for said chamber on the opposite side of said first electrode element to assure that all of the air flowing through said inlet passage into said chamber passes through said aperture, means for supplying a high voltage to said electrode elements to produce an electrical arc therebetween, said spiral flow of air through said aperture being effective to rotate the arc within said aperture for subjecting a high proportion of said air flow to the arc for efficiently generating a nitrogen dioxide gas, means defining a water storage chamber, an absorption coil of tubing having substantial length, means for recirculating water from said storage chamber through said tubing forming said coil, and means for introducing the gas generated by said combustion unit directly into the water flowing within said tubing forming said coil to provide substantial gas-water exposure time for the nitrogen oxides to dissolve into the water.
Claim 15
Dependent Claim
20 words
Apparatus as defined in claim 8 wherein said tubing forming said coil has a length greater than one hundred feet.
Claim 16
Dependent Claim
19 words
Apparatus as defined in claim 8 wherein said tubing comprises a plastics material and extends along a helical path.
Claim 17
Dependent Claim
29 words
Apparatus as defined in claim 8 wherein said combustion chamber is generally spherical in configuration, and said second electrode elements is disposed generally within the center of said chamber.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1982-02-26 | 1982-08-28 | 1983-02-27 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1986-02-26 | 1986-08-28 | 1987-02-27 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1990-02-26 | 1990-08-28 | 1991-02-27 | $7700.00 | Window Closed / Lapsed |