US4131638A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Process for the manufacture of calcium silicate hydrate objects
Assignee: Johns Manville Corp
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Filing: 1977-07-05
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Granted: 1978-12-26
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Expires: 1997-07-05
Abstract
Abstract An improved "pre-autoclaving" process for the formation of fiber-reinforced calcium silicate hydrate bodies (such as thermal insulation) is disclosed. The improvement comprises first cooling the crystal slurry from the reactor in a heat exchanger and then metering the cooled slurry through a venturi to reduce the pressure and control the flow rate.
Inventors
- 👤 Thomas E. Whitaker
- 👤 Samuel Myles
- 👤 Ian P. Gardner
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-01 15:06
CPC Classifications
C; C01; C01B; C01B33/00; C01B33/20; C01B33/24; C04; C04B; C04B28/00; C04B28/18; C04B40/00; C04B40/02; C04B40/024; C04B2111/00; C04B2111/00017; Y; Y02; Y02P; Y02P40/00; Y02P40/60; Y02W; Y02W30/00; Y02W30/50; Y02W30/91
Claims Analysis
Total Claims: 7
Claim 1
Independent Claim
179 words
In the process for the formation of shaped calcium silicate hydrate objects which comprises forming an aqueous slurry of a siliceous material and a source of calcium oxide, heating said slurry in a reactor in the presence of saturated steam at a pressure of at least 75 psig for a period of at least 0.5 hour to form hydrated calcium silicate crystals from said siliceous material and said source of calcium oxide, removing from said reactor said hydrated calcium silicate crystals in the form of a slurry of said crystals dispersed in aqueous medium, forming said crystals into shaped objects while simultaneously separating a portion of said aqueous medium from said crystals and then drying said shaped objects, the improvement which comprises: (a) passing said slurry through a heat exchanger where the temperature of said slurry is substantially reduced; and (b) thereafter metering the cooled slurry through a venturi wherein the pressure on said slurry is reduced and the flow rate controlled into a receiver, from which receiver said slurry can be subsequently withdrawn for molding into said objects.
Claim 2
Dependent Claim
179 words
In the process for the formation of shaped calcium silicate hydrate objects which comprises forming an aqueous slurry of a siliceous material and a source of calcium oxide, heating said slurry in a reactor in the presence of saturated steam at a pressure of at least 75 psig for a period of at least 0.5 hour to form hydrated calcium silicate crystals from said siliceous material and said source of calcium oxide, removing from said reactor said hydrated calcium silicate crystals in the form of a slurry of said crystals dispersed in aqueous medium, forming said crystals into shaped objects while simultaneously separating a portion of said aqueous medium from said crystals and then drying said shaped objects, the improvement which comprises: (a) passing said slurry through a heat exchanger where the temperature of said slurry is substantially reduced; and (b) thereafter metering the cooled slurry through a venturi wherein the pressure on said slurry is reduced and the flow rate controlled into a receiver, from which receiver said slurry can be subsequently withdrawn for molding into said objects.
Claim 3
Dependent Claim
27 words
An improved process as in claim 1 wherein the temperature of said slurry is reduced in said heat exchanger by about 100° F to about 150° F.
Claim 4
Dependent Claim
20 words
An improved process as in claim 1 wherein the pressure on said slurry is reduced to ambient by said venturi.
Claim 5
Dependent Claim
25 words
An improved process as in claim 1 wherein fibers are mixed into said slurry of crystals prior to forming said crystals into said shaped objects.
Claim 6
Dependent Claim
29 words
An improved process as in claim 4 wherein finely ground scrap calcium silicate hydrate is also mixed into said slurry prior to forming said crystals into said shaped objects.
Claim 7
Dependent Claim
32 words
An improved process as in claim 1 wherein water is used as the cooling medium in said heat exchanger and thereafter the water is used as preheated feed water to said reactor.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1981-12-25 | 1982-06-26 | 1982-12-26 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1985-12-25 | 1986-06-26 | 1986-12-26 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1989-12-25 | 1990-06-26 | 1990-12-26 | $7700.00 | Window Closed / Lapsed |