US4128516A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Process for the gentle degasification of coagulation-sensitive PVC latices
Assignee: Wacker Chemie AG
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Filing: 1977-07-07
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Granted: 1978-12-05
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Expires: 1997-07-07
Abstract
Abstract In the process for the gentle degasification of coagulation-sensitive PVC latices in a confined space under reduced pressure and stirring at elevated temperatures with steam injection onto the latex surface, the improvement consisting essentially of conducting said degasification at a selected temperature from 50° C to 80° C at a pressure corresponding to the boiling pressure of water at the selected temperature, stirring said latex by an inclined stirrer whereby a rolling action of said latex in said confined space is effected and introducing said steam into the gas space above said latex but directed along the surface of the confined space.
Inventors
- 👤 Hans Geschonke
- 👤 Rainer Rompeltien
- 👤 Wolfgang Rummel
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-02 02:20
CPC Classifications
C; C08; C08F; C08F6/00; C08F6/001; C08F6/003
Claims Analysis
Total Claims: 12
Claim 1
Independent Claim
240 words
In the process for the gentle degasification of coagulation-sensitive PVC latices in a confined space under reduced pressure and stirring at elevated temperatures with steam injection onto the latex surface, the improvement consisting essentially of conducting said degasification at a selected temperature from 50° C. to 80° C. at a pressure corresponding to the boiling pressure of water at the selected temperature, stirring said latex by an inclined stirrer mounted in a perpendicular plane to the vessel wall and inclined from the vertical by an angle β of 20° to 45° in a clockwise direction, said inclined stirrer extending beyond the wall of said vessel by the length L said latex surface being between a minimum height H 1 , and a maximum height H 2 in said vessel having a diameter D, where the ratio of L to D is from 0.3 to 0.1, the ratio of the lower limit of H 1 is 0.3 > H 1 to D > 0.1, the ratio of the upper limit H.sub. 2 is 1 > H 2 to D > 0.2, said stirrer being situated so that effective stirring occurs at H 1 and H 2 is at about 50% of the total liquid capacity of said vessel, whereby a rolling action of said latex in said confined space is effected and introducing said steam into the gas space above said latex but directed along the surface of the confined space.
Claim 2
Dependent Claim
240 words
In the process for the gentle degasification of coagulation-sensitive PVC latices in a confined space under reduced pressure and stirring at elevated temperatures with steam injection onto the latex surface, the improvement consisting essentially of conducting said degasification at a selected temperature from 50° C. to 80° C. at a pressure corresponding to the boiling pressure of water at the selected temperature, stirring said latex by an inclined stirrer mounted in a perpendicular plane to the vessel wall and inclined from the vertical by an angle β of 20° to 45° in a clockwise direction, said inclined stirrer extending beyond the wall of said vessel by the length L said latex surface being between a minimum height H 1 , and a maximum height H 2 in said vessel having a diameter D, where the ratio of L to D is from 0.3 to 0.1, the ratio of the lower limit of H 1 is 0.3 > H 1 to D > 0.1, the ratio of the upper limit H.sub. 2 is 1 > H 2 to D > 0.2, said stirrer being situated so that effective stirring occurs at H 1 and H 2 is at about 50% of the total liquid capacity of said vessel, whereby a rolling action of said latex in said confined space is effected and introducing said steam into the gas space above said latex but directed along the surface of the confined space.
Claim 3
Dependent Claim
33 words
The process of claim 1 wherein said steam is directed along the surface of the confined space at an angle α of from 60° to 90° from the vertical in a clockwise direction.
Claim 4
Dependent Claim
30 words
The process of claim 1 wherein said steam is directed in a horizontally circular spray in substantially the center of said confined space to the surface of said confined space.
Claim 5
Dependent Claim
14 words
The process of claim 1 wherein said ratio of L to D is 0.2.
Claim 6
Dependent Claim
24 words
The process of claim 1 wherein said ratio of the upper limit H 2 is 1 > H 2 to D 0.3 to 0.5.
Claim 7
Dependent Claim
14 words
The process of claim 1 wherein said angle β is from 25° to 35°.
Claim 8
Dependent Claim
14 words
The process of claim 2 wherein said angle α is from 70° to 80°.
Claim 9
Dependent Claim
83 words
The process of claim 3 wherein said steam is directed in a horizontally circular spray by means of a circular baffle, parallel to the surface of the latex having a diameter d 1 placed at a distance h from the dome of said confined space having a diameter D, said confined space having a neck of diameter d at its top where the following ratios apply: 0.01 < d 1 /D < 0.05 0.05 < d/D < 0.2 0.02 < h/D < 0.05
Claim 10
Dependent Claim
35 words
The process of claim 8 where the ratio of d 1 to D is from 0.02 to 0.03, the ratio of d to D is 0.1 and the ratio of h to D is 0.03.
Claim 11
Dependent Claim
25 words
The process of claim 8 wherein said circular baffle has a lid set a distance S thereover and S is from 0.5 to 5 mm.
Claim 12
Dependent Claim
13 words
The process of claim 10 wherein S is from 1 to 2 mm.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1981-12-04 | 1982-06-05 | 1982-12-05 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1985-12-04 | 1986-06-05 | 1986-12-05 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1989-12-04 | 1990-06-05 | 1990-12-05 | $7700.00 | Window Closed / Lapsed |