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US4127680A Expired / Lapsed US ⏱️ 0.0 years remaining

Making a capacitor employing a temporary solid mask in the porous anode

Assignee: Vishay Sprague Inc
•
Filing: 1977-02-03
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Granted: 1978-11-28
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Expires: 1997-02-03
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Abstract

Abstract Formed porous tantalum pellets each having an extending anode wire are lowered part way into a molten compound such as napthalene. The napthalene wicks its way into substantially all of the pellet pores. Upon removal from the bath the napthalene freezes within each pellet. A liquid insulating material is applied to the anode wire while being masked from entering the porous pellet by the napthalene. The napthalene is subsequently vaporized from the pores and thereafter manganous nitrate is introduced into the pellet and is pyrolyzed to form MnO2.

Inventors

  • 👤 George A. Shirn
  • 👤 Sidney D. Ross

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-28 17:13
CPC Classifications
H; H01; H01G; H01G9/00; H01G9/004; H01G9/008; H01G9/012

Claims Analysis

Total Claims: 10
Claim 1
Independent Claim 129 words
A method for making a solid electrolyte capacitor having a porous valve metal pellet with a lead wire extending from one surface thereof comprising (a) forming a dielectric film over the surfaces of said porous valve metal pellet; (b) applying a sealing film over at least said one surface and into the pores of said pellet with a molten masking compound selected from naphthalene, camphor, p-dichlorobenzene, and CCl 3 CF 2 Cl; (c) applying an insulative coating in a water-dispersed form to said wire while providing a temperature and atmospheric pressure at which said masking compound is solid; (d) solidifying said coating; and vaporizing said solid masking compound from said one surface so that a space is formed between and completely separates said solidified insulative coating and said pellet.
Claim 2
Independent Claim 129 words
A method for making a solid electrolyte capacitor having a porous valve metal pellet with a lead wire extending from one surface thereof comprising (a) forming a dielectric film over the surfaces of said porous valve metal pellet; (b) applying a sealing film over at least said one surface and into the pores of said pellet with a molten masking compound selected from naphthalene, camphor, p-dichlorobenzene, and CCl 3 CF 2 Cl; (c) applying an insulative coating in a water-dispersed form to said wire while providing a temperature and atmospheric pressure at which said masking compound is solid; (d) solidifying said coating; and vaporizing said solid masking compound from said one surface so that a space is formed between and completely separates said solidified insulative coating and said pellet.
Claim 3
Dependent Claim 34 words
The method of claim 1 wherein said applying a sealing film is accomplished by immersing into said molten masking compound only a portion of said pellet which portion is opposite to said one surface.
Claim 4
Dependent Claim 19 words
The method of claim 2 wherein said applying a sealing film is effected in said one surface by capillarity.
Claim 5
Dependent Claim 41 words
The method of claim 1 wherein the melting temperature of said masking compound at one atmosphere is at least 30° C. and wherein said applying of said insulative coating is accomplished in an ambient of about 23° C. at one atmosphere.
Claim 6
Dependent Claim 22 words
The method of claim 1 wherein said liquid form of said insulative coating consists of highly fluorinated polymer particles dispersed in water.
Claim 7
Dependent Claim 12 words
The method of claim 5 wherein said highly fluorinated polymer is polytetrafluoroethylene.
Claim 8
Dependent Claim 25 words
The method of claim 6 wherein said solidifying is accomplished simultaneously with said vaporizing by elevating the temperature above 23° C. and drying said coating.
Claim 9
Dependent Claim 31 words
The method of claim 1 wherein said application of said insulative coating is accomplished by submersing the whole of said pellet with said solid masking compound into said liquid insulative material.
Claim 10
Dependent Claim 23 words
The method of claim 8 additionally comprising, after said solidifying and said vaporizing, removing the excess insulative material by a mechanical agitating means.

References Cited (Backward Citations)

US3438809A Cited
US3817782A Cited
US3823347A Cited
US3948706A Cited
US3967000A Cited
US4042420A Cited
US4022928A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1981-11-27 1982-05-29 1982-11-28 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1985-11-27 1986-05-29 1986-11-28 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1989-11-27 1990-05-29 1990-11-28 $7700.00 Window Closed / Lapsed

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