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US4117031A Expired / Lapsed US ⏱️ 0.0 years remaining

Crude oil demulsifiers

Assignee: Hoechst AG
•
Filing: 1975-09-22
•
Granted: 1978-09-26
•
Expires: 1995-09-22
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Abstract

Abstract A condensation product obtained by first preparing A. an addition product of aliphatic aldehydes and phenol in a molar ratio of about 1 : 1 to 3 : 1, at temperatures in the range of from about 50° to 80° C, in the presence of an alkaline catalyst, And separately therefrom B. a block polymer, obtained from a polypropylene glycol having a molecular weight from about 1500 to 2500 by the addition of about 30 to 50% by weight of ethylene oxide in the presence of an alkaline catalyst, And subsequently C. condensing about 0.5 to 4 moles of a) with 1 mole of b), after previous neutralization, if necessary in the presence of inert solvents, at 80° to 150° C, and removing the reaction water formed, And its use as demulsifying agent for the separation of water from crude oil emulsions.

Inventors

  • 👤 Johannes Macenka
  • 👤 Manfred Fischer
  • 👤 Fritz Joachim Gohlke

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-31 12:35
CPC Classifications
C; C08; C08G; C08G65/00; C08G65/02; C08G65/32; C08G65/329; C08G65/331; C08G81/00; C10; C10G; C10G33/00; C10G33/04

Claims Analysis

Total Claims: 4
Claim 1
Independent Claim 127 words
A condensation product obtained by first preparing a. an addition product of aliphatic aldehydes and phenol in a molar ratio of about 1 : 1 to 3 : 1, at temperatures in the range of from about 50° to 80° C, in the presence of an alkaline catalyst, and separately therefrom b. a block polymer, obtained from a polypropylene glycol having a molecular weight from about 1500 to 2500 by the addition of about 30 to 50% by weight of ethylene oxide in the presence of an alkaline catalyst, and subsequently c. condensing about 0.5 to 4 moles of a) with 1 mole of b), after previous neutralization, if necessary in the presence of inert solvents, at 80° to 150° C, and removing the reaction water formed.
Claim 2
Dependent Claim 127 words
A condensation product obtained by first preparing a. an addition product of aliphatic aldehydes and phenol in a molar ratio of about 1 : 1 to 3 : 1, at temperatures in the range of from about 50° to 80° C, in the presence of an alkaline catalyst, and separately therefrom b. a block polymer, obtained from a polypropylene glycol having a molecular weight from about 1500 to 2500 by the addition of about 30 to 50% by weight of ethylene oxide in the presence of an alkaline catalyst, and subsequently c. condensing about 0.5 to 4 moles of a) with 1 mole of b), after previous neutralization, if necessary in the presence of inert solvents, at 80° to 150° C, and removing the reaction water formed.
Claim 3
Dependent Claim 25 words
A condensation product as claimed in claim 1, wherein the molar ratio for preparing addition product (a) is 1.8 : 1 to 2.2 : 1.
Claim 4
Dependent Claim 37 words
A condensation product as claimed in claim 1, wherein the block polymer (b) is prepared from a polypropylene glycol having a molecular weight of from 1700 to 2200 and 35 to 40% by weight of ethylene oxide.

References Cited (Backward Citations)

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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1981-09-25 1982-03-27 1982-09-26 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1985-09-25 1986-03-27 1986-09-26 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1989-09-25 1990-03-27 1990-09-26 $7700.00 Window Closed / Lapsed

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