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US4115308A Expired / Lapsed US ⏱️ 0.0 years remaining

High-shear process for preparing silicate-containing paste-form detergent compositions

Assignee: Procter and Gamble Co
•
Filing: 1976-12-27
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Granted: 1978-09-19
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Expires: 1996-12-27
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Abstract

Abstract A process for preparing alkaline, silicate-containing paste-form detergent compositions, having good dispensing properties, is disclosed. In the disclosed process, the solid and liquid components of the detergent composition are subjected to high-shear mixing, followed by a simultaneous mixing and cooling step in which the temperature of the mixture is reduced to less than about 100 DEG F when the temperature of the mixture exceeds about 120 DEG F during the high-shear mixing operation. In a preferred single-step embodiment, the solid and liquid components are subjected to high-shear mixing while simultaneously being cooled such that the temperature of the mixture during mixing does not exceed about 120 DEG F.

Inventors

  • 👤 Raymond Ellwood Guerry

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-29 06:20
CPC Classifications
C; C11; C11D; C11D3/00; C11D3/02; C11D3/04; C11D3/08; C11D11/00; C11D11/0094; C11D17/00; C11D17/0008; C11D17/003

Claims Analysis

Total Claims: 13
Claim 1
Independent Claim 191 words
A process for the production of alkaline, silicate-containing, paste-form detergent compositions, comprising from about 30 to about 80% of solid inorganic components selected from the group consisting of silicates, phosphates, polyphosphates, carbonates, bicarbonates, borates, sulfates, and mixtures thereof; and containing at least about 0.5% of an alkoxylated nonionic surfactant, wherein the alkoxy moiety is selected from the group consisting of ethylene oxide, propylene oxide, and mixtures thereof; wherein the amount of water-soluble alkali metal silicate in the final composition is from about 10 to about 40%; and wherein the final composition contains from about 10 to about 50% of a detergency builder selected from the group consisting of polyphosphates, carbonates, bicarbonates, organic builders and mixtures thereof; comprising the steps of: (a) high-shear mixing the solid and liquid components of said composition, such that the temperature of the mixture exceeds about 80° F; the ratio by weight, of said solid components to said liquid components being from about 4:1 to about 1:2; followed by (b) simultaneously mixing and cooling said mixture to a temperature of less than about 80° F when a temperature of about 120° F is exceeded in step (a).
Claim 2
Dependent Claim 191 words
A process for the production of alkaline, silicate-containing, paste-form detergent compositions, comprising from about 30 to about 80% of solid inorganic components selected from the group consisting of silicates, phosphates, polyphosphates, carbonates, bicarbonates, borates, sulfates, and mixtures thereof; and containing at least about 0.5% of an alkoxylated nonionic surfactant, wherein the alkoxy moiety is selected from the group consisting of ethylene oxide, propylene oxide, and mixtures thereof; wherein the amount of water-soluble alkali metal silicate in the final composition is from about 10 to about 40%; and wherein the final composition contains from about 10 to about 50% of a detergency builder selected from the group consisting of polyphosphates, carbonates, bicarbonates, organic builders and mixtures thereof; comprising the steps of: (a) high-shear mixing the solid and liquid components of said composition, such that the temperature of the mixture exceeds about 80° F; the ratio by weight, of said solid components to said liquid components being from about 4:1 to about 1:2; followed by (b) simultaneously mixing and cooling said mixture to a temperature of less than about 80° F when a temperature of about 120° F is exceeded in step (a).
Claim 3
Dependent Claim 24 words
A process according to claim 1 wherein the temperature which the mixture exceeds during the high-shear mixing of step (a) is about 100° F.
Claim 4
Dependent Claim 24 words
A process according to claim 1 wherein the temperature which the mixture exceeds during the high-shear mixing of step (a) is about 120° F.
Claim 5
Dependent Claim 30 words
A process according to claim 1 wherein the mixture of solid and liquid components is cooled during the high-shear mixing, such that its temperature does not exceed about 120° F.
Claim 6
Dependent Claim 23 words
A process according to claim 4 wherein the temperature which the mixture does not exceed during the high-shear mixing is about 100° F.
Claim 7
Dependent Claim 23 words
A process according to claim 5 wherein the temperature which the mixture does not exceed during the high-shear mixing is about 85° F.
Claim 8
Dependent Claim 155 words
A process for the production of alkaline, silicate-containing, paste-form detergent compositions, exhibiting good flow and dispensing properties, containing at least about 0.5% of a surface active agent selected from the group consisting of nonionic surfactants, anionic surfactants, zwitterionic surfactants, and mixtures thereof; from about 10 to about 40% of a water-soluble alkali metal silicate component and from about 10 to about 50% of a detergency builder selected from the group consisting of polyphosphates, carbonates, bicarbonates, organic builders and mixtures thereof; comprising the step of (a) high-shear mixing the solid and liquid components of said composition, such that the temperature of the mixture exceeds about 80° F, the ratio, by weight of said solid components to said liquid components being from about 4:1 to about 1:2, followed by (b) simultaneously mixing and cooling said mixture to a temperature of less than about 80° F when a temperature of about 120° F is exceeded in step (a).
Claim 9
Dependent Claim 155 words
A process for the production of alkaline, silicate-containing, paste-form detergent compositions, exhibiting good flow and dispensing properties, containing at least about 0.5% of a surface active agent selected from the group consisting of nonionic surfactants, anionic surfactants, zwitterionic surfactants, and mixtures thereof; from about 10 to about 40% of a water-soluble alkali metal silicate component and from about 10 to about 50% of a detergency builder selected from the group consisting of polyphosphates, carbonates, bicarbonates, organic builders and mixtures thereof; comprising the step of (a) high-shear mixing the solid and liquid components of said composition, such that the temperature of the mixture exceeds about 80° F, the ratio, by weight of said solid components to said liquid components being from about 4:1 to about 1:2, followed by (b) simultaneously mixing and cooling said mixture to a temperature of less than about 80° F when a temperature of about 120° F is exceeded in step (a).
Claim 10
Dependent Claim 30 words
A process according to claim 7 wherein the mixture of solid and liquid components is cooled during the high-shear mixing, such that its temperature does not exceed about 120° F.
Claim 11
Dependent Claim 33 words
A process according to claim 8 wherein the surface-active agent is an alkoxylated nonionic surfactant, wherein the alkoxy moiety is selected from the group consisting of ethylene oxide, propylene oxide, and mixtures thereof.
Claim 12
Dependent Claim 23 words
A process according to claim 9 wherein the temperature which the mixture does not exceed during the high-shear mixing is about 100° F.
Claim 13
Dependent Claim 23 words
A process according to claim 10 wherein the temperature which the mixture does not exceed during the high-shear mixing is about 85° F.

References Cited (Backward Citations)

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US3450813A Cited
US3825498A Cited
US3817875A Cited
US3836641A Cited
US3803041A Cited
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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1981-09-18 1982-03-20 1982-09-19 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1985-09-18 1986-03-20 1986-09-19 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1989-09-18 1990-03-20 1990-09-19 $7700.00 Window Closed / Lapsed

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