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US4113649A Expired / Lapsed US ⏱️ 0.0 years remaining

Method for the solubilizing of alkali metal salts with polyethyleneglycoldiethers and the utilization thereof

Assignee: Studiengesellschaft Kohle gGmbH
•
Filing: 1976-08-04
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Granted: 1978-09-12
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Expires: 1996-08-04
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Abstract

Abstract Process of solubilizing alkali- and alkali-earth metal salts, characterized in that the salts are reacted in the presence of solvents if desired, with open-chain polyethyleneglycoldiethers of the general formula RO--[CH.sub.2 CH.sub.2 O].sub.n R' wherein n = 6 or more and R and R' are identical or different and represent alkyl, aryl or cycloalkyl groups respectively, the polyethyleneglycoldiethers having at least 7 oxygen atoms which are separated from one another each by two carbon atoms. The process can also be used to dissolve alkali metals.

Inventors

  • 👤 Herbert Lehmkuhl
  • 👤 Farroch Rabet

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-01 21:33
CPC Classifications
C; C07; C07C; C07C67/00; C07C67/10; C07C67/11; C07C17/00; C07C17/093; C07C17/20; C07C17/202; C07C17/208; C07C201/00; C07C201/06; C07C201/16; C07C253/00; C07C253/14; C07F; C07F1/00; C07F1/005; Y; Y10; Y10S; Y10S516/00; Y10S516/01

Claims Analysis

Total Claims: 15
Claim 1
Independent Claim 56 words
Process of solubilizing a material which is an alkali metal, an alkali metal salt or an alkaline earth metal salt, which comprises contacting the material with open-chain polyethyleneglycoldiether of the formula RO--[CH.sub.2 CH.sub.2 O].sub.n R' wherein n = 6 or more and R and R' are identical or different and each is alkyl, aryl or cycloalkyl.
Claim 2
Dependent Claim 56 words
Process of solubilizing a material which is an alkali metal, an alkali metal salt or an alkaline earth metal salt, which comprises contacting the material with open-chain polyethyleneglycoldiether of the formula RO--[CH.sub.2 CH.sub.2 O].sub.n R' wherein n = 6 or more and R and R' are identical or different and each is alkyl, aryl or cycloalkyl.
Claim 3
Dependent Claim 24 words
Process of claim 1, wherein said ether is contained in an organic solvent and increases the solubility of the material in the organic solvent.
Claim 4
Dependent Claim 24 words
Process of claim 1, wherein said ether is contained in an organic solvent and the conductivity in the solvent is increased by the material.
Claim 5
Dependent Claim 37 words
Process of claim 1, wherein the material is a salt and the ether containing the dissolved salt is contacted with a compound different from the salt for a substitution reaction between said dissolved salt and said compound.
Claim 6
Dependent Claim 11 words
Process of claim 1, wherein said material is an alkali metal.
Claim 7
Dependent Claim 42 words
Process of claim 1, wherein the material is dissolved in the ether at less than 60° C., and following dissolution of the material in the ether, the material is at least partially separated from the ether by heating to above 60° C.
Claim 8
Dependent Claim 11 words
Process of claim 5, wherein the heating is to 60°-250° C.
Claim 9
Dependent Claim 12 words
Process of claim 1, wherein the salt is an alkali metal salt.
Claim 10
Dependent Claim 13 words
Process of claim 1, wherein the salt is an alkaline earth metal salt.
Claim 11
Dependent Claim 11 words
Process of claim 1, wherein the salt is an organic salt.
Claim 12
Dependent Claim 13 words
Process of claim 1, wherein the salt is an organic alkali metal salt.
Claim 13
Dependent Claim 8 words
Process of claim 1, wherein n is 7-45.
Claim 14
Dependent Claim 10 words
Process of claim 1, wherein n is at least 7.
Claim 15
Dependent Claim 12 words
Process of claim 4, wherein said material is an alkali metal salt.

References Cited (Backward Citations)

US3684707A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1981-09-11 1982-03-13 1982-09-12 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1985-09-11 1986-03-13 1986-09-12 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1989-09-11 1990-03-13 1990-09-12 $7700.00 Window Closed / Lapsed

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