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US4107339A Expired / Lapsed US ⏱️ 0.0 years remaining

Soluble coffee process and product

Assignee: Mondelez UK Ltd
•
Filing: 1977-07-26
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Granted: 1978-08-15
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Expires: 1997-07-26
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Abstract

Abstract Soluble coffee process involving the addition of a partial condensate of volatile flavorful components to a concentrated coffee extract which has previously been stripped of its volatile flavorful components and subjecting this enhanced concentrated coffee extract to a dehydration process which maximizes the retention of the flavorful components to provide a soluble coffee product with distinct green/nutty flavor notes.

Inventors

  • 👤 Brian Clifford Shrimpton

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-05 17:03
CPC Classifications
A; A23; A23F; A23F5/00; A23F5/46; A23F5/48; A23F5/50; A23F5/505; A23F5/24; A23F5/28; A23F5/34

Claims Analysis

Total Claims: 7
Claim 1
Independent Claim 251 words
In a process for the preparation of soluble coffee powder obtained by dehydrating an aqueous roasted and ground coffee extract, the improvements which comprise; a. evaporatively stripping the volatile flavourful components from the aqueous coffee extract in an evaporation zone at an absolute pressure ranging from 16 inches mercury to atmospheric pressure and vaporizing 5 to 15% of the water in the aqueous coffee extract, said water vapour containing the stripped flavourful coffee components; b. partially condensing the stripped volatile flavourful components-containing water vapour mixture in a condensing zone at an absolute pressure ranging from 16 inches mercury to atmospheric pressure, the condensate as it exits from the condensing zone is within a temperature range from 33° F to 70° F to recover an aqueous solution of condensed flavourful and aroma component; c. concentrating the stripped aqueous coffee extract from step (a) to form a concentrated coffee extract having a solids content ranging from 37% to 55% (w/w); d. admixing the aqueous solution of flavourful components of step (b) with the concentrated coffee extract of step (c); e. feeding the mixture of step (d) to a spray dryer within a temperature range from 27° F to 200° F; f. spray drying the mixture of step (e) at a droplet size of between 100 and 300 microns using a spray drying nozzle pressure of from 700 to 2500 psig, an inlet air temperature of between 250° F and 550° F and an outlet air temperature of between 180° F and 230° F.
Claim 2
Dependent Claim 251 words
In a process for the preparation of soluble coffee powder obtained by dehydrating an aqueous roasted and ground coffee extract, the improvements which comprise; a. evaporatively stripping the volatile flavourful components from the aqueous coffee extract in an evaporation zone at an absolute pressure ranging from 16 inches mercury to atmospheric pressure and vaporizing 5 to 15% of the water in the aqueous coffee extract, said water vapour containing the stripped flavourful coffee components; b. partially condensing the stripped volatile flavourful components-containing water vapour mixture in a condensing zone at an absolute pressure ranging from 16 inches mercury to atmospheric pressure, the condensate as it exits from the condensing zone is within a temperature range from 33° F to 70° F to recover an aqueous solution of condensed flavourful and aroma component; c. concentrating the stripped aqueous coffee extract from step (a) to form a concentrated coffee extract having a solids content ranging from 37% to 55% (w/w); d. admixing the aqueous solution of flavourful components of step (b) with the concentrated coffee extract of step (c); e. feeding the mixture of step (d) to a spray dryer within a temperature range from 27° F to 200° F; f. spray drying the mixture of step (e) at a droplet size of between 100 and 300 microns using a spray drying nozzle pressure of from 700 to 2500 psig, an inlet air temperature of between 250° F and 550° F and an outlet air temperature of between 180° F and 230° F.
Claim 3
Dependent Claim 67 words
A process as claimed in claim 1, wherein the mixture of step (d), having a soluble solids content of 35 to 37%, is cooled to 40° F to 50° F and is spray dried using a spray drying nozzle pressure of 700 psig to 1000 psig, an inlet air temperature of 420° F to 460° F and an outlet air temperature of 190° F to 210° F.
Claim 4
Dependent Claim 38 words
A process as claimed in claim 1, wherein 0.2 to 2 cubic feet under standard pressure and temperature conditions of non-condensable gases are introduced into the condenser zone per one pound of condensate exiting from the condenser zone.
Claim 5
Dependent Claim 84 words
A process as claimed in claim 1, wherein further to the spray drying of step (f) the spray dried coffee soluble solids are milled to an average particle size of less than 50 microns and agglomerated by steam fusing the milled particles at a temperature ranging from 100° F to 250° F to form granules of coffee soluble solids having a moisture content of 4% to 7%, screening the granules and gently after-drying the desired screened fraction to a final moisture content of 3.5%.
Claim 6
Dependent Claim 22 words
A process as claimed in claim 4, including the step of plating the resulting after dried granules with expressed coffee aroma oil.
Claim 7
Dependent Claim 35 words
A process as claimed in claim 1, wherein the stripped volatile flavourful component - containing water vapour mixture is condensed in a two-stage condensing zone the second stage condensing zone being maintained at atmospheric pressure.

References Cited (Backward Citations)

US3809781A Cited
US3965269A Cited
US4045586A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1981-08-14 1982-02-13 1982-08-15 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1985-08-14 1986-02-13 1986-08-15 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1989-08-14 1990-02-13 1990-08-15 $7700.00 Window Closed / Lapsed

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