US4101414A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Rerefining of used motor oils
Assignee: Estech Specialty Chemicals Corp
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Filing: 1975-09-02
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Granted: 1978-07-18
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Expires: 1995-09-02
Abstract
Abstract Screened and drained used lubricating oil stock is predistilled in a steam stripping still for about 4 hours or more. The thus predistilled used oil then flows to an evaporator for a vacuum distillation at a temperature below the cracking temperature of the stock, about 480°-650° F., to effect an evaporation of the used lubricating oil and its separation from a concentrate by-product of heavy lube hydrocarbons and additives.
Inventors
- 👤 Yang J. Kim
- 👤 Belton R. Williams
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-26 20:28
CPC Classifications
C; C10; C10M; C10M175/00; C10M175/0025; C10M175/0033
Claims Analysis
Total Claims: 15
Claim 1
Independent Claim
137 words
A method for rerefining used lubricating oils, comprising the steps of: predistilling a used oil stock by steam stripping said stock within the range of between about 480° F. and about 650° F. and below the cracking temperature thereof for at least 4 hours, said predistilling step removing NO x gases, a light oil component and residual water from the stock to leave a predistilled stock; thereafter vacuum distilling the predistilled stock at below the cracking temperature thereof in a high vacuum environment, said vacuum distilling step including forming a thin film of the predistilled stock on a heated surface and wiping said film to assist in evaporating the stock and to avoid coking, fouling and buildup of impurities, and said vacuum distilling step including vaporizing a vacuum distilled stock to separate it from a viscous concentrate.
Claim 2
Independent Claim
137 words
A method for rerefining used lubricating oils, comprising the steps of: predistilling a used oil stock by steam stripping said stock within the range of between about 480° F. and about 650° F. and below the cracking temperature thereof for at least 4 hours, said predistilling step removing NO x gases, a light oil component and residual water from the stock to leave a predistilled stock; thereafter vacuum distilling the predistilled stock at below the cracking temperature thereof in a high vacuum environment, said vacuum distilling step including forming a thin film of the predistilled stock on a heated surface and wiping said film to assist in evaporating the stock and to avoid coking, fouling and buildup of impurities, and said vacuum distilling step including vaporizing a vacuum distilled stock to separate it from a viscous concentrate.
Claim 3
Dependent Claim
22 words
The method of claim 1 wherein said high vacuum environment is within the range from about 0.1 to about 2.0 mm Hg.
Claim 4
Dependent Claim
27 words
The method of claim 1 wherein said predistilling temperature and said vacuum distillation temperature are each within the range of about 480° F. to about 650° F.
Claim 5
Dependent Claim
15 words
The method of claim 1 wherein said predistilling is carried out at approximately atmospheric pressure.
Claim 6
Dependent Claim
28 words
The method of claim 1 further comprising distilling said vacuum distilled stock in the presence of a clay, filtering the clay distilled stock; and collecting the filtered stock.
Claim 7
Dependent Claim
46 words
The method of claim 1 further comprising treating the vacuum distilled stock with a strong acid or base to form and remove a sludge therefrom; distilling the chemically treated stock in the presence of a clay; filtering the clay distilled stock; and collecting the filtered stock.
Claim 8
Dependent Claim
39 words
The method of claim 1 wherein said predistilling step is preceded by a flashing step including heating the stock to approximately 100-200° F., permitting materials volatile at this temperature to expand to gases, and collecting and incinerating said gases.
Claim 9
Dependent Claim
22 words
The method of claim 1, further comprising collecting said separated viscous concentrate as a useful by-product having a very low vapor pressure.
Claim 10
Dependent Claim
138 words
A viscous concentrate formed by the steps of: predistilling a used lubricating oil stock by steam stripping said stock at a temperature between about 480° F. and about 650° F. and below the cracking temperature thereof for at least 4 hours, said predistilling step removing NO x gases, a light oil component and residual water from the stock to leave a predistilled stock; thereafter vacuum distilling the predistilled stock by forming a thin film of the predistilled stock on a heated surface and wiping said film to assist in evaporating the stock and to avoid coking, fouling and buildup of impurities, said vacuum distilled taking place below the cracking temperature of the predistilled stock in a high vacuum environment, whereby a viscous concentrate is formed and removed from a vaporized, vacuum distilled stock; and collecting said viscous concentrate.
Claim 11
Dependent Claim
138 words
A viscous concentrate formed by the steps of: predistilling a used lubricating oil stock by steam stripping said stock at a temperature between about 480° F. and about 650° F. and below the cracking temperature thereof for at least 4 hours, said predistilling step removing NO x gases, a light oil component and residual water from the stock to leave a predistilled stock; thereafter vacuum distilling the predistilled stock by forming a thin film of the predistilled stock on a heated surface and wiping said film to assist in evaporating the stock and to avoid coking, fouling and buildup of impurities, said vacuum distilled taking place below the cracking temperature of the predistilled stock in a high vacuum environment, whereby a viscous concentrate is formed and removed from a vaporized, vacuum distilled stock; and collecting said viscous concentrate.
Claim 12
Dependent Claim
31 words
The viscous concentrate of claim 9 wherein said concentrate is an anti-corrosion concentrate suitable for coating vehicle frames and the lubricating oil stock contains heavy lube hydrocarbons, additives and metal compounds.
Claim 13
Dependent Claim
18 words
The concentrate of claim 10 wherein the additives and metal components remain substantially unaltered during the processing steps.
Claim 14
Dependent Claim
23 words
The anti-corrosion concentrate of claim 10 wherein the concentrate has a viscosity within the range of 4,000 to 20,000 SUS at 210° F.
Claim 15
Dependent Claim
22 words
The anti-corrosion concentrate of claim 10 in diluted form with a petroleum solvent making it easily adaptable to spray or aerosol applications.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1981-07-17 | 1982-01-16 | 1982-07-18 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1985-07-17 | 1986-01-16 | 1986-07-18 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1989-07-17 | 1990-01-16 | 1990-07-18 | $7700.00 | Window Closed / Lapsed |