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US4101303A Expired / Lapsed US ⏱️ 0.0 years remaining

Perforate glass structures and method of making the same

Assignee: International Telephone and Telegraph Corp
•
Filing: 1970-12-21
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Granted: 1978-07-18
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Expires: 1990-12-21
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Abstract

Abstract A channel-type electron multiplier made in the shape of a glass wafer having holes through a central portion thereof, and an imperforate glass border fused to the periphery of the wafer, the wafer glass having a thermal coefficient of expansion less than that of the border glass. In manufacture, a brief fast cooling step aids in the production of a strong, permanent bond between wafer and border.

Inventors

  • 👤 John Treagus Balkwill

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-06 04:09
CPC Classifications
H; H01; H01J; H01J9/00; H01J9/02; H01J9/12; H01J9/125; C; C03; C03B; C03B23/00; C03B23/20; C03B23/207; C03B25/00; C03B25/02; C03B37/00; C03B37/01; C03B37/02; C03B37/025; C03B37/028; C03B37/10; C03B37/14; C03B37/15; C03B2203/00; C03B2203/02; C03B2203/04; C03B2203/10; C03B2203/12; H01J2201/00; H01J2201/32

Claims Analysis

Total Claims: 5
Claim 1
Independent Claim 260 words
A method of making a perforate glass plate comprising the steps of: heating and drawing a first glass rod and a surrounding first glass tube to a smaller diameter, said first glass tube having a given thermal expansion coefficient; cutting said drawn first rod and tube into equal lengths; packing a hexagon mold full of said rod and tube lengths with said rod and tube lengths parallel; heating said mold to tack said tubes together; heating and drawing said tacked tubes and rods to a smaller size hexagon; cutting said smaller hexagon into equal lengths; placing said hexagon lengths in parallel positions inside a second glass tube; heating and evacuating said second glass tube to force it into contact with and fuse with said hexagon lengths to make a first boule; grinding off said second tube to make said first boule have a cylindrical surface; inserting said ground first boule into a third glass tube having a larger thermal expansion coefficient than said first tube; heating said ground first boule and said third tube and evacuating said third tube to force it into contact with said ground first boule and cause said ground first boule and said third glass tube to fuse together to make a second boule; slicing said second boule in a plane transverse to its axis to produce a thin wafer; removing said rod glass from said wafer by etching to form a plurality of holes therethrough; and heating said etched wafer in a hydrogen atmosphere so that said third glass tube remains fused to said wafer.
Claim 2
Independent Claim 260 words
A method of making a perforate glass plate comprising the steps of: heating and drawing a first glass rod and a surrounding first glass tube to a smaller diameter, said first glass tube having a given thermal expansion coefficient; cutting said drawn first rod and tube into equal lengths; packing a hexagon mold full of said rod and tube lengths with said rod and tube lengths parallel; heating said mold to tack said tubes together; heating and drawing said tacked tubes and rods to a smaller size hexagon; cutting said smaller hexagon into equal lengths; placing said hexagon lengths in parallel positions inside a second glass tube; heating and evacuating said second glass tube to force it into contact with and fuse with said hexagon lengths to make a first boule; grinding off said second tube to make said first boule have a cylindrical surface; inserting said ground first boule into a third glass tube having a larger thermal expansion coefficient than said first tube; heating said ground first boule and said third tube and evacuating said third tube to force it into contact with said ground first boule and cause said ground first boule and said third glass tube to fuse together to make a second boule; slicing said second boule in a plane transverse to its axis to produce a thin wafer; removing said rod glass from said wafer by etching to form a plurality of holes therethrough; and heating said etched wafer in a hydrogen atmosphere so that said third glass tube remains fused to said wafer.
Claim 3
Dependent Claim 51 words
The invention as defined in claim 1, wherein the glass of said first tube has a thermal expansion coefficient of about 90 × 10 -7 inch per degree Centigrade, and the glass of said third tube has a thermal expansion coefficient of about 93 × 10 -7 inch per degree Centigrade.
Claim 4
Dependent Claim 33 words
The invention as defined in claim 1, wherein said rod glass is of a type which can be etched by hydrochloric acid from said first and third tubed glasses without etching the latter.
Claim 5
Dependent Claim 58 words
The invention as defined in claim 1, wherein said second boule is cooled after the said heating thereof about 100° C. from the fusion temperature of said first and third tube glasses within a period of from about 1 to 2 minutes, and cooled to room temperature thereafter at a rate less than about 100° C. per hour.

References Cited (Backward Citations)

US3226589A Cited
US3216807A Cited
US3224851A Cited
US3294504A Cited
US3380817A Cited
US3502455A Cited
US3558377A Cited
US3551228A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1981-07-17 1982-01-16 1982-07-18 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1985-07-17 1986-01-16 1986-07-18 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1989-07-17 1990-01-16 1990-07-18 $7700.00 Window Closed / Lapsed

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