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US4100240A Expired / Lapsed US ⏱️ 0.0 years remaining

Liquid polymer extrusion process and product

Assignee: Dow Silicones Corp
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Filing: 1976-09-30
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Granted: 1978-07-11
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Expires: 1996-09-30
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Abstract

Abstract In accordance with a preferred embodiment of this invention there is provided a process for extruding an oriented-fiber reinforced tubular product. This product preferably is formed from a crosslinked polysiloxane elastomer produced by the curing of a fiber containing "liquid polymer" polysiloxane precursor. The subject process involves pumping the fiber containing precursor through a heated non-pumping extruder. The extruder initiates the curing reaction, shapes the reacting precursor into a tubular form and orients the fibers.

Inventors

  • 👤 Giovanni Bassani

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-28 11:57
CPC Classifications
B; B29; B29C; B29C48/00; B29C48/25; B29C48/30; B29C48/32; B29C48/33; B29C48/022; B29C48/03; B29C48/09; B29K; B29K2101/00; B29K2101/10; B29K2105/00; B29K2105/06; B29K2105/12; B29K2301/00; B29K2301/10; B29K2709/00; B29K2709/08; Y; Y10; Y10T; Y10T428/00; Y10T428/13; Y10T428/1352; Y10T428/1372

Claims Analysis

Total Claims: 4
Claim 1
Independent Claim 195 words
A method of forming an oriented-fiber reinforced elastomeric tubular product by continuously extruding a liquid polymer precursor, said method employing a heated non-pumping extruder having rotatable forming surfaces to shape the precursor as it cures into said tubular product, said precursor being characterized by a room temperature Brookfield viscosity in the range of from 20 to 4000 centipoise and a cure time when heated to from about 150° to 250° C. of about 3 to about 1/2 seconds and wherein said non-pumping extruder the fibers are oriented to both provide increased strength to the tubular product and to facilitate said method by adding strength to the semi-cured extrudate as it emerges from said non-pumping extruder; said method comprising the steps of: (a) pumping said fiber containing liquid polymer precursor through said non-pumping extruder which is heated to initiate the curing reaction said precursor having a residence time in said extruder such that as the curing precursor emerges from the die it has reached a substantially self-sustaining state; and simultaneously (b) rotating at least one of the forming surfaces to orient said fibers; and (c) heating the semi-cured extrudate to drive the curing reaction toward completion.
Claim 2
Independent Claim 195 words
A method of forming an oriented-fiber reinforced elastomeric tubular product by continuously extruding a liquid polymer precursor, said method employing a heated non-pumping extruder having rotatable forming surfaces to shape the precursor as it cures into said tubular product, said precursor being characterized by a room temperature Brookfield viscosity in the range of from 20 to 4000 centipoise and a cure time when heated to from about 150° to 250° C. of about 3 to about 1/2 seconds and wherein said non-pumping extruder the fibers are oriented to both provide increased strength to the tubular product and to facilitate said method by adding strength to the semi-cured extrudate as it emerges from said non-pumping extruder; said method comprising the steps of: (a) pumping said fiber containing liquid polymer precursor through said non-pumping extruder which is heated to initiate the curing reaction said precursor having a residence time in said extruder such that as the curing precursor emerges from the die it has reached a substantially self-sustaining state; and simultaneously (b) rotating at least one of the forming surfaces to orient said fibers; and (c) heating the semi-cured extrudate to drive the curing reaction toward completion.
Claim 3
Independent Claim 196 words
A method of forming an oriented-fiber reinforced elastomeric polysiloxane tubular product by continuously extruding a liquid polymer polysiloxane precursor, said metod employing a heated non-pumping extruder having rotatable forming surfaces to form the precursor as it cures into said tubular product, said precursor being characterized by a room temperature visocity in the range of from 20 to 4000 centipoise and a cure time when heated to from about 150° to 250° C. of about 3 to about 1/2 seconds and wherein said non-pumping extruder the fibers are oriented to both provide increased strength to the tubular product and to facilitate said method by adding strength to the semi-cured extrudate as it emerges from said non-pumping extruder; said method comprising the steps of: (a) pumping said fiber containing liquid polymer precursor through said non-pumping extruder which is heated to initiate the curing reaction said precursor having a residence time in said extruder such that as the curing precursor emerges from the die it has reached a substantially self-sustaining state; and simulatenously (b) rotating at least one of the forming surfaces to orient said fibers; and (c) heating the semi-cured extrudate to drive the curing reaction toward completion.
Claim 4
Independent Claim 196 words
A method of forming an oriented-fiber reinforced elastomeric polysiloxane tubular product by continuously extruding a liquid polymer polysiloxane precursor, said metod employing a heated non-pumping extruder having rotatable forming surfaces to form the precursor as it cures into said tubular product, said precursor being characterized by a room temperature visocity in the range of from 20 to 4000 centipoise and a cure time when heated to from about 150° to 250° C. of about 3 to about 1/2 seconds and wherein said non-pumping extruder the fibers are oriented to both provide increased strength to the tubular product and to facilitate said method by adding strength to the semi-cured extrudate as it emerges from said non-pumping extruder; said method comprising the steps of: (a) pumping said fiber containing liquid polymer precursor through said non-pumping extruder which is heated to initiate the curing reaction said precursor having a residence time in said extruder such that as the curing precursor emerges from the die it has reached a substantially self-sustaining state; and simulatenously (b) rotating at least one of the forming surfaces to orient said fibers; and (c) heating the semi-cured extrudate to drive the curing reaction toward completion.

References Cited (Backward Citations)

US3279501A Cited
US3651187A Cited
US3697473A Cited
US3953006A Cited
US4057610A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1981-07-10 1982-01-09 1982-07-11 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1985-07-10 1986-01-09 1986-07-11 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1989-07-10 1990-01-09 1990-07-11 $7700.00 Window Closed / Lapsed

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