Abstract In a nuclear magnetic resonance spectrometer, the probe structure includes an analysis channel RF magnetic coil disposed in RF magnetic field exchanging relation with a sample of gyromagnetic resonators under analysis for detecting nuclear magnetic resonance of the sample. A control group of nuclear magnetic resonators is also disposed in the sample region and nuclear magnetic resonance of the control group is excited and detected by a second RF magnetic coil. The control RF coil is formed and arranged relative to the sample RF magnetic coil to minimize cross coupling between the sample and control channels. In a preferred embodiment, the control RF magnetic coil is coaxially disposed of the analysis RF coil and is further segmented into a pair of axially spaced portions disposed at opposite ends of the analysis coil and connected in magnetic field bucking relation relative to each other so that the RF magnetic field generated by the control RF coil cancels in the region of the analysis RF coil.
In a nuclear magnetic resonance spectrometer of the type having an analysis channel and a control channel coupled in radio frequency magnetic field exchanging relation via separate analyzing and control radio frequency coil means to a common region for containing both an analysis group of nuclear magnetic resonators and a control group of nuclear magnetic resonators for controlling the resonance conditions of both groups, the improvement wherein: said control radio frequency coil means is formed and arranged relative to said analysis radio frequency coil means so that one of said coil means includes first and second spaced portions wound on a common axis for flow of the radio frequency current therethrough such that the RF magnetic field region produced by said spaced portions of said one coil means are in opposite directions within the region bounded by said other coil means.
Claim 2
Dependent Claim
141 words
In a nuclear magnetic resonance spectrometer of the type having an analysis channel and a control channel coupled in radio frequency magnetic field exchanging relation via separate analyzing and control radio frequency coil means to a common region for containing both an analysis group of nuclear magnetic resonators and a control group of nuclear magnetic resonators for controlling the resonance conditions of both groups, the improvement wherein: said control radio frequency coil means is formed and arranged relative to said analysis radio frequency coil means so that one of said coil means includes first and second spaced portions wound on a common axis for flow of the radio frequency current therethrough such that the RF magnetic field region produced by said spaced portions of said one coil means are in opposite directions within the region bounded by said other coil means.
Claim 3
Dependent Claim
28 words
The apparatus of claim 1 wherein said analysis coil means is said other coil means and is disposed in between said spaced portions of said control coil means.