US4089848A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Extraction of protein food values from oats
Assignee: DuPont Canada Inc
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Filing: 1976-02-02
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Granted: 1978-05-16
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Expires: 1996-02-02
Abstract
Abstract A process for the extraction of food values from oats is disclosed. Acid-soluble protein may be obtained by de-oiling comminuted groats, treating the de-oiled groats with an aqueous solution of pH 9.5-11.5, acidifying the alkaline solution after separation of insoluble material to a pH of 1.8-3.2, preferably 2.2-2.8, and separating acid-soluble protein from the acidified solution after separation of insoluble material. Each step in the process is controlled so as to minimize denaturing of acid-soluble protein. Techniques for separation of acid-soluble protein from the acidified solution are disclosed. The separation of other protein products, bran, flour and gum is also disclosed. The use of protein products as emulsifying agents is disclosed.
Inventors
- 👤 Albert Bell
- 👤 John Roger Brooke Boocock
- 👤 Richard Walton Oughton
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-23 20:16
CPC Classifications
A; A23; A23J; A23J1/00; A23J1/12
Claims Analysis
Total Claims: 15
Claim 1
Independent Claim
98 words
A process for the separation of acid-soluble protein from oats comprising the steps of: a. comminuting dehulled oats, b. extracting oil from the comminuted groats so obtained using an organic solvent for the oil, c. treating the de-oiled groats so obtained at least once with an aqueous alkaline solution of pH 9.5-11.5 and separating the insoluble material therefrom, d. acidifying the alkaline solution so obtained to a pH of 1.8-3.2 and separating the acid-insoluble material therefrom, and e. separating acid-soluble protein from the solution of acid-soluble material, whereby an acid-soluble protein that is not significantly denatured is obtained.
Claim 2
Dependent Claim
98 words
A process for the separation of acid-soluble protein from oats comprising the steps of: a. comminuting dehulled oats, b. extracting oil from the comminuted groats so obtained using an organic solvent for the oil, c. treating the de-oiled groats so obtained at least once with an aqueous alkaline solution of pH 9.5-11.5 and separating the insoluble material therefrom, d. acidifying the alkaline solution so obtained to a pH of 1.8-3.2 and separating the acid-insoluble material therefrom, and e. separating acid-soluble protein from the solution of acid-soluble material, whereby an acid-soluble protein that is not significantly denatured is obtained.
Claim 3
Dependent Claim
56 words
The process of claim 1 in which the step of separating acid-soluble protein from the solution of acid-soluble material is selected from the group consisting of (i) increasing the pH of the solution of acid-soluble material to 4.2-4.8 and separating the precipitate of acid-soluble protein so formed, and (ii) freeze drying the solution of acid-soluble material.
Claim 4
Dependent Claim
33 words
The process of claim 2 in which, in step (b), the organic solvent is selected from the group consisting of hexane, cyclohexane, commercial heptane and aliphatic alcohols of 1 to 6 carbon atoms.
Claim 5
Dependent Claim
33 words
The process of claim 3 in which, in step (c), the alkaline solution is a solution of an alkali selected from the group consisting of alkali metal hydroxides, calcium hydroxide and ammonium hydroxide.
Claim 6
Dependent Claim
36 words
The process of claim 4 in which, in step (d), the alkaline solution is acidified with a solution of an acid selected from the group consisting of phosphoric acid, hydrochloric acid, fumaric acid and citric acid.
Claim 7
Dependent Claim
40 words
The process of claim 2 in which the step of separating acid-soluble protein from the solution of acid-soluble material comprises increasing the pH of the solution of acid-soluble material to 4.2-4.8 and separating the precipitate of acid-soluble protein so formed.
Claim 8
Dependent Claim
52 words
The process of claim 6 in which in step (b) the organic solvent is selected from the group consisting of hexane, commercial heptane, 2-propanol and 1-butanol, in step (c) the alkaline solution is a solution of sodium or potassium hydroxide and in step (d) the acid is phosphoric acid or hydrochloric acid.
Claim 9
Dependent Claim
17 words
The process of claim 7 in which the solvent is hexane and the acid is phosphoric acid.
Claim 10
Dependent Claim
25 words
The process of claim 2 in which the step of separating acid-soluble protein from the acid-soluble material comprises freeze drying the solution of acid-soluble material.
Claim 11
Dependent Claim
52 words
The process of claim 9 in which in tep (b) the organic solvent is selected from the group consisting of hexane, commercial heptane, 2-propanol and 1-butanol, in step (c) the alkaline solution is a solution of sodium or potassium hydroxide and in step (d) the acid is phosphoric acid or hydrochloric acid.
Claim 12
Dependent Claim
17 words
The process of claim 10 in which the solvent is hexane and the acid is phosphoric acid.
Claim 13
Dependent Claim
17 words
The process of claim 2 in which the de-oiled groats is extracted twice with the alkaline solution.
Claim 14
Dependent Claim
29 words
The process of claim 2 in which the insoluble material obtained in step (c) in treated for the separation of fractions comprised of starch, of bran or of gum.
Claim 15
Dependent Claim
17 words
The process of claim 1 in which, in step (d), the pH is in the range 2.2-2.8.
References Cited (Backward Citations)
US2233439A
Cited
US2377853A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1981-05-15 | 1981-11-14 | 1982-05-16 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1985-05-15 | 1985-11-14 | 1986-05-16 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1989-05-15 | 1989-11-14 | 1990-05-16 | $7700.00 | Window Closed / Lapsed |